Gas liquid separator and associated methods

Patent metadata

Field	Value
Publication number	US-10821379-B2
Application number	US-201715792418-A
Country	US
Kind code	B2
Filing date	Oct 24, 2017
Priority date	Oct 25, 2016
Publication date	Nov 3, 2020
Grant date	Nov 3, 2020

Abstract

Exemplary embodiments are directed to a gas liquid separator that includes a chamber for receiving a fluid mixture, a fluid mixture inlet, a solvent outlet, and a gas outlet. The gas liquid separator can include a sensor disposed around or within the chamber for sensing at least one of a solvent level or a gas level. The gas liquid separator can include a regulator connected to at least one of the solvent outlet or the gas outlet for regulating at least one of the solvent level or the gas level within the chamber. Exemplary methods of regulating at least one of the solvent level or the gas level within a gas liquid separator of a CO2-based chromatography flow system are also provided.

First claim

The invention claimed is:

1. A gas liquid separator, comprising:
a chamber for receiving a fluid mixture, the fluid mixture being introduced into the chamber for separation into a gas and a liquid solvent;
a fluid mixture inlet providing an inlet for the fluid mixture into the chamber;
a solvent outlet for discharging the liquid solvent from the chamber after separation of the liquid solvent from the gas;
a gas outlet for discharging the gas from the chamber after separation of the gas from the liquid solvent;
a gas level sensor for sensing a gas level in the chamber;
a pressure sensor located downstream of the gas outlet to detect a pressure within a piping for the gas outlet; and
a regulator located downstream of the pressure sensor and connected to the gas outlet for regulating the gas level within the chamber in response to signals received from the gas level sensor and the pressure sensor.

2. The gas liquid separator of claim 1 , wherein the fluid mixture comprises CO 2 and the liquid solvent.

3. The gas liquid separator of claim 1 , further comprising a liquid level sensor for sensing a solvent level within the chamber.

4. The gas liquid separator of claim 3 , wherein the liquid level sensor is at least one of an ultrasonic sensor or an optical sensor.

5. The gas liquid separator of claim 3 , wherein the liquid level sensor is disposed on a top surface of the chamber for sensing a depth of the chamber to a surface of the liquid solvent.

6. The gas liquid separator of claim 3 , wherein the liquid level sensor is disposed at or near the solvent outlet for sensing an amount of the liquid solvent and the gas received by the solvent outlet.

7. The gas liquid separator of claim 1 , wherein the regulator is at least one of a pressure regulator of an on/off valve.

8. The gas liquid separator of claim 7 , wherein at least one of the pressure regulator or the on/off valve is communicatively connected to the gas level sensor.

9. The gas liquid separator of claim 8 , wherein the pressure regulator automatically adjusts the pressure within the gas outlet based on a signal received from the gas level sensor to regulate the gas level within the chamber.

10. The gas liquid separator of claim 8 , wherein the on/off valve automatically adjusts within the gas outlet based on a signal received from the gas level sensor to regulate the gas level within the chamber.

11. The gas liquid separator of claim 7 , wherein the pressure regulator is a pressure control valve.

12. The gas liquid separator of claim 7 , wherein the pressure regulator is an on/off valve.

13. The gas liquid separator of claim 1 , wherein regulating the gas level within the chamber with the regulator maintains a separation and a balance of the liquid solvent and the gas within the chamber.

14. The gas liquid separator of claim 13 , wherein the separation and the balance of the liquid solvent and the gas within the chamber prevents the gas from being discharged from the solvent outlet and the liquid solvent from being discharged from the gas outlet.

15. The gas liquid separator of claim 1 , wherein the solvent outlet comprises a fixed restriction outlet and the regulator is connected to the gas outlet.

16. The gas liquid separator of claim 1 , comprising a capacitive gas chamber disposed along the gas outlet for introduction of gas into the gas outlet or removal of gas from the gas outlet to dampen a pressure response during regulation of at least one of the solvent level or the gas level within the chamber.

17. The gas liquid separator of claim 1 , comprising a pressure sensor connected to the gas outlet for sensing a pressure within the gas outlet.

18. The gas liquid separator of claim 1 , comprising a liquid level sensor connected to at least one of the gas outlet or the solvent outlet for sensing a flow within at least one of the gas outlet or the solvent outlet.

Assignees

• Waters Technologies Corp

Inventors

• Shreve Joshua A

Classifications

• G01N30/32 Primary

  of pressure or speed (G01N30/36 takes precedence) · CPC title

• B01D46/71

  with pressurised gas, e.g. pulsed air · CPC title

• F24F8/10

  by separation, e.g. by filtering · CPC title

• B01D15/40

  using supercritical fluid as mobile phase or eluent · CPC title

• G01N30/80

  Fraction collectors · CPC title