Process for steam drawing carbon-fiber precursor acrylic fiber bundle

Patent metadata

Field	Value
Publication number	US-10604871-B2
Application number	US-201414900459-A
Country	US
Kind code	B2
Filing date	Jun 17, 2014
Priority date	Jun 21, 2013
Publication date	Mar 31, 2020
Grant date	Mar 31, 2020

Abstract

This process for manufacturing a carbon-fiber precursor acrylic fiber bundle and this steam drawing apparatus are characterized in that the drawing of an acrylic fiber bundle with a pressured-steam drawing apparatus is conducted by: opening an acrylic fiber bundle by blowing a fluid thereto; supplying humidifying steam to the opened acrylic fiber bundle at a fiber temperature of 80 to 130° C. to adjust the water content of the fiber bundle to 3 to 7%; and thereafter drawing the resulting acrylic fiber bundle in a pressurized-steam atmosphere. Thus, the present invention can prevent the breaking of a single fiber, the fluffing of the fiber bundle, and the breaking of the whole of the fiber bundle, though such defects are susceptible to occurring in a case where an acrylic fiber bundle is drawn by steam drawing at a high draw ratio, at a higher speed, or into a fiber having a small denier.

First claim

The invention claimed is:

1. A process for manufacturing a carbon-fiber precursor acrylic fiber bundle, comprising:
drawing an acrylic fiber bundle in a pressurized steam atmosphere, and in the following order:
opening the acrylic fiber bundle by spraying a fluid to the acrylic fiber bundle;
preheating the opened acrylic fiber bundle to 80° C. to 130° C.;
supplying a humidifying steam to the preheated acrylic fiber bundle thereby making the moisture content of the acrylic fiber bundle to be 3% to 7%; and
drawing the humidified acrylic fiber bundle in a pressurized steam atmosphere.

2. The process according to claim 1 , wherein the preheating is performed with a preheating roll or a heating plate.

3. The process according to claim 1 ,
wherein the humidifying steam is supplied to the preheated acrylic fiber bundle by introducing the preheated acrylic fiber bundle into a yarn humidifying device to which the humidifying steam is supplied.

4. The process according to claim 1 ,
wherein the humidifying steam is supplied to the preheated acrylic fiber bundle by spraying the humidifying steam to the preheated acrylic fiber bundle.

5. The process according to claim 1 ,
wherein the humidifying steam supplied to the preheated acrylic fiber bundle is a saturated steam.

6. The process according to claim 1 , comprising preheating the opened acrylic fiber bundle to 80° C. to 120° C.

7. The process according to claim 6 , wherein the moisture content of the acrylic fiber bundle is made to be 4% to 6%.

8. The process according to claim 1 , comprising preheating the opened acrylic fiber bundle to 80° C. to 100° C.

9. The process according to claim 8 , wherein the moisture content of the acrylic fiber bundle is made to be 4% to 6%.

10. The process according to claim 9 , comprising opening the acrylic fiber bundle by spraying air or steam to the acrylic fiber bundle at a flow rate of 300 to 700 NL/min and a pressure of 1 to 5 kgf/cm 2 .

11. The process according to claim 1 , wherein the moisture content of the acrylic fiber bundle is made to be 4% to 6%.

12. The process according to claim 1 , comprising opening the acrylic fiber bundle by spraying air or steam to the acrylic fiber bundle at a flow rate of 300 to 700 NL/min and a pressure of 1 to 5 kgf/cm 2 .

Assignees

• Mitsubishi Chem Corp

Inventors

• Tada Akishige
• Mizutori Yukihiro

Classifications

• D06C3/00

  Stretching, tentering or spreading textile fabrics; Producing elasticity in textile fabrics (shaping or stretching tubular fabrics upon cores or internal frames D06C5/00) · CPC title

• D01D5/16

  using rollers, or like mechanical devices, e.g. snubbing pins · CPC title

• D01F9/21

  from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds · CPC title

• D02J1/225

  Mechanical characteristics of stretching apparatus · CPC title

• D01F6/18

  from polymers of unsaturated nitriles, e.g. polyacrylonitrile, polyvinylidene cyanide · CPC title