Late stage addition of rheology modifier

Patent metadata

Field	Value
Publication number	US-10695281-B2
Application number	US-201816204725-A
Country	US
Kind code	B2
Filing date	Nov 29, 2018
Priority date	Oct 28, 2013
Publication date	Jun 30, 2020
Grant date	Jun 30, 2020

Abstract

Methods of making personal care compositions, such as dentifrices, involving the addition of rheology modifiers at a later stage in the personal care composition formation process.

First claim

The invention claimed is:

1. A method of producing a personal care composition comprising:
a) forming in a mix tank, an aqueous premix containing at least 10% water and having a lower viscosity than a packaged personal care composition;
b) transferring the aqueous premix from the mix tank to a high energy dispersion device;
c) adding rheology modifier in line to the aqueous premix as the aqueous premix is transferred through the high energy dispersion device;
d) deaerating the aqueous premix; and
e) packaging the aqueous premix to produce the packaged personal care composition.

2. The method of claim 1 , wherein the transferring through the high energy dispersion device is at a flow rate of from about 10 Kg/min to about 1000Kg/min.

3. The method of claim 2 , wherein deaerating is done through an inline deaeration device.

4. The method of claim 3 , wherein, following addition of the rheology modifier to the aqueous premix, viscosity of the aqueous premix between the high energy dispersion device and inline deaeration device is between about 0.01 Pa·s and about 1,000 Pa·s measured at 10 sec−1.

5. The method of claim 3 , wherein the inline deaeration device reduces the air level of the aqueous premix to about 0.01% or less, by volume of the aqueous premix.

6. The method of claim 1 , wherein the rheology modifier is added in an amount from about 0.1% to about 10% by weight of the personal care composition.

7. The method of claim 1 , wherein the rheology modifier is at least one of xanthan gum, carboxymethyl cellulose, carrageenan, carbomer, hydroxyethyl cellulose, guar gum, or thickening silica.

8. The method of claim 1 , wherein the viscosity of the aqueous premix as it is transferred out of the mix tank is below about 150 Pa·s.

9. The method of claim 1 wherein, following addition of the rheology modifier to the aqueous premix, a surfactant is added to the aqueous premix following deaeration.

10. A method of producing a personal care composition comprising:
a) forming in a mix tank, an aqueous premix containing at least 10% water and having a lower viscosity than a packaged personal care composition;
b) transferring the aqueous premix from the mix tank to a high energy dispersion device;
c) adding rheology modifier in line to the aqueous premix as the aqueous premix is transferred through the high energy dispersion device;
d) deaerating the aqueous premix using an inline deaeration device; and
e) packaging the aqueous premix to produce the packaged personal care composition; wherein the inline deaeration device is positioned such that pressure drop between the high energy dispersion device and inline deaeration device is less than pumping pressure head of the high energy dispersion device.

11. The method of claim 10 , wherein, following addition of the rheology modifier to the aqueous premix, the viscosity of the aqueous premix between the high energy dispersion device and inline deaeration device is between about 0.01 Pa·s and about 1,000 Pa·s measured at 10 sec−1.

12. The method of claim 10 , wherein the inline deaeration device reduces the air content of the aqueous premix to about 0.01% or less, by volume of the aqueous premix.

13. The method of claim 10 , wherein the transferring through the high energy dispersion device is at a flow rate of from about 10Kg/min to about 1000Kg/min.

14. The method of claim 10 , wherein the rheology modifier is added in an amount from about 0.1% to about 5% by weight of the personal care composition.

15. The method of claim 10 , wherein the rheology modifier is at least one of xanthan gum, carboxymethyl cellulose, carrageenan, carbomer, hydroxyethyl cellulose, guar gum, or thickening silica.

16. The method of claim 10 , wherein the viscosity of the aqueous premix as it is transferred out of the mix tank is below about 150 Pa·s.

17. The method of claim 10 wherein, following addition of the rheology modifier to the aqueous premix, a surfactant is added to the aqueous premix following deaeration.

18. The method of claim 17 , wherein surfactant levels are from about 0.1% to about 15%, by weight of the personal care composition.

19. The method of claim 17 , wherein the surfactant is at least one of anionic, amphoteric, non-ionic, zwitterionic or cationic surfactants.

Assignees

• Procter & Gamble

Inventors

• Agerton Mark Lewis
• Alexander Steven Robert
• Berta James Albert
• Blum Gina Lynn
• Caggioni Marco
• Dawes Susan Marie
• Farren David Michael
• Hedin Justin Thomas Lydon
• Miller Charles Phillip
• Novicki Christa Marie
• Payne Melissa Cherie
• Schottelkotte Molly Rose
• Wesner John Christopher
• Wood Randall Lee

Classifications

• A61K8/042 Primary

  Gels · CPC title

• B01J13/00

  Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons · CPC title

• A61K8/04

  Dispersions; Emulsions · CPC title

• A61Q11/00

  Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses · CPC title

• A61K8/73

  Polysaccharides · CPC title