High shear thin film machine for dispersion and simultaneous orientation-distribution of nanoparticles within polymer matrix

Patent metadata

Field	Value
Publication number	US-10675598-B2
Application number	US-201615561503-A
Country	US
Kind code	B2
Filing date	Mar 23, 2016
Priority date	Mar 24, 2015
Publication date	Jun 9, 2020
Grant date	Jun 9, 2020

Abstract

An improved a device and method for dispersion and simultaneous orientation of nanoparticles within a matrix is provided. A mixer having a shaft and a stator is provided. The shaft may have a rupture region and erosion region. Further, an orienter having an angled stationary plate and a moving plate are provided. The nanoparticles and the matrix are fed into the mixer. A rotational force is applied to the shaft to produce shearing forces. The shearing forces disperse and exfoliate the nanoparticles within the matrix. The dispersed mixture is outputted onto the moving plate. The moving plate is forced across the angled stationary plate to produce fully developed laminar shear flow. The fully developed laminar shear flow or the two-dimensional extensional drag flow orients the dispersed nanoparticles-matrix mixture.

First claim

What is claimed is:

1. A method to disperse and orient nanoparticles within a matrix, the method comprising:
providing a mixer having a stator and a shaft;
providing an orienter having a stationary plate and a moving plate;
feeding the nanoparticles and the matrix into the mixer;
applying a rotational force to the shaft, wherein shearing forces disperse the nanoparticles within the matrix;
exposing the nanoparticles and the matrix to an erosion region of the shaft having a substantially smooth surface;
outputting a dispersed mixture onto the moving plate; and
moving the moving plate, horizontally along a track, across the stationary plate, wherein the dispersed mixture is pressed between the moving plate and the stationary plate, and wherein the distance between the moving plate and the stationary plate decreases as the moving plate moves past the stationary plate; and
orienting the dispersed mixture with a laminar shear flow or a two-dimensional extensional drag flow.

2. The method of claim 1 , further comprising:
exposing the nanoparticles and the matrix to a rupture region of the shaft having surface irregularities.

3. The method of claim 1 , wherein the moving plate is coincident with a first horizontal plane and the stationary plate is angled relative to a second horizontal plane parallel and proximate to the first horizontal plane.

4. The method of claim 1 , further comprising:
pumping a fluid through one or more cooling channels within the stator of the mixer.

5. The method of claim 4 , further comprising:
inserting an elongated member within the one or more cooling channels to increase gas velocity passing through the one or more cooling channels.

6. The method of claim 4 , further comprising:
providing threading on a surface of the one or more cooling channels to increase surface area of the surface of the one or more cooling channels for dissipating heat.

7. The method of claim 1 , further comprising:
inserting a volume modifier into one or more cooling channels within the stator of the mixer to increase velocity and still maintain constant flow rates.

Assignees

• South Dakota Board Of Regents

Inventors

• Dash Ilchgerel
• Winter Robb M

Classifications

• B01F3/14

  Operations & Transport · mapped topic

• B01F2215/0049

  Operations & Transport · mapped topic

• B01F15/065

  Operations & Transport · mapped topic

• B01F7/00816 Primary

  Operations & Transport · mapped topic

• C08J3/203

  Solid polymers with solid and/or liquid additives · CPC title