Method for recovering pulp fiber from used hygiene product

Patent metadata

Field	Value
Publication number	US-10646386-B2
Application number	US-201616064073-A
Country	US
Kind code	B2
Filing date	Oct 24, 2016
Priority date	Dec 25, 2015
Publication date	May 12, 2020
Grant date	May 12, 2020

Abstract

Provided is a method for efficiently recovering pulp fiber from used hygiene products that include pulp fiber and a polymer absorbent. This method is characterized by including a step for introducing the used hygiene product into a treatment tank in which an aqueous solution with ozone dissolved therein has been introduced, and a step for treating the used hygiene product while infusing water into the treatment tank at a first flow rate, extracting the aqueous solution from the treatment tank at a second flow rate and introducing a gas containing ozone into the aqueous solution in the treatment tank, thereby decomposing the polymer absorbent, lowering the molecular weight thereof, and making the same dissolvable.

First claim

The invention claimed is:

1. A method of recovering pulp fibers from a used hygiene product which includes pulp fibers and a polymer absorbent material, the method comprising:
introducing the used hygiene product into a treatment tank with an ozone dissolved aqueous solution; and
decomposing the polymer absorbent material to lower a molecular weight of the polymer absorbent material and make the polymer absorbent material dissolvable,
wherein said decomposing comprises treating the used hygiene product under a circulation mode by
injecting water into the treatment tank by a first flow rate,
discharging the aqueous solution from the treatment tank by a second flow rate, and
introducing an ozone containing gas into the aqueous solution inside the treatment tank, wherein

a product of an ozone concentration (mass ppm) of the aqueous solution and a time (minute) of the treating the used hygiene product is 100 to 6000 mass ppm·minute.

2. The method according to claim 1 , wherein
the first flow rate R 1 (unit: L/minute) and a volume V (unit: L) of the aqueous solution inside the treatment tank satisfy formula (1):
0.05 ≤R 1 /V≤ 0.2  (1).

3. The method according to claim 1 , wherein
an ozone concentration of the aqueous solution is 1 to 30 mass ppm.

4. The method according to claim 1 , wherein
an ozone concentration of the ozone containing gas is 40 to 60 g/m 3 .

5. The method according to claim 1 , wherein
a flow rate R O (unit: L/minute) of the ozone containing gas and a volume V (unit: L) of the aqueous solution inside the treatment tank satisfy formula (2):
0.5 ≤R O /V≤ 1.25  (2).

6. The method according to claim 1 , wherein
a volume V (unit: L) of the aqueous solution inside the treatment tank and a mass W (unit: kg) of the used hygiene product satisfy formula (3):
3 ≤V/W≤ 50  (3).

7. The method according to claim 1 , further comprising:
extracting, from the treatment tank, a residue of the hygiene product from which the polymer absorbent material is removed.

8. The method according to claim 1 , further comprising:
washing a residue of the hygiene product and decomposing the residue of the hygiene product into components, by stirring the residue of the hygiene product from which the polymer absorbent material is removed in an aqueous solution or in water, including a disinfectant.

9. The method according to claim 8 , wherein
the disinfectant is sodium hypochlorite, chlorine dioxide, acidic electrolyzed water, ozone water, acidic ozone water, or ozone water including organic acid.

10. The method according to claim 8 , further comprising:
separating the pulp fibers from the decomposed residue of the hygiene product.

11. The method according to claim 1 , further comprising:
drying the pulp fibers until the dried pulp fibers have a moisture percentage of 5 to 13%.

12. The method according to claim 11 , wherein
a temperature at which the pulp fibers are dried in said drying is 100 to 200° C.

13. The method according to claim 1 , further comprising: separating and recovering a plastic material.

14. The method according to claim 1 , wherein
the second flow rate is the same as the first flow rate.

Assignees

• Unicharm Corp

Inventors

• Konishi Takayoshi
• Hiraoka Toshio
• Kameda Noritomo
• Ichiura Hideaki

Classifications

• A61F13/84 Primary

  Accessories, not otherwise provided for, for absorbent pads · CPC title

• D21C5/02

  Working-up waste paper (mechanical part D21B1/08, D21B1/32) · CPC title

• A61L2/18

  Liquid substances · CPC title

• A61L2/04

  Heat (radiation A61L2/08) · CPC title

• C08J11/16

  by treatment with inorganic material (C08J11/14 takes precedence) · CPC title