Vacuum distillation and desalination
US-2018345167-A1 · Dec 6, 2018 · US
US10760032B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10760032-B2 |
| Application number | US-201916281856-A |
| Country | US |
| Kind code | B2 |
| Filing date | Feb 21, 2019 |
| Priority date | Feb 21, 2018 |
| Publication date | Sep 1, 2020 |
| Grant date | Sep 1, 2020 |
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A method for removing oil from seed flakes, including introducing seed flakes into an extractor, thereby producing an extracted seed flake stream and a miscella stream, introducing the extracted seed flake stream into a DTDC column, thereby producing a first solvent recycle stream and a seed meal stream, and introducing the miscella stream into a distillation system, thereby producing a second solvent recycle stream and a seed oil stream.
Opening claim text (preview).
What is claimed is: 1. A method for removing oil from seed flakes, comprising: a. Introducing seed flakes into an extractor, thereby producing an extracted seed flake stream and a miscella stream, b. Introducing the extracted seed flake stream into a DTDC column, thereby producing a first solvent recycle stream and a seed meal stream, and c. Introducing the miscella stream into a distillation system, thereby producing a second solvent recycle stream and a seed oil stream, wherein the first solvent recycle stream, the second solvent recycle stream, or both pass through a heater before being recycled to the extractor. 2. The method of claim 1 , wherein the extractor further comprises drive sockets, and one or more cells that are attached to one or more conveyer chains, wherein the one or more conveyer chains are driven by the drive sockets at both ends of the extractor. 3. The method of claim 1 , wherein the extractor further comprises one or more top rails, one or more cells comprising wheels that are configured to ride along the one or more top rails. 4. The method of claim 1 , wherein the extractor further comprises one or more hoppers configured to receive the miscella stream, wherein the one or more hoppers have sides with angles of more than 25 degrees from the vertical. 5. The method of claim 1 , wherein the extractor comprises a final hopper at one end of the extractor, and wherein the final hopper has sides with angles of more than 50 degrees from the vertical. 6. The method of claim 1 , wherein the DTDC column comprises a top, and a shaft configured to support one or more trays, and wherein the shaft is supported at the top. 7. The method of claim 1 , wherein the DTDC column comprises at least one dryer section and at least one cooler section, and wherein the at least one dryer section and/or the at least one cooler section comprises at least one air transfer duct comprising sloping walls and having no low point or flat spots where seed fines may accumulate. 8. The method of claim 1 , wherein the DTDC column comprises one or more decks each of which comprises one or more trays upon which the seed flakes are dispersed, wherein each of the one or more decks comprises at least one electronic level indicator, and a valve between each of the one or more decks, wherein the level of the seed flakes on the one or more decks are controlled by opening or closing the respective valve until the at least one electronic level indicator senses a predetermined level. 9. The method of claim 1 , wherein the DTDC column further comprises a separate pre-desolventizer located upstream of the DTDC. 10. The method of claim 1 , wherein the DTDC column comprises one or more decks each of which comprises one or more trays upon which the seed flakes are dispersed, wherein each deck has a dedicated blower. 11. The method of claim 1 , wherein the miscella stream is treated in a three-stage fines removal system after removal from the extractor, wherein the first-stage comprises one or more cyclonic separators, the second-stage comprises one or more filters, and the third stage comprises a settling tank. 12. The method of claim 9 , wherein the second-stage filters are automatic metal edge filters. 13. The method of claim 1 , wherein prior to entering the distillation system, the miscella is introduced into a phase separator. 14. The method of claim 1 , wherein an air-lock is provided between the extractor and the DTDC, thus allowing the extractor to operate without requiring that the DTDC be pressurized.
in combination with at least one evaporator · CPC title
by extracting · CPC title
with steam · CPC title
Condensation of solvent vapours (condensation in general B01D5/00) · CPC title
Condensation of vapours; Recovering volatile solvents by condensation (B01D8/00 takes precedence; condensers F28B) · CPC title
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