Processes for analysis and optimization of multiphase separators, particularly in regard to simulated gravity separation of immiscible liquid dispersions

Patent metadata

Field	Value
Publication number	US-10870070-B2
Application number	US-201916363118-A
Country	US
Kind code	B2
Filing date	Mar 25, 2019
Priority date	May 3, 2016
Publication date	Dec 22, 2020
Grant date	Dec 22, 2020

Abstract

The present invention is directed to systems and methods for evaluating performance, performing process control, optimization and design of gravity separation process systems that are used to separate immiscible liquid dispersions (e.g., water-in-oil, oil-in-water mixtures) and emulsions for two-phase (liquid-liquid) or three-phase (gas-liquid-liquid) systems. According to one aspect, the design, simulation and control of such systems is performed using computational fluid dynamics (CFD) software that is configured for determining the separation efficiency of separators on the basis of the true geometry and multidimensional flow field and for a distribution of droplet sizes with the influence of the emulsion concentration on the rheology of the oil-in-water or water-in-oil dispersion. The results of the CFD simulations can be used to adjust input parameters of the separator to maximize the separation efficiency of the separator such that it outputs liquid streams containing minimal amounts of immiscible liquid dispersions.

First claim

What is claimed is:

1. A computer implemented method to evaluate and control the separation performance of a separator for separating a multi-phase, multi-fluid stream consisting of gas and an immiscible liquid dispersion within an internal volume of the separator and outputting one or more streams of processed gas and one or more streams of processed liquids separated from the immiscible liquid dispersion, wherein the one or more streams of processed liquids are selected from the group consisting of a water outlet stream and an oil outlet stream, and wherein the immiscible liquid dispersion includes a continuous or dispersed gas phase, a dispersed liquid phase and a continuous liquid phase within an internal volume of the separator, the method comprising the steps of:
receiving operational input parameters at a hardware processor of a controller computing device, wherein the processor is executing program code that is in the form of one or more software modules and stored in a non-transitory storage medium, and wherein the operational input parameters include:
fluid property data for the immiscible liquid dispersion including one or more of density, viscosity and surface tension, and
static or dynamic settling data for the immiscible liquid dispersion;

generating, with the processor, a computational fluid dynamics (CFD) model of the separator, wherein generating the CFD model includes:
modeling, a droplet size distribution for the dispersed liquid phase within the internal volume as a function of an initial droplet size distribution and the static or dynamic settling data, and
generating a phase interaction model of a phase interaction between the dispersed liquid phase and the continuous liquid phase as a function of the fluid property data;

determining, with the processor based on the CFD model, adjustments to one or more of the operational input parameters, wherein the adjusted one or more operational parameters are determined based on the CFD model to change a separation efficiency of the separator;
controlling, with the processor, the separator according to the adjusted one or more operational input parameters, wherein the controlling step comprises sending, by the processor to the separator over a communication interface, a control signal configured to adjust a setting of one or more of a water outlet stream control valve, an oil outlet stream control valve, an operating temperature of the separator, a demulsifier chemical injection rate, an inlet control valve and a gas outlet control valve, as a function of the adjusted one or more operational input parameters;
monitoring, with the processor, a liquid-liquid separation efficiency of the separator in real-time during operation of the separator using one or more sensors exposed to respective outlet streams, wherein the liquid-liquid separation efficiency is determined by measuring one or more of a fraction of water in the oil outlet stream and a fraction of oil in the water outlet stream; and
dynamically performing, with the processor during operation of the separator based on the monitoring step, the receiving, generating, determining and controlling steps such that the monitored liquid-liquid separation efficiency of the separator is changed and the one or more streams of processed liquids separated from the immiscible liquid dispersion contain less than a prescribed amount of the immiscible liquid dispersion therein.

2. The method of claim 1 , further comprising:
outputting from the separator the one or more streams of processed liquids separated from the immiscible liquid dispersion and containing less than the prescribed amount of the immiscible liquid dispersion therein.

3. The method of claim 1 , wherein the control signal is configured to adjust a setting of one or more of the water outlet stream control valve, the oil outlet stream control valve and the inlet valve to define a liquid level and an interface level within the internal volume as a function of the one or more operational input parameters, and wherein the control signal adjusts the setting of the gas outlet control valve to achieve a pressure within the internal volume as a function of the one or more operational input parameters.

4. The method of claim 1 , wherein the immiscible liquid dispersion comprises an emulsion selected from the group consisting of: an oil in water emulsion, a water in oil emulsion, and wherein the static or dynamic settling data is obtained using a batch bottle test, or continuous flow container testing or separator vessel testing, and wherein the step of receiving the static or dynamic settling data includes monitoring the immiscible liquid dispersion in real-time during operation of the separator to determine a time-varying vertical distribution of a settling or rising phase in the separator.

5. The method of claim 4 , wherein the time varying vertical distribution is determined by the processor using a sensor device provided within one or more of the internal volume of the separator, an inlet stream and the one or more streams of processed liquids of the separator and configured to take one or more of: ultrasonic measurements, gamma densitometry measurements, nuclear magnetic resonance NMR measurements, and electrical tomography measurements of the immiscible liquid dispersion.

6. The method of claim 5 , wherein the time-varying vertical distribution is measured in the separator and utilized by the processor to dynamically perform the steps of generating the CFD model, determining adjustments to one or more of the operational input parameters, and controlling the separator according to the adjusted one or more operational input parameters.

7. The method of claim 4 , further comprising: selecting, with the processor, coalescence and breakage kernels based on the static or dynamic settling data.

8. The method of claim 1 , wherein the fluid property data comprises values or gradients of values for one or more variables including: density, viscosity, surface tension, momentum, velocity, turbulence energy dissipation rate, turbulent kinetic energy, and demulsifier or surfactant concentration.

9. The method of claim 8 , wherein an evolution of the droplet size distribution is modeled as a function of droplet size, coalescence and breakage kernels and one or more of the variables of the fluid property data.

10. The method of claim 1 , further comprising: defining, with the processor, a three-dimensional geometric model of the internal volume of the separator and internal components therein, wherein the internal components include one or more of: inlet devices, perforated plates, baffles, vortex breakers, weirs, coalescer packs, and devices obstructing or partially obstructing a flow of gas and liquid within the internal volume of the separator.

11. The method of claim 10 , further comprising: defining, with the processor, a computational mesh representing the internal volume of the separator.

12. The method of claim 1 , further comprising: determining, for the dispersed liquid phase within the internal volume, a droplet size distribution and wherein an evolution of the droplet size distribution is modeled based on droplet size, droplet coalescence and breakage kernels, and one or more variables of the fluid property data.

13. The method of claim 12 , further comprising: determining, with the processor, the droplet size distribution of the immiscible liquid dispersion contained within the internal volume, and wherein the droplet size distribution is determined based on the evolution of the droplet size distribution.

14. The method of claim 13 , further comprising: measuring one or more of: at l

Assignees

• Saudi Arabian Oil Co

Inventors

• Oshinowo Olanrewaju Malcolm

Classifications

• G16C20/10 Primary

  Analysis or design of chemical reactions, syntheses or processes · CPC title

• B01D21/34

  Controlling the feed distribution; Controlling the liquid level {; Control of process parameters} · CPC title

• B01D17/0211

  with baffles · CPC title

• B01D17/0208

  by sedimentation · CPC title

• G05B13/041

  in which a variable is automatically adjusted to optimise the performance · CPC title