Dental resin composite material, method of producing dental resin composite material, and polyaryletherketone resin for producing dental resin composite material

Patent metadata

Field	Value
Publication number	US-10813850-B2
Application number	US-201716335069-A
Country	US
Kind code	B2
Filing date	Oct 12, 2017
Priority date	Oct 13, 2016
Publication date	Oct 27, 2020
Grant date	Oct 27, 2020

Abstract

A dental resin composite material is provided that is reduced in darkness of its color tone, and also reduced in burning and color unevenness. Specifically provided are a dental resin composite material including 100 parts by mass of a polyaryletherketone resin, 10 parts by mass to 300 parts by mass of inorganic particles, and 90 ppm or less of an impurity having an aromatic ring, a method of producing the dental resin composite material, and a polyaryletherketone resin for producing a dental resin composite material, to be used for producing the dental resin composite material.

First claim

The invention claimed is:

1. A method of producing a dental resin composite material, comprising:
a step of heating polyaryletherketone resin powder containing an impurity having an aromatic ring in a heat treatment apparatus to form a polyaryletherketone resin containing 150 ppm or less of the impurity having the aromatic ring, wherein a heating temperature is in a range of a glass transition temperature of the polyaryletherketone resin powder or more to less than a melting point of the polyaryletherketone resin powder, and an internal gas in the heat treatment apparatus is replaced with an external gas existing outside of the heat treatment apparatus while the heating is performed; and
a step of mixing 100 parts by mass of the polyaryletherketone resin containing 150 ppm or less of the impurity having the aromatic ring and 10 parts by mass to 300 parts by mass of inorganic particles in a molten state.

2. The method of producing the dental resin composite material according to claim 1 ,
wherein, when the heating is performed, a volatile component containing the impurity having the aromatic ring is generated from the heating of the polyaryletherketone resin powder in the heat treatment apparatus, and
when the heating is performed, the internal gas having the volatile component is replaced with the external gas so as to prevent the volatile component from adhering to the polyaryletherketone resin powder heated in the heat treatment apparatus.

3. The method of producing the dental resin composite material according to claim 1 ,
wherein an average particle diameter of the polyaryletherketone resin powder is in a range of 150 μm to 2,000 μm.

4. The method of producing the dental resin composite material according to claim 1 ,
wherein the internal gas contains an inert gas.

5. The method of producing the dental resin composite material according to claim 1 ,
wherein the heat treatment apparatus has an absorption filter through which the internal gas passes.

6. The method of producing the dental resin composite material according to claim 1 ,
wherein the internal gas is continuously or intermittently replaced with the external gas while the heating is performed.

Assignees

• Tokuyama Dental Corp

Inventors

• Yamagawa Junichiro
• Shimizu Tomonao
• Nagasawa Yuko
• Uehara Anna

Classifications

• A61K6/831 Primary

  comprising non-metallic elements or compounds thereof, e.g. carbon · CPC title

• A61K6/827

  Leucite · CPC title

• A61K6/84

  comprising metals or alloys · CPC title

• A61K6/891 Primary

  Compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds · CPC title