Molybdenum crucible

Patent metadata

Field	Value
Publication number	US-10858759-B2
Application number	US-201716079733-A
Country	US
Kind code	B2
Filing date	Feb 23, 2017
Priority date	Feb 26, 2016
Publication date	Dec 8, 2020
Grant date	Dec 8, 2020

Abstract

The molybdenum crucible includes a cylindrical side wall and a bottom provided integrally with one end of the side wall. The side wall includes a coarse grain region configured to extend from an outer wall toward an inner wall and a fine grain region configured to extend from the inner wall toward the outer wall so as to be in contact with the coarse grain region. The ratio of the coarse grain region in the side wall in the thickness direction thereof is 10% or more and less than 90%. The coarse grain region is defined as such a region in which crystal grains having a grain size of 1 mm or more determined by an intercept method in the height direction of the crucible occupy 95% or more of an area of a measurement region.

First claim

The invention claimed is:

1. A molybdenum crucible comprising:
a cylindrical side wall; and
a bottom provided integrally with one end of the cylindrical side wall,
the cylindrical side wall including:
a coarse grain region which is defined as in the following and configured to extend from an outer wall toward an inner wall; and
a fine grain region which is defined as in the following and configured to extend from the inner wall toward the outer wall so as to be in contact with the coarse grain region,
a ratio of the coarse grain region in the cylindrical side wall in a thickness direction thereof is 10% or more and less than 90%,
the coarse grain region being defined as such a region in which crystal grains having a grain size of 1 mm or more determined by an intercept method in a height direction of the crucible occupy 95% or more of an area of a measurement region, and
the fine grain region being defined as such a region in which crystal grains having a grain size of 10 μm or more and 500 μm or less determined by the intercept method in the height direction of the crucible occupy 95% or more of an area of a measurement region,
wherein the molybdenum crucible has a purity of 99.9 mass % or more, and consists of only inevitable impurities as a remainder.

2. The molybdenum crucible according to claim 1 , wherein
the ratio of the coarse grain region in the cylindrical side wall in the thickness direction thereof is 40% or more and less than 80%.

3. The molybdenum crucible according to claim 1 , wherein
when the cylindrical side wall is equally divided into 8 parts in the thickness direction from the inner wall side toward the outer wall side, a side-wall outer region which is the seventh part when counted from the inner wall side is the coarse grain region, and
when the cylindrical side wall is equally divided into 8 parts in the thickness direction from the inner wall side toward the outer wall side, a side-wall inner region which is the second part when counted from the inner wall side is the fine grain region.

4. The molybdenum crucible according to claim 3 , wherein
an aspect ratio of crystal grains in the side-wall inner region is 1.0 or more and 2.0 or less.

5. The molybdenum crucible according to claim 3 , wherein
an aspect ratio of crystal grains in the side-wall inner region is 1.0 or more and 1.5 or less.

6. The molybdenum crucible according to claim 1 , wherein
the molybdenum crucible has a Vickers hardness Hv of 140 or more and 190 or less.

7. The molybdenum crucible according to claim 1 , wherein
the molybdenum crucible has a Vickers hardness Hv of 150 or more and 180 or less.

Assignees

• Almt Corp

Inventors

• Watanabe Makoto
• Fukaya Yoshitake
• Katoh Masahiro
• Nishino Hidenobu

Classifications

• F27D1/0006

  Linings or walls formed from bricks or layers with a particular composition or specific characteristics · CPC title

• C22F1/00

  Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working (apparatus for mechanical working of metal B21, B23, B24) · CPC title

• B22F2998/10

  Processes characterised by the sequence of their steps · CPC title

• C22F1/18

  High-melting or refractory metals or alloys based thereon · CPC title

• F27B14/10

  Crucibles · CPC title