Tool for differential compression of a powder material, including a deformable membrane

Patent metadata

Field	Value
Publication number	US-10703012-B2
Application number	US-201615371855-A
Country	US
Kind code	B2
Filing date	Dec 7, 2016
Priority date	Dec 8, 2015
Publication date	Jul 7, 2020
Grant date	Jul 7, 2020

Abstract

A tool to differentially compress a powder material comprises a differential compression piston and a support. The piston comprises a first part configured to apply a pressure on a first region of an external surface of the powder material. The piston comprises a second part with a recess which is located at a lateral distance from the first part and which is configured to face a second region of the external surface of the powder material. The tool further comprises a membrane that can be deformed by the piston. The deformable membrane is configured to at least partially retain the powder material in the tool.

First claim

The invention claimed is:

1. A method for manufacturing an element by sintering and by differential compression of a powder material by means of a tool to differentially compress a powder material, wherein the tool comprises:
a differential compression piston comprising a first part and a second part, and
a support for the powder material, that is configured to be on a side opposite to the differential compression piston with respect to the powder material,
wherein the differential compression piston and the support are configured so that the first part applies a first pressure on a first region of an external surface that delimits the powder material,
wherein the second part comprises a recess which is at a lateral distance from the first part and wherein the recess is configured to face a second region of the external surface of the powder material,
wherein the tool further comprises a membrane that is deformable by the action of the differential compression piston,
wherein the deformable membrane is configured to at least partially retain the powder material in the tool relative to the second part, when the deformable membrane is located between the powder material and the differential compression piston and when the deformable membrane is deformed during the compression applied by the first part and by reaction of the powder material on the membrane facing the recess,
wherein the second part is motionless relative to the first part, so as to make an element with an external surface comprising a first region with a higher density than a second region of the external surface of the element,
wherein the method comprises:
sintering and compressing, with the tool, the first region of the external surface of the powder material and the second region of the external surface of the powder material facing the second part of the tool, so as to make an element with an external surface comprising a first region with a higher density than a second region of the external surface of the element,
wherein the powder material is located between the support and the membrane, the membrane being mechanically deformed during the compression applied by the first part and by reaction of the powder material on the membrane facing the recess.

2. The method according to claim 1 , in which the powder material comprises manganese or tin suicide.

3. The method according to claim 2 , in which the powder material comprises electrically doped manganese or electrically doped tin silicide.

4. The method according to claim 2 , in which the powder material comprises a silicide with formula MnSi 1.77 and/or Mg 2 Si x Sn 1-x where x is between 0.2 and 0.8.

5. The method according to claim 1 for manufacturing a washer, including a machining step of the second region.

6. The method according to claim 1 , in which the second part includes a setback portion forming a second stage of the piston, wherein the setback portion is offset from the recess relative to the first part forming a first stage of the piston.

7. The method according to claim 1 , in which the second part comprises a through hole.

8. The method according to claim 1 , in which the support comprises a piston configured to apply a uniform pressure on the external surface of the powder material.

9. The method according to claim 1 , in which the support comprises a differential compression piston configured to apply a pressure on the first region different from the pressure on the second region.

10. The method according to claim 1 , in which the differential compression piston is rotationally symmetrical about a longitudinal axis of the tool.

11. The method according to claim 1 , in which the deformable membrane comprises a flexible sheet.

12. The method according to claim 1 , in which the flexible sheet includes a metallic material and/or graphite.

Assignees

• Commissariat Energie Atomique

Inventors

• Boidot Mathieu

Classifications

• B30B15/064 Primary

  with heating or cooling means · CPC title

• B30B11/02

  using a ram exerting pressure on the material in a moulding space · CPC title

• C04B2235/66

  Specific sintering techniques, e.g. centrifugal sintering · CPC title

• C04B35/58085

  based on silicides · CPC title

• B28B3/003 Primary

  Pressing by means acting upon the material via flexible mould wall parts, e.g. by means of inflatable cores, isostatic presses (isostatic presses in general B30B5/02) · CPC title