Method for purification of animal or vegetable fats

Patent metadata

Field	Value
Publication number	US-10738264-B2
Application number	US-201716337744-A
Country	US
Kind code	B2
Filing date	Sep 28, 2017
Priority date	Sep 30, 2016
Publication date	Aug 11, 2020
Grant date	Aug 11, 2020

Abstract

Present invention relates to a novel process for purification of lipid material for further use as such as e.g. a source of fuel or chemicals.

First claim

The invention claimed is:

1. A method for purifying lipid material, wherein the method comprises:
a) storing the lipid material in a settling tank at elevated temperature;
b) allowing impurities to settle to a bottom of the settling tank to thereby form an oily sludge phase;
c) separating the formed oily sludge phase from a remainder of the lipid material,
d) further processing the lipid material;
e) purifying said separated oily sludge phase from impurities; and optionally
f) returning purified oil from the purifying step e) to said settling tank,
wherein the method in step e) includes a heat treatment step which includes:
i. heating said oily sludge phase to a temperature of from about 150° C. to about 300° C.;
ii. adding polar solvent to said oily sludge phase for removal of impurities from oil phase; and
iii. separating and recovering purified oil;
wherein said elevated temperature in step a) is from about 40° C. to about 120° C., and wherein settling in the settling tank takes place without any form of stirring.

2. The method according to claim 1 , wherein a time during which the impurities in the lipid material is allowed to settle to the bottom of the settling tank is selected to be from about 5 hours, about 10 hours, about 15 hours, about 1 day, about 2 days, about 3 days, about 4 days, or about 5 days.

3. The method according to claim 1 , wherein the lipid material is originated from biological material.

4. The method according to claim 1 , wherein the lipid material is selected from used cooking oil, vegetable oils or any kind or animal fats of any kind or mixtures thereof.

5. The method according to claim 1 , wherein the lipid material is selected from any fossil based oil or product, industrial oils used, fuel oils and gasoline (petrol), including all used products in either a refining process, or used lubrication oils, or waste plastic pyrolysis oils.

6. The method according to claim 1 , wherein separating in step c) comprises:
phase separation by decantation, whereby the lipid material is separated from the oily sludge.

7. The method according to claim 1 , wherein the heating in step i) is performed during a period of time which is selected to be about 5 to about 60 minutes, about 10 minutes to about 50 minutes, about 15 minutes to about 40 minutes, or about 20 minutes to about 30 minutes.

8. The method according to claim 1 , wherein the heating in step i) is about 170° C. to about 240° C.

9. The method according to claim 1 , wherein the polar solvent is water, methanol or ethanol or any combination thereof.

10. The method according to claim 1 , wherein the recovered purified oil in step iii) is subjected to a filtration and/or centrifugation and/or mechanical removal to remove impurities present in the sludge.

11. The method according to claim 1 , comprising:
bleaching the separated and recovered purified oil.

12. The method according to claim 1 , wherein impurities are one or more of polyethylene, calcium salts, sodium salts or phosphorous salts.

13. The method according to claim 1 , comprising:
removing at least about 90% of the original content of polyethylene in the lipid material.

14. The method according to claim 1 , wherein the heating in step i) is to a temperature of about 180° C. to about 200° C.

15. The method according to claim 1 , comprising:
removing at least about 95% of the original content of polyethylene in the lipid material.

16. The method according to claim 1 , comprising:
removing at least about 97% of the original content of polyethylene in the lipid material.

17. The method according to claim 1 , comprising:
removing at least about 98% of the original content of polyethylene in the lipid material.

18. The method according to claim 1 , comprising:
removing at least about 99% of the original content of polyethylene in the lipid material.

Assignees

• Neste Oyj

Inventors

• Bergström Pia
• Toukoniitty Blanka
• Malm Annika
• Waddilove Mervi

Classifications

• C11B3/16 Primary

  by mechanical means · CPC title

• C11B3/006

  by extraction · CPC title

• C11B3/00 Primary

  Refining fats or fatty oils · CPC title

• C11B3/08

  with oxidising agents · CPC title

• C11C1/10

  by distillation · CPC title