Continuous method for the precipitation of lignin from black liquor
US-2015345076-A1 · Dec 3, 2015 · US
US10774471B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10774471-B2 |
| Application number | US-201815902093-A |
| Country | US |
| Kind code | B2 |
| Filing date | Feb 22, 2018 |
| Priority date | Jan 31, 2018 |
| Publication date | Sep 15, 2020 |
| Grant date | Sep 15, 2020 |
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A method of recycling a by-product generated in a papermaking process including, pulverizing a by-product produced in a papermaking process to prepare a pulverized product, burning the pulverized product to prepare a burned product, hydrating the burned product to prepare a hydrate; and manufacturing paper from the hydrate and a paper slurry is provided, which allows reuse of by-products generated in conventional papermaking processes such as lime mud and lime kiln CaO, which is environmentally friendly as well as cost-effective, and also the level of whiteness of the by-products such as lime mud and lime kiln CaO generated in a papermaking process can be improved to that of a high-grade raw material, making it possible to also improve the whiteness of paper.
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What is claimed is: 1. A method of recycling a by-product generated in a papermaking process comprising: pulverizing a by-product produced in a papermaking process to prepare a pulverized product; burning the pulverized product to prepare a burned product; hydrating the burned product to prepare a hydrate; and manufacturing paper from the hydrate and a paper slurry; wherein the by-product generated in the papermaking process comprises at least one of lime mud, lime kiln CaO, and the by-product is obtained through an in-situ method for synthesizing precipitated calcium carbonate (PCC) filler in a pulp slurry. 2. The method of claim 1 , wherein, burning the pulverized product is performed at a temperature of 900 to 1,300° C. for 0.5 to 3 hours. 3. The method of claim 1 , wherein, hydrating the burned product is performed at a temperature of 20 to 90° C. for 3 to 12 hours after adding water. 4. The method of claim 1 , wherein the hydrate is Ca(OH) 2 . 5. The method of claim 1 , wherein manufacturing the paper comprises, adding the paper slurry into a reaction tank, adding the hydrate into the reaction tank and mixing to form a mixture, injecting CO 2 gas into the mixture, and adding the CO 2 gas-injected mixture to a sheet former for molding into paper. 6. The method of claim 5 , wherein the CO 2 gas is injected into the mixture at an injection rate of 50 cc/min. 7. The method of claim 5 , wherein the paper slurry is deinked pulp slurry.
Aspects concerning the production and the treatment of green and white liquors, e.g. causticizing green liquor · CPC title
Production or processing of lime, e.g. limestone regeneration of lime in pulp and sugar mills · CPC title
Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for (volatile compounds obtained by decomposition of spent liquors in order to regenerate them D21C11/125; compounds obtained by fractionating the liquors in order to regenerate them D21C11/0042) · CPC title
Inorganic compounds · CPC title
Secondary fibres (working-up waste paper D21C5/02) · CPC title
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