Method for making ceramic matrix composite articles with progressive melt infiltration
US-2016175960-A1 · Jun 23, 2016 · US
US10723659B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10723659-B2 |
| Application number | US-201816017457-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 25, 2018 |
| Priority date | Jun 25, 2018 |
| Publication date | Jul 28, 2020 |
| Grant date | Jul 28, 2020 |
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A blade for a gas turbine engine, and methods of manufacture of such a blade having a continuous density gradient so that the portion of the blade nearest the rotator shaft is of a higher density than the portion of the blade furthest from the rotator shaft.
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What is claimed is: 1. A method comprising: reducing potential stress of a centrifugal load on a blade for a gas turbine engine by manufacturing a density gradient in a ceramic matrix composite of the blade by infiltrating a porous fiber preform, wherein the density gradient includes a change in density between a blade root-end of the blade and a blade tip-end of the blade. 2. The method of claim 1 , wherein manufacturing the density gradient comprises varying a percentage of silicon carbide in the blade along a radial direction, wherein the radial direction is in a direction away from a point around which the blade is configured to rotate. 3. The method of claim 1 wherein manufacturing the density gradient comprises: providing the porous fiber preform, the porous fiber preform comprising a preform root-end and a preform tip-end; infiltrating the porous fiber preform with a chemical vapor matrix material; infiltrating the porous fiber preform with a ceramic-containing slurry; and infiltrating the porous fiber preform with a ceramic-containing melt material. 4. The method of claim 3 wherein infiltrating with the chemical vapor matrix material comprises exposing the chemical vapor matrix material to the preform root-end at a first partial pressure that is greater than a second partial pressure of the chemical vapor matrix material applied to the preform tip-end. 5. The method of claim 4 further comprising arranging the porous fiber preform within a chemical vapor infiltration mask having a plurality of chemical vapor inlets including a first inlet and a second inlet, wherein the first inlet is larger than the second inlet, wherein the first inlet is located closer to the preform root-end of the porous fiber preform than to the tip-end, wherein the second inlet is located closer to the preform tip-end than to the preform root-end. 6. The method of claim 4 wherein infiltrating with the chemical vapor matrix material comprises heating the preform root-end to create a temperature differential between the preform root-end and the preform tip-end. 7. The method of claim 5 wherein infiltrating the porous fiber preform with a ceramic-containing slurry material comprises exposing the preform root-end in a first amount of ceramic-containing slurry that is greater than a second amount of ceramic-containing slurry applied to the preform tip-end. 8. The method of claim 7 further comprising applying a slurry infiltration mask to a portion of the tip-end of the porous fiber preform before infiltrating the porous fiber preform with the ceramic-containing slurry, and removing the slurry infiltration mask from the porous fiber preform. 9. The method of claim 8 wherein the slurry infiltration mask comprises a plurality of slurry inlets. 10. The method of claim 2 wherein manufacturing the density gradient comprises: providing the porous fiber preform, the porous fiber preform comprising a preform root-end and a preform tip-end; infiltrating the porous fiber preform with a chemical vapor matrix material; infiltrating the porous fiber preform with a ceramic-containing slurry material; applying a high-char yielding resin to the tip-end of the porous fiber preform in a first amount that is greater than a second amount of the high-char yielding resin applied to the preform root-end of the porous fiber preform; pyrolyzing the high-char yielding resin by which a silicon carbon gradient is formed; and forming the density gradient in the ceramic matric composite by infiltrating the porous fiber preform with a ceramic-containing melt material, which forms a silicon carbide gradient. 11. The method of claim 10 further comprising infiltrating the porous fiber preform with a ceramic-containing melt material. 12. The method of claim 1 wherein manufacturing the density gradient comprises: providing the porous fiber preform, the porous fiber preform comprising a preform root-end and a preform tip-end; infiltrating the porous fiber preform with a chemical vapor matrix material comprising at least one metal; infiltrating the porous fiber preform with a metal-containing slurry; and infiltrating the porous fiber preform with a metal-containing melt material. 13. The method of claim 1 wherein manufacturing the density gradient comprises: providing the porous fiber preform, the porous fiber preform comprising a preform root-end and a preform tip-end; infiltrating the porous fiber preform with a chemical vapor matrix material; and infiltrating the porous fiber preform with a ceramic-oxide containing slurry. 14. A method of manufacturing a blade for a gas turbine engine with a density gradient between a blade root-end of the blade and a blade tip-end of the blade, the method comprising: providing a porous preform comprising a preform root-end and a preform tip-end; infiltrating the porous preform with a chemical vapor matrix material; applying a slurry infiltration mask to a portion of the tip-end of the porous preform infiltrating the porous preform with a ceramic-containing slurry; and removing the slurry infiltration mask from the porous preform. 15. The method of claim 14 wherein the slurry infiltration mask comprises a plurality of slurry inlets. 16. An apparatus comprising: a blade for a gas turbine engine comprising a blade root-end and a blade tip-end, wherein a ceramic matrix composite of the blade has a density gradient, wherein the density gradient includes a change in density between a blade root-end of the blade and a tip-end of the blade, wherein a rate of change in density is constant along the density gradient. 17. The apparatus of claim 16 wherein the blade is a compressor blade. 18. The apparatus of claim 16 wherein the blade is a turbine blade. 19. The apparatus of claim 16 wherein the blade is contiguous along a longitudinal axis of the blade and further comprises a blade root-end chemical composition and a blade tip-end chemical composition wherein the blade root-end composition transitions into the blade tip-end composition.
Products showing a density-gradient · CPC title
having a specific pre-form · CPC title
Coating cavities or hollow spaces, e.g. interior of tubes; Infiltration of porous substrates · CPC title
Silicon · CPC title
Zirconia · CPC title
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