Method for producing impregnated pitch from petroleum-based raw material and impregnated pitch produced thereby

Patent metadata

Field	Value
Publication number	US-10844286-B2
Application number	US-201716473336-A
Country	US
Kind code	B2
Filing date	Dec 26, 2017
Priority date	Dec 27, 2016
Publication date	Nov 24, 2020
Grant date	Nov 24, 2020

Abstract

The present invention relates to a method for producing an impregnated pitch from a petroleum-based raw material and to an impregnated pitch produced using the same, and when the method for producing an impregnated pitch according to the present invention is used, it is possible to produce an impregnated pitch having a high carbonization yield (40 wt % or more) and low quinoline insoluble matter (QI, 2% or less) for improving efficiency of an impregnation process from a petroleum-based raw material. Therefore, when an impregnation process is applied to a carbon compact by using the impregnated pitch according to the present invention, it is possible to remarkably reduce micropores inside the carbon compact, and to produce a carbon compact having physical properties such as excellent electrical conductivity and mechanical strength.

First claim

What is claimed is:

1. A method for producing an impregnated pitch comprising the following steps:
heat-treating a petroleum-based raw material in an inert gas atmosphere under the pressure of 10˜40 bar (step 1);
heat-treating the petroleum-based raw material which had been heat-treated in step 1 at normal pressure (step 2); and
distillating the petroleum-based raw material which had been heat-treated in step 2 under reduced pressure (step 3).

2. The method for producing an impregnated pitch according to claim 1 , wherein the heat-treatment in step 1 is performed in a temperature range of 300° C. to 450° C.

3. The method for producing an impregnated pitch according to claim 1 , wherein the heat-treatment in step 1 is performed for 0.5˜10 hours.

4. The method for producing an impregnated pitch according to claim 1 , wherein the heat-treatment in step 2 is performed in a temperature range of 300° C. to 450° C.

5. The method for producing an impregnated pitch according to claim 1 , wherein the heat-treatment in step 2 is performed for 0.5˜10 hours.

6. The method for producing an impregnated pitch according to claim 1 , wherein the distillation under reduced pressure in step 3 is performed in a temperature range of 100° C. to 250° C.

7. The method for producing an impregnated pitch according to claim 1 , wherein the distillation under reduced pressure in step 3 is performed for 0.5˜10 hours.

8. The method for producing an impregnated pitch according to claim 1 , wherein the inert gas is one or more gases selected from the group consisting of nitrogen, helium, neon or argon.

9. The method for producing an impregnated pitch according to claim 1 , wherein the petroleum-based raw material is one or more materials selected from the group consisting of pyrolyzed fuel oil (PFO), naphtha cracking bottom oil (NCB), ethylene cracker bottom oil (EBO), vacuum residue (VR), de-asphalted oil (DAO), atmospheric residue (AR), FCC-DO (fluid catalytic cracking decant oil), RFCC-DO (residue fluid catalytic cracking decant oil) and heavy aromatic oil.

Assignees

• Korea Res Inst Chemical Tech

Inventors

• Kim Jong Gu
• Jeon Young-Pyo
• Im Ji Sun
• Song Byung Jin
• Bai Byong Chol
• Ko Seung Hyun
• Choi Jong Eun

Classifications

• C10C3/06

  by distillation · CPC title

• C10C3/04 Primary

  by blowing or oxidising {, e.g. air, ozone} · CPC title

• C10C3/002 Primary

  by thermal means · CPC title