Manufacture of intermediate strength proppant or lost circulation material from drill cuttings
US-9714377-B2 · Jul 25, 2017 · US
US10689952B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10689952-B2 |
| Application number | US-201514956873-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 2, 2015 |
| Priority date | Dec 4, 2014 |
| Publication date | Jun 23, 2020 |
| Grant date | Jun 23, 2020 |
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Embodiments disclosed herein relate to a method including passing liquid carbon dioxide over drill cuttings carrying contaminants to form a mixture comprising liquid carbon dioxide and a portion of the contaminants; measuring a property of the mixture; and terminating the passing liquid carbon dioxide over drill cuttings based on the measured property.
Opening claim text (preview).
What is claimed is: 1. A method comprising: passing liquid carbon dioxide over drill cuttings carrying contaminants in an extraction tank to form a mixture comprising liquid carbon dioxide and a portion of the contaminants; transferring the mixture through a transfer line; measuring a property of the mixture as the mixture is being transferred, via the transfer line, through at least one measurement device, wherein the measured property of the mixture is a viscosity of the mixture, the measured property of the mixture is indicative of an extent to which the contaminants have been removed from the drill cuttings, and the at least one measurement device consists of at least one viscometer; terminating the passing liquid carbon dioxide over drill cuttings based on the measured property; and utilizing the liquid carbon dioxide as a transport medium to effectuate transfer of the drill cuttings from the extraction tank to a cleaned cuttings holding vessel based on the measured property. 2. The method of claim 1 , wherein the passing liquid carbon dioxide comprises contacting the drill cuttings with liquid carbon dioxide at a temperature in a range from about 10° C. to about 30° C. and a pressure in a range from about 50 bar to about 70 bar. 3. The method of claim 1 , wherein the measured property of the mixture is indicative of a contaminant content. 4. The method of claim 1 , further comprising separating the mixture by adjusting a solvating power of the liquid carbon dioxide. 5. The method of claim 4 , wherein the adjusting the solvating power comprises expanding the mixture to vaporize at least a portion of the liquid carbon dioxide. 6. The method of claim 5 , further comprising: recovering vaporized carbon dioxide; liquefying the vaporized carbon dioxide; recycling the liquefied carbon dioxide. 7. The method of claim 1 , wherein the passing and the measuring are performed at least until the measured property achieves a steady state or a pseudo steady state. 8. The method of claim 1 , wherein the terminating is performed at a time period of between 15 minutes and 45 minutes after the measured property achieves a steady state or a pseudo steady state. 9. The method of claim 1 , further comprising fluidly connecting the extraction tank vessel to a separation tank vessel via the transfer line. 10. The method of claim 9 , further comprising holding the drill cuttings carrying the contaminants in the extraction tank vessel, separating the mixture at or in the separation tank vessel, and providing a measuring device in, or fluidly connected to, the transfer line.
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