Device for mixing powders by cryogenic fluid and generating vibrations

Patent metadata

Field	Value
Publication number	US-10688459-B2
Application number	US-201615772327-A
Country	US
Kind code	B2
Filing date	Nov 3, 2016
Priority date	Nov 4, 2015
Publication date	Jun 23, 2020
Grant date	Jun 23, 2020

Abstract

A device for mixing powders by a cryogenic fluid, characterised in that it comprises: a chamber for mixing the powders, comprising a cryogenic fluid, provided with means for forming a fluidised powder bed; a chamber for supplying powders in order to allow the powders to be introduced into the mixing chamber; a chamber for supplying cryogenic fluid in order to allow the cryogenic fluid to be introduced into the mixing chamber; a system for generating vibrations in the fluidised powder bed; and a system for controlling the system for generating vibrations.

First claim

The invention claimed is:

1. Device for mixing powders by a cryogenic fluid, comprising:
a chamber for mixing the powders, comprising a cryogenic fluid, provided with means for forming a fluidised powder bed,
a chamber for supplying powders in order to allow the powders to be introduced into the mixing chamber,
a chamber for supplying cryogenic fluid in order to allow the cryogenic fluid to be introduced into the mixing chamber,
a system for generating vibrations in the fluidised powder bed,
a system for controlling the system for generating vibrations.

2. Device according to claim 1 , wherein the powders to be mixed are actinide powders.

3. Device according to claim 1 , wherein the cryogenic fluid comprises a slightly hydrogenated liquid, which is a liquid comprising at most one hydrogen atom per molecule of liquid, having a boiling temperature less than that of water.

4. Device according to claim 1 , wherein it further comprises a system for analysing the concentration of the suspension of powders and of the cryogenic fluid in the mixing chamber, of which the operation is in particular controlled by the controlling system.

5. Device as claimed in claim 1 , wherein the mixing chamber is configured in such a way that the introduction of cryogenic fluid into the latter allows for a fluidisation of the powders to be mixed by percolation of the cryogenic fluid through the powder bed fluidised as such.

6. Device as claimed in claim 1 , wherein the mixing chamber comprises a distribution system, in particular a grille or a sintered part, of the cryogenic fluid through the fluidised bed of powders in order to allow for a homogeneous distribution of the cryogenic fluid in the fluidised bed.

7. Device as claimed in claim 1 , wherein the system for generating vibrations is at least partially located in the fluidised bed of powders.

8. Device according to claim 7 , wherein the system for generating vibrations comprises sonotrodes introduced into the fluidised bed of powders.

9. Device according to claim 8 , wherein the sonotrodes are controlled independently by the controlling system in order to induce a periodic phase shift of the phases between the sonotrodes in order to introduce unsteady interferences that improve the mixture within the fluidised bed powders.

10. Device according to claim 7 , wherein the sonotrodes are configured to generate pseudo-chaotic oscillations of the Van der Pol type.

11. Device as claimed in claim 1 , wherein it further comprises means for agitation in the mixing chamber so as to allow the mixing of the powders placed in suspension in the cryogenic fluid.

12. Device as claimed in claim 1 , wherein it comprises a system of electrostatic charge of the powders intended to be introduced into the mixing chamber.

13. Device according to claim 12 , wherein a portion of the powders is put into contact with a portion of the electrostatic charge system in order to be positively electrostatically charged and wherein the other portion of the powders is put into contact with the other portion of the electrostatic charge system in order to be negatively electrostatically charged, in order to allow for a differentiated local agglomeration.

14. Device as claimed in claim 1 , wherein the cryogenic fluid is liquefied nitrogen.

15. Method for mixing powders by a cryogenic fluid, implemented by means of a device as claimed in claim 1 , comprising the following steps:
a) introduction of powders intended to be mixed into the mixing chamber through the chamber for supplying powders,
b) introduction of cryogenic fluid intended to allow for the fluidisation of the fluidised bed of powders into the mixing chamber through the chamber for supplying cryogenic fluid,
c) setting into vibration of the suspension of powders and of cryogenic fluid in the mixing chamber through the system for generating vibrations,
d) obtaining of a mixture formed from powders after evaporation of the cryogenic fluid.

16. Method according to claim 15 , wherein during the first step a), the powders are electrostatically charged differently in order to favour differentiated local agglomeration.

17. Method according to claim 15 , wherein it also comprises the step of controlling the system for generating vibrations through the controlling system.

Assignees

• Commissariat Energie Atomique

Inventors

• Brothier Méryl
• Vaudez Stéphane

Classifications

• B01F33/40

  Mixers using gas or liquid agitation, e.g. with air supply tubes · CPC title

• B01F31/80

  Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations · CPC title

• B01F23/80

  After-treatment of the mixture · CPC title

• B01F23/66 Primary

  by evaporating or liquefying at least one of the components; using a fluid which is evaporated after mixing · CPC title

• B01F23/60

  Mixing solids with solids · CPC title