Method for detecting oil on tobacco products and packaging

Patent metadata

Field	Value
Publication number	US-10782279-B2
Application number	US-201514938561-A
Country	US
Kind code	B2
Filing date	Nov 11, 2015
Priority date	Nov 11, 2014
Publication date	Sep 22, 2020
Grant date	Sep 22, 2020

Abstract

A process for detecting oil or lubricant contamination in a manufactured product, the process comprising adding at least two fluorescent taggants to oils or lubricants contained in processing machinery for said product, irradiating said product, causing at least one of said taggants to fluoresce and detecting radiation emitted by said fluorescing taggant in an oil-contaminated product.

First claim

We claim:

1. A process for detecting lubricant contamination in a manufactured product, the process comprising:
adding a first fluorescent taggant and a second fluorescent taggant to a lubricant used in processing machinery for the product, the first fluorescent taggant being different than the second fluorescent taggant;
irradiating the product with a first radiation spectrum, wherein the irradiation causes the first fluorescent taggant to fluoresce;
visually detecting radiation emitted by the fluorescing first fluorescent taggant by an operator of the process;
irradiating the product with a second radiation spectrum, wherein the irradiation causes the second fluorescent taggant to fluoresce; and
electronically detecting radiation emitted by the fluorescing second fluorescent taggant by an electronic radiation detection device.

2. The process of claim 1 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant fluoresces upon irradiation with ultraviolet radiation.

3. The process of claim 2 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant emits radiation in the visible spectrum.

4. The process of claim 1 , wherein both of the first fluorescent taggant and the second fluorescent taggant fluoresce upon irradiation with ultraviolet radiation.

5. The process of claim 1 , wherein the first fluorescent taggant and the second fluorescent taggant are added to the lubricant at different concentration levels, with the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant being added at a sufficient concentration level for an emission to be visually detectable by the operator of the process.

6. The process of claim 1 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant is added to the lubricant at a concentration of about 50 ppb to about 100 ppm.

7. The process of claim 1 , further comprising:
conveying the product past an electronic radiation detection apparatus that detects radiation emitted by the fluorescing second fluorescent taggant.

8. The process of claim 1 , wherein the first fluorescent taggant and the second fluorescent taggant are Stokes-shifting taggants that absorb radiation at a first wavelength and fluoresce at a second wavelength, the second wavelength different from the first wavelength.

9. The process of claim 1 , wherein the product is a cigarette rod wrapped in paper.

10. The process of claim 1 , wherein the product is a food product.

11. The process of claim 1 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant are oil soluble.

12. The process of claim 1 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant are oil dispersible.

13. A process for detecting lubricant contamination in a tobacco product, the process comprising:
adding a first fluorescent taggant and a second fluorescent taggant to a lubricant used in processing machinery for the product, the first fluorescent taggant being different than the second fluorescent taggant;
irradiating the product with a first radiation spectrum, wherein the irradiation causes the first fluorescent taggant to fluoresce;
visually detecting radiation emitted by the fluorescing first fluorescent taggant by an operator of the process;
irradiating the product with a second radiation spectrum, wherein the irradiation causes the second fluorescent taggant to fluoresce; and
electronically detecting radiation emitted by the fluorescing second fluorescent taggant by an electronic radiation detection device.

14. The process of claim 13 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant fluoresce upon irradiation with ultraviolet radiation.

15. The process of claim 14 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant emit radiation in the visible spectrum.

16. The process of claim 13 , wherein both of the first fluorescent taggant and the second fluorescent taggant fluoresce upon irradiation with ultraviolet radiation.

17. The process of claim 13 , wherein the first fluorescent taggant and the second fluorescent taggant are added to the lubricant at different concentration levels, with the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant being added at a sufficient concentration level for its emission to be visually detectable by the operator of the process.

18. The process of claim 13 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant are added to the lubricant at a concentration of about 50 ppb to about 100 ppm.

19. The process of claim 13 , further comprising:
conveying the product past an electronic radiation detection apparatus that detects radiation emitted by the fluorescing second fluorescent taggant.

20. The process of claim 13 , wherein the first fluorescent taggant and the second fluorescent taggant are Stokes-shifting taggants that absorb radiation at a first wavelength and fluoresce at a second wavelength, the second wavelength different from the first wavelength.

21. The process of claim 13 , wherein the product is a cigarette rod wrapped in paper.

22. The process of claim 13 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant are oil soluble.

23. The process of claim 13 , wherein the first fluorescent taggant, the second fluorescent taggant, or both the first fluorescent taggant and the second fluorescent taggant are oil dispersible.

24. A process for identifying a source of oil contamination of a product produced in a manufacturing process having multiple machines in series, each of the multiple machines containing a lubricant, comprising:
adding a first fluorescent taggant to the lubricant of each machine in the series;
adding a second fluorescent taggant to the lubricant of each machine in the series, the second fluorescent taggant being different from the first fluorescent taggant, and the second fluorescent taggant of each machine in the series being different from the second fluorescent taggant in other machines in the series;
irradiating the product with a first radiation spectrum;
visually detecting radiation emitted by the first fluorescent taggant by an operator of the process;
removing the radiation emitting product from the process;
irradiating the radiation emitting product with a second radiation spectrum; and
electronically detecting radiation emitted by the second fluorescent taggant by an electronic radiation detection device.

25. The process of claim 24 , further comprising:
identifying the source of the lubricant contamination based on the detected radiation emitted by the second fluorescent taggant.

26. The process o

Assignees

• Altria Client Services Llc

Inventors

• Cadieux Jr Edmond J
• Wood Robert E

Classifications

• G01N21/6447

  by visual observation · CPC title

• G01N33/28 Primary

  Oils {, i.e. hydrocarbon liquids} (edible oils or edible fats G01N33/03) · CPC title

• G01N21/94

  Investigating contamination, e.g. dust (G01N21/85 takes precedence) · CPC title

• G01N21/643

  non-biological material · CPC title

• G01N2021/6441

  with two or more labels · CPC title