Manufacturing method for ethanol aqueous solution

Patent metadata

Field	Value
Publication number	US-10745657-B2
Application number	US-201515514546-A
Country	US
Kind code	B2
Filing date	Sep 29, 2015
Priority date	Sep 30, 2014
Publication date	Aug 18, 2020
Grant date	Aug 18, 2020

Abstract

The purpose of the present invention is to provide a simple method in which, when distilling a mixture of ethanol, water, and biological raw materials, more aromatic components can be obtained and undesirable odors can be prevented from transferring to the distillate. To achieve this, ethanol and water are added during distillation.

First claim

The invention claimed is:

1. A method for producing an ethanol aqueous solution having an aroma of a plant raw material using distillation, comprising the steps of:
a first step comprising distilling a mixture of an amount of plant raw material, a first amount of ethanol and a first amount of water, and
a second step of adding
(a) a composition consisting of a second amount of ethanol and a second amount of water to the mixture during a remainder of the distillation, or
(b) separately adding only a second amount of ethanol and a second amount of water, to the mixture during a remainder of the distillation,
to form a liquid distillate,

wherein after the second step, an ethanol concentration of the liquid distillate at the time of the liquid distillate's production is from 10 to 50%.

2. The method according to claim 1 , wherein the addition of the second amount of ethanol and the second amount of water is initiated after the ethanol concentration of the liquid distillate has dropped to the range from 10 to 50%.

3. The method according to claim 1 , wherein the addition of the second amount of ethanol and the second amount of water is initiated after the liquid distillate is produced in a volume from 0.10 to 035 times the total volume of the first amount of ethanol and the first amount of water.

4. The method according to claim 1 , wherein the second amount of ethanol and the second amount of water are added at a volume ratio of from 5:95 to 50:50.

5. The method according to claim 1 , wherein the total volume of the second amount of ethanol and the second amount of water is from 0.01 to 3 times the total volume of the first amount of ethanol and the first amount of water.

6. The method according to claim 1 , wherein the distillation pressure is atmospheric pressure.

7. The method according to claim 1 , wherein the plant raw material is selected from a group consisting of: fruits, fruit peels, herbs, and a combination thereof.

8. The method according to claim 1 , wherein the plant raw material is selected from a group consisting of citrus fruits, peels of citruses, and a combination thereof.

9. The method according to claim 1 , wherein the second step consists of adding the composition consisting of the second amount of ethanol and the second amount of water to the mixture during the remainder of the distillation.

Assignees

• Suntory Holdings Ltd

Inventors

• Nakajima Mihoko
• Torii Kazuyuki

Classifications

• C12H6/02

  by distillation · CPC title

• A23L2/06

  from citrus fruits · CPC title

• A23G9/32

  characterised by the composition {containing organic or inorganic compounds} · CPC title

• A23G4/06

  characterised by the composition {containing organic or inorganic compounds} · CPC title

• A23G3/36

  characterised by the composition {containing organic or inorganic compounds} · CPC title