Analyzer and warm-up determination method

Patent metadata

Field	Value
Publication number	US-10648902-B2
Application number	US-201816168892-A
Country	US
Kind code	B2
Filing date	Oct 24, 2018
Priority date	Dec 26, 2017
Publication date	May 12, 2020
Grant date	May 12, 2020

Abstract

A spectrophotometer 1 comprises a control unit 45 with a warming-up determination unit 452 that determines the completion of a warming-up based on a variation amount of a detection signal in a predetermined duration when a light detector 7 detects a light from a sample chamber without loading the sample. Specifically, the warming-up determination unit 452 calculates a difference between a signal intensity of the detection signal detected by the light detector 7 at the time when the predetermined time passes and a signal intensity of the detection signal detected by the light detector 7 at a previous time and determines that a warming-up is complete when a value of the difference is less than a first threshold value. The warming-up determination unit 452 automatically determines the completion of warming-up independently from the determination by the user.

First claim

What is claimed is:

1. An analytical instrumentation, comprising:
a sample chamber that loads a sample;
a light source that radiates a light to a position of said sample in said sample chamber;
a light detector that detects said light from said sample chamber;
a warming-up determination unit that determines completion of warming-up of said analytical instrumentation based upon a variation amount of a detection signal in a predetermined duration when said light detector detects said light from said sample chamber without loading said sample;
wherein said warming-up determination unit determines that a difference between a detection signal at a time when said predetermined duration passes and a detection signal at a previous time, when said predetermined duration has passed, is less than a threshold value every time when said predetermined duration passes, and that said warming-up is complete when said difference less than said threshold value takes place multiple continuous times.

2. The analytical instrumentation, according to claim 1 , further comprising:
an input value detection circuit configured to detect a voltage or a current value input into the light source, wherein:
said warming-up determination unit determines that said warming-up is complete based on at least one variation amount selected from a group consisting of the voltage input to said light source in said predetermined duration and the current input to said light source in said predetermined duration.

3. The analytical instrumentation, according to claim 1 , further comprising:
a spectroscope that disperses light from said light source; and
a temperature detector that detects a temperature of said spectroscope;
wherein said warming-up determination unit determines that warming-up of said analytical instrumentation is complete based on a variation amount of said temperature detected with said temperature detector in a predetermined duration.

4. The analytical instrumentation, according to claim 1 , further comprising:
a duration determination unit that determines said predetermined duration with respect to a next determination with said warming-up determination unit based on said variation amount of said detection signal when said warming-up determination unit performs a determination during said predetermined duration.

5. The analytical instrumentation, according to claim 1 , further comprising:
a memory storage that stores a reference time that is a benchmark for said completion of said warming-up; and
a duration determination unit that determines said predeteimined duration, wherein the closer to the reference time said predetermined duration is, the shorter said predetermined duration is.

6. The analytical instrumentation, according to claim 1 , wherein said light source further comprising:
a first light source made of a deuterium lamp and a second light source made of a tungsten lamp; and
a light source switching unit that selectively switches a light from between said first light source and said second light source, so that a selected light is incident to said light detector;
wherein said light detector detects a light from said first light source in the predetermined duration.

7. A method of determining a warming-up of an analytical instrumentation that comprises a sample chamber that loads a sample, a light source that radiates a light to a position of said sample in said sample chamber, and a light detector that detects said light from said sample chamber; comprising:
a step of determining a completion of said warming-up based upon a variation amount of a detection signal in a predetermined duration when said light detector detects said light from said sample chamber without loading said sample in said sample chamber; and
wherein said step of determining additionally determines that a difference between a detection signal at a time when said predetermined duration passes and a detection signal at a previous time, when said predetermined duration has passed, is less than a threshold value every time when said predetermined duration passes, and that said warming-up is complete when said difference less than said threshold value takes place multiple continuous times.

Assignees

• Shimadzu Corp

Inventors

• Zushi Jumpei
• Yoshimura Hiroyuki

Classifications

• G01N21/01

  Arrangements or apparatus for facilitating the optical investigation · CPC title

• G01N2021/0162

  using microprocessors for control of a sequence of operations, e.g. test, powering, switching, processing · CPC title

• G01J3/027 Primary

  Control of working procedures of a spectrometer; Failure detection; Bandwidth calculation · CPC title

• G01N2201/126

  Microprocessor processing · CPC title

• G01N21/17

  Systems in which incident light is modified in accordance with the properties of the material investigated (where the material investigated is optically excited causing a change in wavelength of the incident light G01N21/63) · CPC title