Continuous annealing method for low coercive force cold-rolled electromagnetic pure iron plate and strip

Patent metadata

Field	Value
Publication number	US-10697040-B2
Application number	US-201615762623-A
Country	US
Kind code	B2
Filing date	Sep 1, 2016
Priority date	Sep 28, 2015
Publication date	Jun 30, 2020
Grant date	Jun 30, 2020

Abstract

A continuous annealing method for low coercive force cold-rolled electromagnetic pure iron plate and strip. Control parameters of each stages in a continuous annealing process are as follows: 750-850° C. at a heating stage; 750-850° C. at a soaking stage, the soaking time is 100-150 s; an outlet temperature of 575-675° C. at a slow-cooling stage, the cooling speed in slow-cooling stage is 2.5-10° C./s; an outlet temperature of 380-420° C. at a fast-cooling stage, the cooling speed of the fast-cooling stage is 15-25° C./s; and 270-310° C. at an overaging stage. The annealing medium is a non-oxidizing atmosphere composed of H2 and N2. After annealing, the cold-rolled electromagnetic pure iron plate and strip is leveled and pressed such that the leveling elongation rate of the plate and strip is controlled within the range of 0.2±0.1%. The process of the continuous annealing method is simple, and the produced cold-rolled electromagnetic pure iron plate and strip can achieve an overall performance of low coercive force and good formability without further magnetic annealing.

First claim

The invention claimed is:

1. A continuous annealing method for low coercive force cold-rolled electromagnetic pure iron sheet, wherein control parameters of each stage in a continuous annealing process are as follows: 750-850° C. at a heating stage; 750-850° C. at a soaking stage, with a soaking time being 100-150 s; an outlet temperature of 575-675° C. at a slow-cooling stage, with a cooling speed in the slow-cooling stage being 2.5-10° C./s; an outlet temperature of 380-420° C. at a fast-cooling stage, with a cooling speed of the fast-cooling stage being 15-25° C./s; and 270-310° C. at an overaging stage; an annealing medium is a non-oxidizing atmosphere composed of H 2 and N 2 ; after annealing, the cold-rolled electromagnetic pure iron sheet strip is leveled and pressed such that a leveling elongation rate of the sheet strip is controlled within a range of 0.2±0.1%.

2. The continuous annealing method for low coercive force cold-rolled electromagnetic pure iron sheet strip according to claim 1 , wherein a thickness of the said cold-rolled electromagnetic pure iron sheet strip is 0.5-3.0 mm.

3. The continuous annealing method for low coercive force cold-rolled electromagnetic pure iron sheet strip according to claim 1 , wherein a percent composition by mass of the elements of the said cold-rolled electromagnetic pure iron sheet strip is: C≤0.005%, Si≤0.1%, Mn=0.1-0.5%, P≤0.02%, S≤0.003%, Al≤0.005% or Al=0.1-1.5%, B≤0.007%, [N]≤0.005%, [O]≤0.02%, and the rest is Fe and unavoidable impurities.

4. The continuous annealing method for low coercive force cold-rolled electromagnetic pure iron sheet strip according to claim 3 , wherein the said cold-rolled electromagnetic pure iron sheet strip after annealing has a coercive force of 60-100 A/m, a yield strength of not less than 120 MPa, a elongation of not less than 35%.

5. The continuous annealing method for low coercive force cold-rolled electromagnetic pure iron sheet strip according to claim 3 , wherein hot-rolled processing parameters of the said cold-rolled electromagnetic pure iron sheet strip are: heating temperature of 1000-1200° C.; final rolling temperature of 750-900° C.; reeling temperature of 550-720° C.; cold-rolled reduction rate of within 30-55%.

Assignees

• Baoshan Iron & Steel

Inventors

• Yan Yuanyuan
• Liang Gaofei
• Cheng Guoping
• Lin Changqing

Classifications

• C21D9/561

  with a controlled atmosphere or vacuum · CPC title

• C21D8/1272

  Final recrystallisation annealing · CPC title

• C21D8/1244

  characterised by the heat treatment · CPC title

• C21D8/12

  during manufacturing of articles with special electromagnetic properties · CPC title

• C21D1/74

  Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material · CPC title