Methods for gel reduction in polyolefins

Patent metadata

Field	Value
Publication number	US-10682797-B2
Application number	US-201615545384-A
Country	US
Kind code	B2
Filing date	Jan 20, 2016
Priority date	Jan 21, 2015
Publication date	Jun 16, 2020
Grant date	Jun 16, 2020

Abstract

Methods for extrusion of polyolefins (112) that control specific energy input to the extruder (102) for gel reduction. Disclosed herein is an example method for forming plastic products (120, 208) with reduced gels, comprising: melting a polyolefin resin (112) in extruder (102) to form a melt; adjusting specific energy input in the extruder (102) to reduce gels in the melt; and forming the melt into a polyolefin product (120, 208). Disclosed herein is also an example method for forming plastic products (120, 20) with reduced gels, comprising: melting a polyolefin resin in extruder (102) to form a melt; selecting a throttle valve (104) position for gel reduction; setting the throttle valve (104) at the selected throttle valve (104) position to restrict flow of the melt out of the extruder (102); and forming the melt into a polyolefin product (120, 208).

First claim

What is claimed is:

1. A method for forming plastic products with reduced gels, comprising:
melting a polyolefin resin in extruder to form a melt;
adjusting specific energy input in the extruder to reduce gels in the melt;
forming the melt into a polyolefin product, and
passing the melt through a screen pack, wherein the screen pack comprises an inlet screen having a size from 20 mesh to 80 mesh, one or more intermediate screens having a size of 100 mesh or greater, and an outlet screen having a size from 20 mesh to 80 mesh, wherein the one or more intermediate screens comprise a screen having a size from 20 mesh 80 mesh sandwiched between screens of 100 mesh or larger, wherein each screen having the size from 20 mesh to 80 mesh is separated by one or more screens having the size of 100 mesh or greater.

2. The method of claim 1 , wherein the step of adjusting the specific energy input comprises adjusting a throttle valve at an exit of the extruder to increase the specific energy input in the extruder.

3. The method of claim 1 , wherein the step of adjusting the specific energy input comprises restricting flow of the melt out of the extruder.

4. The method of claim 1 , wherein the step of adjusting the specific energy input comprises increasing suction pressure on a melt pump.

5. The method of claim 1 , wherein the one or more intermediate screens comprise at least one screen having a size from 200 mesh to 250 mesh.

6. The method of claim 1 , further comprising passing the melt through a pelletizer configured to form the melt into pellets.

7. The method of claim 1 , further comprising passing the melt through a die configured to form the first melt and/or the second melt into a polyolefin film.

8. The method of claim 1 , wherein the polyolefin resin comprises a polyolefin made from ethylene monomers or branched higher alpha-olefin monomers containing from 3 to 20 carbon atoms.

9. The method of claim 1 , wherein the polyolefin resin comprises a polyolefin having a density of from 0.910 g/cm 3 to 0.975 g/cm 3 .

10. The method of claim 1 , wherein the polyolefin resin comprises a polyolefin having a melt index ranging from 0.1 g/10 min to about 1000 g/10 min.

11. The method of claim 1 , wherein the polyolefin product comprises pellets, pipe, sheet, or a film.

12. A method for forming plastic products with reduced gels, comprising:
melting a polyolefin resin in extruder to form a melt;
selecting a throttle valve position for gel reduction;
setting the throttle valve at the selected throttle valve position to restrict flow of the melt out of the extruder;
forming the melt into a polyolefin product, and
passing the melt through a screen pack, wherein the screen pack comprises an inlet screen having a size from 20 mesh to 80 mesh, one or more intermediate screens having a size of 100 mesh or greater, and an outlet screen having a size from 20 mesh to 80 mesh, wherein the one or more intermediate screens comprise a screen having a size from 20 mesh 80 mesh sandwiched between screens of 100 mesh or larger, wherein each screen having the size from 20 mesh to 80 mesh is separated by one or more screens having the size of 100 mesh or greater.

13. The method of claim 12 , further comprising passing the melt through a pelletizer configured to form the melt into pellets.

14. The method of claim 12 , further comprising passing the melt through a die configured to form the first melt and/or the second melt into a polyolefin film.

15. The method of claim 12 , wherein the polyolefin resin comprises a polyolefin made from ethylene monomers or branched higher alpha-olefin monomers containing from 3 to 20 carbon atoms.

16. The method of claim 12 , wherein the polyolefin resin comprises a polyolefin having a density of from 0.910 g/cm 3 to 0.975 g/cm 3 .

17. The method of claim 12 , wherein the polyolefin resin comprises a polyolefin having a melt index range from 0.1 g/10 min to about 1000 g/10 min.

Assignees

• Univation Tech Llc

Inventors

• Abe Daudi A
• Locklear Brandon C
• Chu Yuet Meng
• Veariel T R

Classifications

• B29B9/065

  under-water, e.g. underwater pelletizers · CPC title

• B29B7/488

  Parts, e.g. casings, sealings; Accessories, e.g. flow controlling or throttling devices (discharging B29B7/582; feeding B29B7/60) · CPC title

• B29B7/428

  Parts or accessories, e.g. casings, feeding or discharging means · CPC title

• Y02P70/10

  Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working · CPC title

• B29C48/2552

  provided in the feeding, melting, plasticising or pumping zone, e.g. screw, barrel, gear-pump or ram · CPC title