Reactor for gas-liquid mass transfer

Patent metadata

Field	Value
Publication number	US-10865459-B2
Application number	US-202016921992-A
Country	US
Kind code	B2
Filing date	Jul 7, 2020
Priority date	Jan 17, 2018
Publication date	Dec 15, 2020
Grant date	Dec 15, 2020

Abstract

A reactor for gas-liquid mass transfer between a gas and a liquid or slurry includes a tank for receiving the liquid or slurry having a wall; a drive shaft; an upward pumping impeller; and an aerating apparatus disposed above the upward pumping impeller and extending between the drive shaft and the wall of the tank at a first distance (d 1 ) from the drive shaft and at a second distance (d 2 ) from the wall of the tank, the aerating apparatus encircling the drive shaft at least partially. The aerating apparatus has an outward inclined or curved inner surface for directing at least a part of the flow over the inner surface.

First claim

The invention claimed is:

1. A reactor for gas-liquid mass transfer between a gas and a liquid or slurry, the reactor comprising:
a tank for receiving the liquid or slurry, the tank having a wall;
a drive shaft extending vertically in the tank and rotatable about a vertical axis;
an upward pumping impeller for creating a flow of the liquid or slurry received in the tank generally upward and at the surface of the liquid or slurry, the upward pumping impeller being rotatable by the drive shaft and disposed in the upper part of the tank;
an aerating apparatus disposed above the upward pumping impeller; wherein the aerating apparatus extends between the drive shaft and the wall of the tank at a first distance (d 1 ) from the drive shaft and at a second distance (d 2 ) from the wall of the tank, the aerating apparatus encircling the drive shaft at least partially,
the aerating apparatus having a lower edge and an upper edge and, extending between the lower edge and the upper edge, an outward inclined or curved inner surface for directing at least a part of the flow over the inner surface outward from the vertical axis and over the upper edge.

2. The reactor according to claim 1 , wherein the aerating apparatus is immovable relative to the tank.

3. The reactor according to claim 1 , wherein the inner surface is outward inclined at an angle (a) of about 200 to about 80° with respect to the vertical axis.

4. The reactor according to claim 1 , wherein the inner surface of the aerating apparatus continuously encircles the vertical axis, thereby forming a closed perimeter.

5. The reactor according to claim 1 , wherein the distance of the lower edge and the upper edge along the inner surface (d 3 ) is about 0.04 to 0.20 times the width (w) of the tank.

6. The reactor according to claim 1 , wherein the distance of the lower edge and the upper edge in the radial direction (d 4 ) is about 0.03 to 0.18 times the width (w) of the tank.

7. The reactor according to claim 1 , wherein the distance of the lower edge and the upper edge in the vertical direction (d 5 ) is about 0.03 to 0.18 times the width (w) of the tank.

8. The reactor according to claim 1 , wherein the upper edge of the aerating apparatus has projections, indentations, and/or alternating projections and indentations.

9. The reactor according to claim 1 , wherein the reactor further comprises one or more baffles arranged between the wall of the tank and the upward pumping impeller, to which the aerating apparatus is attached.

10. The reactor according to claim 1 , wherein the reactor further comprises a second impeller disposed below the upward pumping impeller.

11. The reactor according to claim 1 , wherein the ratio of the height (h) of the tank to the width (w) of the tank is in the range of 1:2 to 2.5:1, for example 0.7:1 to 2:1.

12. The reactor according to claim 1 , wherein the aerating apparatus is disposed above the upward pumping impeller such that when in use, the aerating apparatus is submerged in the liquid or slurry received in the tank when the upward pumping impeller is activated so as to be rotated by the drive shaft.

13. The reactor according to claim 1 , wherein the distance (d 7 ) in the vertical direction between the upward pumping impeller and the lower edge of the aerating apparatus is 0.1 to 0.8 times the diameter (di) of the upward pumping impeller.

14. The reactor according to claim 1 , wherein when in use, the distance (d 8 ) in the vertical direction between the upward pumping impeller and the surface of the liquid or slurry is 0.2 to 1.5 times the diameter (d 1 ) of the upward pumping impeller.

15. The reactor according to claim 1 , wherein the upward pumping impeller has an outer edge disposed at a distance (d 9 ) of the vertical axis, and wherein the upper edge of the aerating apparatus is disposed at a distance (d 10 ) of the vertical axis that is greater than said distance of the outer edge of the upward pumping impeller.

16. The reactor according to claim 1 , wherein the upward pumping impeller has an outer edge disposed at a distance (d 9 ) of the vertical axis, and wherein the lower edge of the aerating apparatus is disposed at a distance (d 11 ) of the vertical axis that is greater than said distance (d 9 ) of the outer edge of the upward pumping impeller.

17. The reactor according to claim 1 , wherein the reactor is a stirred tank reactor for gas-liquid mass transfer between a gas and a liquid or slurry in a hydrometallurgical application.

18. A plant comprising the reactor according to claim 1 .

19. The plant according to claim 18 , wherein the plant is a hydrometallurgical plant further comprising at least one of the following:
a crushing and/or grinding unit for grinding raw material, such as ore;
a unit for dissolution of the raw material in an aqueous solution for producing the slurry to be received in the tank; and/or
a liquid/solid separation unit for separating residual solids from the slurry received in the tank.

20. A method for gas-liquid mass transfer between a gas and a liquid or slurry, the method comprising providing the liquid or the slurry into a reactor according to claim 1 , and into the tank thereof,
rotating the upward pumping impeller, thereby creating a flow of the liquid or slurry received in
the tank generally upward and at the surface of the liquid or slurry, so that the aerating apparatus is submerged in the liquid or slurry received in the tank; wherein
the aerating apparatus disposed above the upward pumping impeller directs the at least the part of the flow over the inner surface outward from the vertical axis and over the upper edge.

21. The method according to claim 20 , wherein the method is a hydrometallurgical method.

Assignees

• Outotec Finland Oy

Inventors

• Latva-Kokko Marko

Classifications

• B01J19/18 Primary

  Stationary reactors having moving elements inside (B01J19/08, B01J19/26 take precedence) · CPC title

• B01F23/2332 Primary

  the stirrer rotating about a horizontal axis; Stirrers therefor · CPC title

• B01F23/234211

  Stirrers thereof · CPC title

• B01F23/2311

  Mounting the bubbling devices or the diffusers · CPC title

• B01F27/91

  with propellers · CPC title