Preparation of imides containing a fluorosulfonyl group
US-2017047607-A1 · Feb 16, 2017 · US
US10680285B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10680285-B2 |
| Application number | US-201816025676-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 2, 2018 |
| Priority date | Nov 13, 2015 |
| Publication date | Jun 9, 2020 |
| Grant date | Jun 9, 2020 |
A practical reading order for non-experts. Skip the full description unless you need deep technical detail.
What the patent document calls the invention.
A short plain-language summary of the technical disclosure.
Who owns or filed the patent and who is credited as inventor.
Filing, priority, publication, and grant dates set the timeline.
The legal scope of protection — read this for what is actually claimed.
Technology tags used to group this patent with similar filings.
Prior art links and similar publications in this corpus.
Official abstract text for this publication.
Methods for preparing electrolyte salts for alkaline earth metal-ion batteries (e.g., calcium and magnesium ion batteries) are described. The electrolyte salts comprise alkaline earth metal (e.g., Mg or Ca) salts of 3,4-dicyano-2-trifluoromethylimidazole (TDI). The methods comprise contacting TDI with an alkaline earth metal bis(trifluoroacetate) salt in trifluoroacetic acid.
Opening claim text (preview).
The embodiments of the invention in which an exclusive property or privilege is claimed are defined as follows: 1. A method for preparing an alkaline earth metal salt of 3,4-dicyano-2-trifluoromethylimidazole (TDI) useful as an electrolyte salt for an alkaline earth metal-ion battery, the method comprising: contacting TDI with a solution containing about 0.5 molar equivalents of an alkaline earth metal bis-trifluoroacetate salt of the formula (CF 3 CO 2 ) 2 M, dissolved in trifluoroacetic acid to form a TDI salt of formula: wherein M is an alkaline earth metal; and recovering the TDI salt. 2. The method of claim 1 , wherein M is Mg. 3. The method of claim 1 , wherein M is Ca. 4. The method of claim 1 , wherein salt of the formula (CF 3 CO 2 ) 2 M, is dissolved in trifluoroacetic acid at a concentration in the range of 0.05 to about 2 molar. 5. The method of claim 4 , wherein M is Mg ion. 6. The method of claim 4 , wherein M is Ca ion. 7. The method of claim 1 , wherein the step of recovering the TDI salt comprises filtration or evaporation of trifluoroacetic acid solvent. 8. A method for preparing an alkaline earth metal salt of 3,4-dicyano-2-trifluoromethylimidazole (TDI) useful as an electrolyte salt for an alkaline earth metal-ion battery, the method comprising: contacting TDI with a solution containing about 0.45 to about 0.75 molar equivalents of an alkaline earth metal bis-trifluoroacetate salt of the formula (CF 3 CO 2 ) 2 M, dissolved in trifluoroacetic acid to form a TDI salt of formula: wherein M is an alkaline earth metal; and recovering the TDI salt. 9. The method of claim 8 , wherein M is Mg. 10. The method of claim 8 , wherein M is Ca. 11. The method of claim 8 , wherein salt of the formula (CF 3 CO 2 ) 2 M, is dissolved in trifluoroacetic acid at a concentration in the range of 0.05 to about 2 molar. 12. The method of claim 11 , wherein M is Mg ion. 13. The method of claim 11 , wherein M is Ca ion. 14. The method of claim 8 , wherein the step of recovering the TDI salt comprises filtration or evaporation of trifluoroacetic acid solvent.
with hydrocarbon radicals, substituted by halogen atoms, attached to other ring members · CPC title
containing one or more sulfur atoms · CPC title
Accumulators with insertion or intercalation of metals other than lithium, e.g. with magnesium or aluminium · CPC title
containing also one or more oxygen atoms, e.g. nitrosyl halides · CPC title
characterised by the solvents · CPC title
Related publications grouped by family.
Answers are generated from the same data shown on this page.