Method and materials to convert a drilling mud into a solid gel based lost circulation material

Patent metadata

Field	Value
Publication number	US-10851279-B2
Application number	US-202016812133-A
Country	US
Kind code	B2
Filing date	Mar 6, 2020
Priority date	Nov 27, 2017
Publication date	Dec 1, 2020
Grant date	Dec 1, 2020

Abstract

A convertible composition comprising a nanosilica drilling fluid, the nanosilica drilling fluid comprising an aqueous based drilling mud, where the aqueous based drilling mud comprises water, and an alkaline nanosilica dispersion, where the alkaline nanosilica dispersion comprises nanosilica; and a chemical activator, the chemical activator operable to hydrolyze in the presence of water to produce an acid, where a weight ratio of the alkaline nanosilica dispersion to the chemical activator is between 1 to 0.001 and 1 to 0.25.

First claim

That which is claimed is:

1. A method for producing a solid gel lost circulation material, the method comprising the steps of:
encountering a lost circulation zone in a wellbore,
where the lost circulation zone occurs when a flow rate of a nanosilica drilling fluid introduced to the wellbore is less than the flow rate of the nanosilica drilling fluid returning from the wellbore,
where the nanosilica drilling fluid comprises water and an alkaline nanosilica dispersion;

mixing an amount of a chemical activator into the nanosilica drilling fluid to produce a convertible composition, where the convertible composition has a pH between 8 and 11, where the chemical activator is a water insoluble hydrolysable polyester, where the water insoluble hydrolysable polyester is selected from the group comprising polylactide, polyhydroxyalkanoates, polyglycolide, polylactoglycolide, polycaprolactone, and combinations of the same, where the amount of the chemical activator is operable to maintain a weight ratio between the alkaline nanosilica dispersion and the chemical activator of between 1 to 0.001 and 1 to 0.25;
introducing the convertible composition into the wellbore;
allowing the convertible composition to circulate to the lost circulation zone;
allowing the chemical activator to hydrolyze to produce an acid as the convertible composition circulates to the lost circulation zone;
allowing the acid to reduce the pH of the convertible composition as the convertible composition circulates to the lost circulation zone;
allowing the solid gel lost circulation material to form when the pH of the convertible composition is less than a gel pH; and
allowing the solid gel to fill the lost circulation zone.

2. The method of claim 1 , where the acid is operable to reduce the pH of the convertible composition to less than 7.

3. The method of claim 1 , where the gel pH is less than 7.

4. The method of claim 1 , where the gel pH is achieved after a hydrolysis time, where the hydrolysis time is between 1 hour and 24 hours.

Assignees

• Saudi Arabian Oil Co

Inventors

• Wagle Vikrant
• Al-Yami Abdullah
• Kalgaonkar Rajendra A
• Alsaihati Zainab

Classifications

• C09K8/03 Primary

  Specific additives for general use in well-drilling compositions · CPC title

• E21B31/005

  using vibrating or oscillating means · CPC title

• E21B33/138

  Plastering the borehole wall; Injecting into the formation · CPC title

• C09K8/5045

  containing inorganic compounds · CPC title

• C09K2208/10

  Nanoparticle-containing well treatment fluids · CPC title