Carbon black composition for manufacturing particulate magnetic recording medium and method of manufacturing particulate magnetic recording medium

Patent metadata

Field	Value
Publication number	US-10640669-B2
Application number	US-201615280095-A
Country	US
Kind code	B2
Filing date	Sep 29, 2016
Priority date	Sep 30, 2015
Publication date	May 5, 2020
Grant date	May 5, 2020

Abstract

The carbon black composition for manufacturing a particulate magnetic recording medium contains carbon black, vinyl chloride resin containing one or more epoxy groups, the secondary monoamine denoted by formula 1, and solvent,

wherein, in formula 1, each of R 1 and R 2 independently denotes an alkyl group branching off at a carbon atom, the carbon atom being present at an α-position relative to an amine nitrogen atom, and having a main structure with 7 or fewer carbon atoms, it being possible for the alkyl group denoted by R 1 to be in the form of a cyclic structure, possible for the alkyl group denoted by R 2 to be in the form of a cyclic structure, and possible for the alkyl group denoted by R 1 and the alkyl group denoted by R 2 be connected to form a cyclic structure, with neither R 1 nor R 2 containing a hydroxyl group.

First claim

What is claimed is:

1. A carbon black composition,
which is a carbon black composition for manufacturing a particulate magnetic recording medium, and comprises:
carbon black,
vinyl chloride resin comprising one or more epoxy groups,
a secondary monoamine which is at least one selected from the group consisting of tetramethylpiperidine, isopropylcyclohexylamine, dicyclohexylamine, and di-sec-butylamine, and
solvent.

2. The carbon black composition according to claim 1 ,
wherein the vinyl chloride resin comprising one or more epoxy groups comprises one or more groups selected from the group consisting of a sulfonic acid group and a salt thereof.

3. The carbon black composition according to claim 1 ,
wherein the molecular weight of the secondary monoamine ranges from 85 to 300.

4. The carbon black composition according to claim 1 ,
wherein the secondary monoamine comprises at least one selected from the group consisting of an alkyl group having a branched methyl group, a piperidine ring, and a cyclohexane ring.

5. The carbon black composition according to claim 1 ,
wherein the boiling point of the secondary monoamine is greater than or equal to 100° C.

6. The carbon black composition according to claim 1 ,
wherein the solvent comprises ketone solvent.

7. The carbon black composition according to claim 1 ,
which comprises 2.0 to 10.0 weight parts of the secondary monoamine per 100.0 weight parts of the carbon black.

8. The carbon black composition according to claim 1 ,
which comprises 20.0 to 50.0 weight parts of the vinyl chloride resin comprising one or more epoxy groups per 100.0 weight parts of the carbon black.

9. The carbon black composition according to claim 1 ,
which is a nonmagnetic layer-forming composition of a particulate magnetic recording medium.

10. A method of manufacturing a particulate magnetic recording medium,
wherein the particulate magnetic recording medium comprises, on a nonmagnetic support, a nonmagnetic layer comprising nonmagnetic powder and binder and a magnetic layer comprising ferromagnetic powder and binder on the nonmagnetic layer,
the method comprises forming the nonmagnetic layer by coating and drying a carbon black composition on a nonmagnetic support,
wherein the carbon black composition comprises:

carbon black,
vinyl chloride resin comprising one or more epoxy groups,
a secondary monoamine which is at least one selected from the group consisting of tetramethylpiperidine, isopropylhexylamine, dicyclohexylamine, and di-sec-butylamine, and solvent.

11. The method of manufacturing a particulate magnetic recording medium according to claim 10 ,
wherein the vinyl chloride resin comprising one or more epoxy groups comprises one or more groups selected from the group consisting of a sulfonic acid group and a salt thereof.

12. The method of manufacturing a particulate magnetic recording medium according to claim 10 ,
wherein the molecular weight of the secondary monoamine ranges from 85 to 300.

13. The method of manufacturing a particulate magnetic recording medium according to claim 10 ,
wherein the secondary monoamine comprises at least one selected from the group consisting of an alkyl group having a branched methyl group, a piperidine ring, and a cyclohexane ring.

14. The method of manufacturing a particulate magnetic recording medium according to claim 10 ,
wherein the boiling point of the secondary monoamine is greater than or equal to 100° C.

15. The method of manufacturing a particulate magnetic recording medium according to claim 10 ,
wherein the solvent comprises ketone solvent.

16. The method of manufacturing a particulate magnetic recording medium according to claim 10 ,
wherein the carbon black composition comprises 2.0 to 10.0 weight parts of the secondary monoamine per 100.0 weight parts of the carbon black.

17. The method of manufacturing a particulate magnetic recording medium according to claim 10 ,
wherein the carbon black composition comprises 20.0 to 50.0 weight parts of the vinyl chloride resin comprising one or more epoxy groups per 100.0 weight parts of the carbon black.

18. The method of manufacturing a particulate magnetic recording medium according to claim 10 ,
which comprises forming the magnetic layer by coating and drying a magnetic layer-forming composition comprising ferromagnetic hexagonal ferrite powder and binder on the nonmagnetic layer.

Assignees

• Fujifilm Corp

Inventors

• Kitagawa Soichiro
• Aoshima Toshihide

Classifications

• C09D127/22 Primary

  modified by chemical after-treatment · CPC title

• C08K5/17

  Amines; Quaternary ammonium compounds · CPC title

• C08K3/04

  Carbon · CPC title

• C08K13/02

  Organic and inorganic ingredients · CPC title

• G11B5/7305

  Physics · mapped topic