Refrigerant analyzer and a method of using the same

Patent metadata

Field	Value
Publication number	US-10648943-B2
Application number	US-201615548378-A
Country	US
Kind code	B2
Filing date	Feb 2, 2016
Priority date	Feb 2, 2015
Publication date	May 12, 2020
Grant date	May 12, 2020

Abstract

A refrigerant analyzer including a pump, a filtering device, a temperature/humidity regulator, an electrochemical sensor, and a control device, wherein the refrigerant analyzer is configured to circulate conditioned air through the sensing chamber for an initialization duration of time to obtain an initial output value, determine whether the initial output value is stabilized below a predetermined initial limit, circulate a refrigerant through the sensing chamber for a sensing duration of time, operate the control device to measure a sensed output value, and operate the control device to determine a measured concentration of at least one contaminant within the refrigerant based on the sensed output value.

First claim

What is claimed is:

1. A method of detecting impurities in a refrigerant utilizing a refrigerant analyzer, wherein the refrigerant analyzer includes an electrochemical sensor operably coupled to a control device, the electrochemical sensor including a counter electrode disposed within an atmospheric regulated chamber and a sensing electrode disposed within a sensing chamber, the method comprising the steps:
circulating conditioned air through the sensing chamber for an initialization duration of time to obtain an initial output value;
determining whether the initial output value is stabilized below a pre-determined initial limit;
circulating a refrigerant through the sensing chamber for a sensing duration of time;
operating the control device to measure a sensed output value; and
operating the control device to determine a measured concentration of at least one contaminant within the refrigerant based on the sensed output value.

2. The method of claim 1 , wherein the pre-determined initial limit is less than or equal to approximately 4 microamperes per square centimeter.

3. The method of claim 1 , further comprising, after step (b) and prior to step (c), circulating a first medium through the sensing chamber for a baseline duration of time to obtain a baseline value.

4. The method of claim 3 , further comprising:
determining whether the baseline value is less than or equal to the initial output value;
and
determining whether the baseline value is increasing, if the baseline value is greater than the initial output value.

5. The method of claim 1 , wherein step (e) further comprises operating the control device to produce a signal indicative of the presence of contaminant(s) within the refrigerant.

6. The method of claim 1 , wherein the initialization duration of time is greater than or equal to approximately 5 minutes.

7. The method of claim 5 , wherein the contaminant(s) comprises methyl chloride.

8. The method of claim 7 , wherein the presence of methyl chloride comprises a measured concentration greater than or equal to approximately 0.5% of the refrigerant tested.

9. The method of claim 5 , wherein the signal is selected from a group consisting of an audio and a visual signal.

10. The method of claim 3 , wherein the baseline duration of time is less than or equal to approximately 3 minutes.

11. The method of claim 3 , wherein the first medium comprises a dry gas.

12. The method of claim 1 , wherein the sensing duration of time is less than or equal to approximately 3 minutes.

13. The method of claim 3 , wherein the measured concentration comprises the difference between the sensed output value and the baseline value.

14. The method of claim 1 , wherein the measured concentration comprises the difference between the sensed output value and the initial output value.

15. A refrigerant analyzer to detect impurities in a refrigerant comprising:
a pump, wherein the pump is configured to circulate conditioned air;
a filtering device operably coupled to the pump;
an electrochemical sensor, wherein the electrochemical sensor is configured to allow a refrigerant to flow therethrough to establish a sensed output value;
a control device operably coupled to the electrochemical sensor, wherein the control device is configured to measure an initial output value of conditioned air, a baseline value of a first medium, measure the sensed output value of the refrigerant, and determine a measured concentration of at least one contaminant within the refrigerant based on the sensed output value; and
a temperature/humidity regulator operably coupled to the electrochemical sensor and the filtering device, wherein the temperature/humidity regulator is configured to regulate a humidity value.

16. The refrigerant analyzer of claim 15 , wherein the electrochemical sensor is further configured to allow the first medium to flow therethrough to establish the baseline value.

17. The refrigerant analyzer of claim 15 , where the measured concentration comprises the difference between the sensed value and the initial output value.

18. The refrigerant analyzer of claim 16 , wherein the measured concentration comprises the difference between the sensed output value and the baseline value.

19. The refrigerant analyzer of claim 16 , wherein the control device is further configured to determine whether the baseline value is less than or equal to the initial output value.

20. The refrigerant analyzer of claim 15 , wherein the control device is further configured to produce a signal indicative of the presence of the at least one contaminant within refrigerant.

21. The refrigerant analyzer of claim 20 , wherein the at least one contaminant comprises methyl chloride.

22. The refrigerant analyzer of claim 21 , wherein the presence of methyl chloride comprises a measured concentration greater than or equal to approximately 0.5% of the refrigerant tested.

23. The refrigerant analyzer of claim 15 , wherein the humidity value is less than or equal to approximately 60 percent relative humidity.

24. The refrigerant analyzer of claim 15 , wherein the first medium comprises a dry gas.

Assignees

• Carrier Corp

Inventors

• Chen Lei
• Yang Zhiwei
• Clough Warren
• Rydkin Ivan

Classifications

• G01N33/0006

  Calibrating gas analysers · CPC title

• G01N27/4074

  for detection of gases other than oxygen · CPC title

• F25B49/00

  Arrangement or mounting of control or safety devices · CPC title

• G01N27/4065 Primary

  Circuit arrangements specially adapted therefor · CPC title

• F25B2400/12

  Inflammable refrigerants · CPC title