Method for producing rare-earth magnets, and rare-earth-compound application device

Patent metadata

Field	Value
Publication number	US-10832864-B2
Application number	US-201615570202-A
Country	US
Kind code	B2
Filing date	Apr 18, 2016
Priority date	Apr 28, 2015
Publication date	Nov 10, 2020
Grant date	Nov 10, 2020

Abstract

A coating tank 1 provided with a net belt passage opening is prepared, a slurry obtained by dispersing a rare-earth-compound powder in a solvent is continuously supplied to the coating tank 1 to cause the coating tank 1 to overflow, and a plurality of sintered magnet bodies 10 are arranged on a net belt conveyor 5 , continuously conveyed horizontally thereon, and passed through the slurry in the coating tank 1 via the net belt passage opening, to apply the slurry to the sintered magnet bodies. The slurry is subsequently dried to continuously apply the powder to the plurality of sintered magnet bodies. As a result, the rare-earth-compound powder can be uniformly applied to the surfaces of the sintered magnet bodies, and the application operation can be performed extremely efficiently.

First claim

The invention claimed is:

1. A method for producing rare-earth magnets by applying a powder containing one or at least two selected from an oxide, a fluoride, an oxyfluoride, a hydroxide, or a hydride of R 2 (wherein R 2 represents one or at least two selected from rare-earth elements including Y and Sc) onto sintered magnet bodies made of an R 1 —Fe—B-based composition (wherein R 1 is one or at least two selected from rare-earth elements including Y and Sc) and heat treated to permit R 2 to be absorbed in the sintered magnet bodies, the method comprising:
providing a coating tank having net belt passage openings at two mutually facing side walls individually and a net belt conveyor for conveying the sintered magnet bodies, the net belt conveyor arranged to pass through the net belt passage openings, so that a plurality of the sintered magnet bodies on the net belt conveyor can be continuously conveyed horizontally through the net belt passage openings;
continuously feeding to the coating tank a slurry dispersing the powder in a solvent, so that i) a level of the slurry in the coating tank is held at a position higher than an upper surface of the sintered magnet bodies on the net belt conveyor to immerse the sintered magnet into the slurry, and ii) the slurry continuously overflows from an upper end portion of the coating tank including the net belt passage openings and the level of slurry is continuously maintained to be at a level above a lower part of the net belt passage openings;
placing the plurality of the sintered magnet bodies on the net belt conveyor and continuously conveying the sintered magnet bodies on the net belt conveyor horizontally through the net belt passage openings so that the sintered magnet bodies are immersed into the slurry in the coating tank to apply the slurry to the sintered magnet bodies; and
drying the sintered magnet bodies to remove the solvent of the slurry thereby continuously applying the powder onto the plurality of sintered magnet bodies.

2. The method for producing rare-earth magnets of claim 1 , wherein the sintered magnet bodies are subjected to plural times of an application process in which the sintered magnet bodies are passed into the slurry in the coating tank and dried.

3. The method for producing rare-earth magnets of claim 1 , wherein the sintered magnet bodies are discharged from the coating tank and air is injected against the conveyed sintered magnet bodies to remove drippings therefrom, followed by drying treatment.

4. The method for producing rare-earth magnets of claim 1 , wherein the drying treatment is carried out by injecting air at a temperature within ±50° C. of a boiling point (T B ) of the solvent for the slurry against the rare-earth magnets.

5. The method for producing rare-earth magnets of claim 1 , wherein a net belt of the net belt conveyor is covered with a pressing net belt and the sintered magnet bodies are conveyed while being held between these net belts.

6. The method for producing rare-earth magnets of claim 1 , wherein
the slurry is fed to a bottom of the coating tank so that i) the level of the slurry in the coating tank is held at the position higher than the upper surface of the sintered magnet bodies on the net belt conveyor to immerse the sintered magnet into the slurry, and ii) the slurry continuously overflows from the upper end portion of the coating tank including the net belt passage openings and the level of slurry is continuously maintained to be at the level above the lower part of the net belt passage openings.

7. The method for producing rare-earth magnets of claim 1 , wherein
the slurry, which is overflowed from the coating tank, is returned to the coating tank.

8. The method for producing rare-earth magnets of claim 1 , wherein
the slurry is overflowed from the coating tank to an outer tank, and
the slurry, which is overflowed from the coating tank, is returned from the outer tank to the coating tank.

9. The method for producing rare-earth magnets of claim 1 , wherein
the slurry, which is overflowed from the coating tank, is returned to the coating tank by a pump.

10. The method for producing rare-earth magnets of claim 1 , wherein
the slurry is overflowed from the coating tank to an outer tank, and
the slurry, which is overflowed from the coating tank, is returned from the outer tank to the coating tank by a pump.

Assignees

• Shinetsu Chemical Co

Inventors

• Kuribayashi Yukihiro
• Kamiya Shogo
• Maegawa Harukazu
• Tanaka Shintaro

Classifications

• B22F3/00

  Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor {; Presses and furnaces} · CPC title

• B05C3/04

  with special provision for agitating the work or the liquid or other fluent material · CPC title

• B05D3/042

  Directing or stopping the fluid to be coated with air · CPC title

• B05D2401/10

  Organic solvent (B05D2401/21 takes precedence) · CPC title

• B05D2401/32

  applied as powders · CPC title