Whitened tobacco compostion

Patent metadata

Field	Value
Publication number	US-10772349-B2
Application number	US-201615230976-A
Country	US
Kind code	B2
Filing date	Aug 8, 2016
Priority date	Feb 13, 2012
Publication date	Sep 15, 2020
Grant date	Sep 15, 2020

Abstract

A method of preparing a whitened tobacco material is provided, the method including the steps of (i) extracting a tobacco material with an aqueous solution to give a tobacco pulp and a tobacco extract; (ii) treating the tobacco pulp with at least one of a caustic reagent and an oxidizing agent for a time and at a temperature sufficient to lighten the color of the tobacco pulp to give a whitened tobacco pulp; (iii) clarifying the tobacco extract to remove higher molecular weight components; and (iv) combining the whitened tobacco pulp with a clarified tobacco extract to form a whitened tobacco material. The whitened tobacco material can be isolated and incorporated into a smokeless tobacco product. The invention also provides a smokeless tobacco product incorporating a whitened tobacco material. The smokeless tobacco product may be a snus-type formulation contained within a sealed pouch.

First claim

What is claimed:

1. A tobacco product comprising a water-permeable pouch containing a whitened tobacco composition, the whitened tobacco composition comprising a translucent tobacco extract carried by a whitened tobacco pulp, wherein the whitened tobacco composition is in a ground, granulated, fine particulate, or powdered form.

2. The tobacco product of claim 1 , wherein the translucent tobacco extract is in the form of a distillate or a filtered tobacco extract.

3. The tobacco product of claim 1 , wherein the translucent tobacco extract is characterized by a low tobacco-specific nitrosamine content of about 150 ng/g or less.

4. The tobacco product of claim 1 , wherein the translucent tobacco extract is characterized by a low benzo[a]pyrene content of about 1 ng/g tobacco extract or less.

5. The tobacco product of claim 1 , wherein the translucent tobacco extract does not comprise any components having a molecular weight greater than about 1000 Da.

6. The tobacco product of claim 1 , further comprising one or more additional components selected from the group consisting of flavorants, fillers, binders, pH adjusters, buffering agents, colorants, disintegration aids, antioxidants, humectants, and preservatives.

7. The tobacco product of claim 1 , comprising about 80% to about 95% whitened tobacco composition; about 0.1% to about 5% artificial sweetener; about 0.5% to about 2% salt; about 1% to about 5% flavoring; and about 1% to about 5% humectant.

8. The tobacco product of claim 7 , wherein the humectant comprises propylene glycol.

9. The tobacco product of claim 1 , wherein the whitened tobacco pulp and the translucent tobacco extract are present in a weight ratio of about 1:1 to about 10:1.

10. The tobacco product of claim 1 , wherein the whitened tobacco pulp and the translucent tobacco extract are present in a weight ratio of about 1.5:1 to about 3:1.

11. The tobacco product of claim 1 , wherein the whitened tobacco pulp comprises a pulp of tobacco lamina, or a tobacco lamina and stem mixture.

12. A method of preparing the tobacco product of claim 1 , comprising: (i) extracting a tobacco material with an aqueous solution to give a tobacco pulp and a tobacco extract; (ii) treating the tobacco pulp with at least one of a caustic reagent and an oxidizing agent for a time and at a temperature sufficient to lighten the color of the tobacco pulp to give a whitened tobacco pulp; (iii) clarifying the tobacco extract to give a translucent tobacco extract; (iv) combining the whitened tobacco pulp with the translucent tobacco extract to form a whitened tobacco material in ground, granulated, fine particulate, or powdered form; and (v) incorporating a whitened tobacco composition comprising the whitened tobacco material within the water-permeable pouch.

13. The method of claim 12 , wherein the whitened tobacco pulp and clarified tobacco extract combined in step (iv) are derived from the same tobacco material.

14. The method of claim 12 , wherein the whitened tobacco pulp and clarified tobacco extract combined in step (iv) are derived from different tobacco materials.

15. The method of claim 12 , wherein the caustic reagent is sodium hydroxide.

16. The method of claim 12 , wherein the oxidizing agent is hydrogen peroxide.

17. The method of claim 12 , wherein the molar ratio of the amount of caustic reagent to oxidizing agent is from about 1:1 to about 1:100.

18. The method of claim 12 , further comprising selecting the tobacco material to be extracted in step (i) by visually inspecting a group of tobacco materials and selecting the tobacco material that is relatively light in color as compared with the remainder of the tobacco materials in the group.

19. The method of claim 12 , wherein the treating step further comprises heating the mixture of tobacco pulp, caustic reagent, and oxidizing agent at a temperature sufficient to increase the rate of whitening.

20. The method of claim 12 , wherein the clarifying step comprises distilling or filtering the tobacco extract.

21. The method of claim 20 , wherein said filtering comprises passing the tobacco extract through a membrane filter having a cutoff molecular weight of 1000 Da.

Assignees

• Reynolds Tobacco Co R

Inventors

• Beeson Dwayne William
• Flinchum Jr Jack Gray
• Gan Huamin

Classifications

• A24B15/24 Primary

  by extraction; Tobacco extracts · CPC title

• A24B15/241

  Extraction of specific substances · CPC title

• A24B15/245 Primary

  Nitrosamines · CPC title

• A24B15/26

  Use of organic solvents for extraction · CPC title

• A24B13/00

  Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff (reconstituted tobacco products A24B3/14) · CPC title