Formation and properties of cellular foam fibrous material

Patent metadata

Field	Value
Publication number	US-10875979-B2
Application number	US-201816122251-A
Country	US
Kind code	B2
Filing date	Sep 5, 2018
Priority date	Sep 5, 2017
Publication date	Dec 29, 2020
Grant date	Dec 29, 2020

Abstract

A foaming process for converting fibrous material into a cellular foam structure includes mixing fibrous material and a solvent-based binding agent to form a mixture; saturating the mixture with a pressurized gas to form a gas-saturated mixture; expanding the gas-saturated mixture by reducing the pressure of the pressurized gas to form an expanded mixture with voids in the fibrous material; and curing the expanded mixture to set the fibrous material and drive off the solvent to provide a stable network of fibrous material having cushioning properties.

First claim

What is claimed:

1. A foaming process for converting fibrous material into a cellular foam structure, comprising:
mixing fibrous material and a solvent-based binding agent to form a mixture;
saturating the mixture with a pressurized gas to form a pressurized gas-saturated mixture;
reducing the pressure of the pressurized gas-saturated mixture to form a first stage expanded mixture with voids in the mixture; and
forming a second stage expanded mixture by boiling the solvent from the solvent-based binding agent to set the fibrous material and drive off the solvent to form a stable cellular foam structure having cushioning properties.

2. The process of claim 1 , wherein the fibrous material comprises natural or synthetic fibrous material.

3. The process of claim 1 , wherein the natural fibrous material comprises plant or wood fiber.

4. The process of claim 1 , wherein the synthetic fibrous material comprises carbon fiber, metal fiber or polymeric fiber.

5. A foaming process for converting fibrous material into a cellular foam structure, comprising:
mixing fibrous material and a solvent-based binding agent to form a mixture;
saturating the mixture with a pressurized gas to form a pressurized gas-saturated mixture;
expanding the gas-saturated mixture by reducing the pressure of the pressurized gas to form an expanded mixture with voids in the mixture; and
curing the expanded mixture to set the fibrous material and drive off the solvent to form a stable cellular foam structure having cushioning properties, wherein the solvent comprises water, methanol, acetone, denatured alcohol, D-limonene, toluene, xylene or dimethyl sulfoxide.

6. A foaming process for converting fibrous material into a cellular foam structure, comprising:
mixing fibrous material and a solvent-based binding agent to form a mixture;
saturating the mixture with a pressurized gas to form a pressurized gas-saturated mixture;
expanding the gas-saturated mixture by reducing the pressure of the pressurized gas to form an expanded mixture with voids in the mixture; and

curing the expanded mixture to set the fibrous material and drive off the solvent to form a stable cellular foam structure having cushioning properties, wherein the binding agent comprises natural rubber, thermal plastic urethane, starch, dextrin, animal glue, casein adhesives or synthetic emulsions.

7. The process of claim 5 , wherein the solvent-based binding agent comprises a water-natural latex combination.

8. The process of claim 1 , wherein the inert gas comprises nitrogen.

9. A batch foaming process for converting fibrous material into a cellular foam structure, comprising:
mixing fibrous material and a solvent-based binding agent to form a mixture;
placing the mixture into a mold;
placing the mold into a pressure vessel, wherein the mold comprises holes that allow the exchange of pressure and solvent between the mixture and the pressure vessel and constrains the expansion of the mixture;
pressurizing the pressure vessel to saturate the mixture with an inert gas to form a gas-saturated mixture and foam the mixture in the mold;
releasing the pressure in the pressure vessel to create voids in the foamed fibrous material; and
curing the foamed fibrous material to preserve the foamed structure and cross-linking the fibers of the fibrous material to provide a stable network of fibrous material having cushioning properties.

10. A continuous foaming process for converting fibrous material into a cellular foam structure, comprising:
mixing a solvent-based binding agent and fibrous material to form a mixture;
feeding the mixture into a screw driven extruder;
saturating the mixture in the extruder with high pressure inert gas;
extruding the saturated mixture from an exit nozzle of the extruder where the mixture undergoes primary expansion through pressure drop; and
transferring the expanded mixture into a vacuum tunnel under controlled temperature where the mixture undergoes secondary expansion, curing and stabilizing of the cellular structure of the foamed product.

11. The process of claim 1 , wherein the solvent comprises water, methanol, acetone, denatured alcohol, D-limonene, toluene, xylene or dimethyl sulfoxide.

12. The process of claim 1 , wherein the binding agent comprises natural rubber, thermal plastic urethane, starch, dextrin, animal glue, casein adhesives or synthetic emulsions.

13. The process of claim 1 , wherein the solvent-based binding agent comprises a water-natural latex combination.

14. The process of claim 1 , wherein the second stage expansion is initiated by a vacuum.

15. The process of claim 9 , wherein the fibrous material comprises natural or synthetic fibrous material.

16. The process of claim 9 , wherein the natural fibrous material comprises plant or wood fiber.

17. The process of claim 9 , wherein the synthetic fibrous material comprises carbon fiber, metal fiber or polymeric fiber.

18. The process of claim 9 , wherein the solvent comprises water, methanol, acetone, denatured alcohol, D-limonene, toluene, xylene or dimethyl sulfoxide.

19. The process of claim 9 , wherein the binding agent comprises natural rubber, thermal plastic urethane, starch, dextrin, animal glue, casein adhesives or synthetic emulsions.

20. The process of claim 9 , wherein the solvent-based binding agent comprises a water-natural latex combination.

21. The process of claim 10 , wherein the fibrous material comprises natural or synthetic fibrous material.

22. The process of claim 10 , wherein the natural fibrous material comprises plant or wood fiber.

23. The process of claim 10 , wherein the synthetic fibrous material comprises carbon fiber, metal fiber or polymeric fiber.

24. The process of claim 10 , wherein the solvent comprises water, methanol, acetone, denatured alcohol, D-limonene, toluene, xylene or dimethyl sulfoxide.

25. The process of claim 10 , wherein the binding agent comprises natural rubber, thermal plastic urethane, starch, dextrin, animal glue, casein adhesives or synthetic emulsions.

26. The process of claim 10 , wherein the solvent-based binding agent comprises a water-natural latex combination.

Assignees

• Ge Changfeng
• Olles Mark
• Cosgrove Kevin
• Diaz Carlos A
• Rochester Institute Tech

Inventors

• Ge Changfeng
• Olles Mark
• Cosgrove Kevin
• Diaz Carlos A

Classifications

• C08L97/02 Primary

  Lignocellulosic material, e.g. wood, straw or bagasse {(manufacture of articles made from lignocellulosic material by dry processes B27N)} · CPC title

• B29C44/358

  Foamed of foamable fibres · CPC title

• B29C44/3496

  The foam being compressed and later released to expand (B29C44/3465 takes precedence) · CPC title

• C08J9/122

  Hydrogen, oxygen, CO2, nitrogen or noble gases · CPC title

• C08J2201/0504

  the liquid phase being aqueous · CPC title