System for increasing the bulk density of metal powder

Patent metadata

Field	Value
Publication number	US-10596629-B2
Application number	US-201615382359-A
Country	US
Kind code	B2
Filing date	Dec 16, 2016
Priority date	Oct 8, 2011
Publication date	Mar 24, 2020
Grant date	Mar 24, 2020

Abstract

An apparatus for increasing the bulk density of metal powder includes a sealed chamber, a nozzle, and a target. The sealed chamber has an inert environment. The nozzle is coupled to an inert gas source and is configured to introduce raw metal powder into a flow of the inert gas for discharge as a cold spray mixture of the raw metal powder and the inert gas into the sealed chamber. The target is housed within the sealed chamber and is configured to receive an impact of the cold spray mixture. The nozzle and the target are configured to flatten the raw metal particles into flattened metal particles in response to the cold spray mixture impacting the target.

First claim

What is claimed is:

1. An apparatus for increasing a bulk density of a metal powder, formed of a metal material, the apparatus comprising:
a sealed chamber;
a nozzle, coupled to an inert gas source and configured to discharge a cold spray mixture of raw metal particles and inert gas into the sealed chamber;
a target, housed within the sealed chamber and configured to receive an impact of the cold spray mixture in a manner causing plastic deformation of the raw metal particles into generally flattened metal particles; and
a target temperature control mechanism, configured to control a temperature of the target and to cool the target in a manner, preventing bonding of the raw metal particles to the target upon impact of the raw metal particles with the target.

2. The apparatus of claim 1 wherein:
the nozzle is configured to accelerate the cold spray mixture such that after impacting the target, the flattened metal particles have a bulk density of at least 10 percent of a theoretical density of the metal material.

3. The apparatus of claim 1 further comprising at least one of the following:
a powder heater for heating the raw metal particles prior to introducing the raw metal particles into the inert gas; or
a gas heater for heating the inert gas prior to discharge of the cold spray mixture from the nozzle.

4. The apparatus of claim 1 further comprising:
a vacuum source for generating sub-atmospheric pressure within the sealed chamber.

5. The apparatus of claim 1 wherein:
the target is formed of a material that is substantially similar to the metal material.

6. The apparatus of claim 1 further comprising:
an inert gas circulation loop fluidly coupling the sealed chamber to the nozzle.

7. The apparatus of claim 1 further comprising:
a container fluidly coupled to the sealed chamber and configured to receive flattened metal particles from the sealed chamber without exposing the flattened metal particles to an external atmosphere.

8. The apparatus of claim 7 wherein:
the container is located below the sealed chamber and receives the flattened metal particles by gravity feed.

9. The apparatus of claim 7 further comprising one or more fill tubes, fluidly coupling the container to the sealed chamber, and wherein each of the one or more fill tubes comprises a disconnect fitting for disconnecting the container from the sealed chamber.

10. The apparatus of claim 9 further comprising:
a cap for sealing each of the one or more fill tubes after disconnection of the container from the sealed chamber.

11. The apparatus of claim 7 wherein the container comprises one of the following:
a can for a hot isostatic pressing process; or
an elastomeric bag for a cold isostatic pressing process.

12. The apparatus of claim 1 wherein the metal powder comprises at least one of the following materials:
titanium, titanium alloy, aluminum, aluminum alloy, iron, iron alloy, steel, steel alloy, nickel-based alloy, copper-based alloy, beryllium, beryllium-based alloy, cobalt, cobalt-based alloy, molybdenum, molybdenum-based alloy, tungsten, or tungsten-based alloy.

13. A system for increasing a bulk density of a metal powder that comprises a metal material, the system comprising:
a sealed chamber;
a nozzle coupled to an inert gas source and configured to discharge a cold spray mixture of raw metal particles and inert gas into the sealed chamber;
a target housed within the sealed chamber and configured to receive an impact of the cold spray mixture in a manner causing plastic deformation of the raw metal particles into generally flattened metal particles;
a container, fluidly coupled to the sealed chamber and configured to receive the flattened metal particles from the sealed chamber without exposing the flattened metal particles to an external atmosphere, and wherein the container is configured for use in a compaction process for compacting the flattened metal particles; and
a target temperature control mechanism, configured to control a temperature of the target and to cool the target in a manner, preventing bonding of the raw metal particles to the target upon impact of the raw metal particles with the target.

14. The system of claim 13 wherein:
the container is located below the sealed chamber and receives the flattened metal particles by gravity feed.

15. The system of claim 13 further comprising:
one or more fill tubes, fluidly coupling the container to the sealed chamber, each of the one or more fill tubes comprising a disconnect fitting for disconnecting the container from the sealed chamber.

16. The system of claim 15 further comprising:
a cap for sealing each one of the one or more fill tubes after the container is disconnected from the sealed chamber.

17. The system of claim 13 wherein the container comprises one of the following:
an elastomeric bag for a cold isostatic pressing process; or
a can for a hot isostatic pressing process.

18. The system of claim 17 further comprising:
a chamber having chamber walls and configured to receive the elastomeric bag; and
a fluid source configured to inject fluid between the elastomeric bag and the chamber walls and hydrostatically pressurize the elastomeric bag in a cold isostatic pressing process to compact the flattened metal particles.

19. The system of claim 17 further comprising:
a degassing furnace for receiving the can; and
heating elements for applying heat to the can to promote release of outgassing material from the flattened metal particles.

20. The system of claim 19 further comprising:
a pressing furnace for receiving the can and containing inert gas for isostatically pressurizing the can in a hot isostatic pressing process to compact the flattened metal particles.

Assignees

• Boeing Co

Inventors

• Slattery Kevin Thomas

Classifications

• C23C24/06

  Compressing powdered coating material, e.g. by milling · CPC title

• B22F2998/00

  Supplementary information concerning processes or compositions relating to powder metallurgy · CPC title

• B22F3/003

  Apparatus, e.g. furnaces (in general F27B) · CPC title

• B22F3/16

  in successive or repeated steps · CPC title

• B22F2201/10

  Inert gases · CPC title