Compact device for mixing fluids

Patent metadata

Field	Value
Publication number	US-10569246-B2
Application number	US-201515514017-A
Country	US
Kind code	B2
Filing date	Aug 14, 2015
Priority date	Sep 29, 2014
Publication date	Feb 25, 2020
Grant date	Feb 25, 2020

Abstract

A device for mixing fluids for a downflow catalytic reactor ( 1 ), having
at least one substantially horizontal collector ( 5 ) provided with a substantially vertical collection conduit ( 7 ) receiving fluids collected by said collector ( 5 ); an injector ( 8 ) injecting a quench fluid opening into said collection conduit ( 7 ); a mixing chamber ( 9 ) located downstream of the collector ( 5 ) in the direction of movement of the fluids, having an inlet end connected directly to the collection conduit ( 7 ) and an outlet end ( 10 ) evacuating the fluids; and a pre-distribution plate ( 11 ) having a plurality of perforations and at least one riser ( 13 ), being located downstream of said mixing chamber ( 9 ) in the direction of movement of the fluids; the section of the mixing chamber ( 9 ) is a parallelogram and has at least one deflector ( 15 ) over at least one of the four internal walls of the mixing chamber ( 9 ) with a parallelogram section.

First claim

The invention claimed is:

1. A device enabling mixing of fluids for a downflow catalytic reactor ( 1 ), said device comprising:
at least one substantially horizontal collector ( 5 ) provided with a substantially vertical collection conduit ( 7 ) enabling fluids to be collected by said collector ( 5 );
at least one injector ( 8 ) enabling injection of a quench fluid which opens into said collection conduit ( 7 );
a mixing chamber ( 9 ) located downstream of the collector ( 5 ) in the direction of movement of the fluids, said chamber comprising an inlet end connected directly to said collection conduit ( 7 ) and an outlet end ( 10 ) enabling evacuation of the fluids; and
a pre-distribution plate ( 11 ) comprising a plurality of perforations and comprising at least one riser ( 13 ), said plate being located downstream of said mixing chamber ( 9 ) in the direction of movement of the fluids;

said mixing chamber ( 9 ) having a parallelogram shaped cross section and comprising at least one deflector ( 15 ) enabling deflection over at least one of the four internal walls of said mixing chamber ( 9 ) having a parallelogram cross section.

2. The device according to claim 1 , wherein the parallelogram cross section of said mixing chamber ( 9 ) is rectangular.

3. The device according to claim 1 , wherein said parallelogram cross section is such that the ratio between the height “h” of the section and the width “w” of said section is in the range of 0.2 to 1.0.

4. The device according claim 1 , wherein said deflector ( 15 ) occupies at most 5% by volume of the total volume of the mixing chamber, and at most 20% of the total surface area of the section of the mixing chamber.

5. The device according to claim 1 , wherein said mixing chamber comprises at least one deflector ( 15 ) located over a longest internal side wall ( 16 ).

6. The device according to claim 5 , comprising a plurality of deflectors ( 15 ) distributed over one or more horizontal levels of said longest internal side wall ( 16 ).

7. The device according to claim 6 , wherein said deflectors are spaced in a regular manner over said longest internal side wall ( 16 ) of the mixing chamber ( 9 ).

8. The device according to claim 6 , wherein said deflectors are spaced in an irregular manner over said longest internal side wall ( 16 ) of the mixing chamber ( 9 ).

9. The device according to claim 1 , wherein said deflector ( 15 ) is a baffle, a vane, an insert, or a blade.

10. The device according to claim 1 , wherein the pre-distribution plate ( 11 ) is located downstream of the mixing chamber ( 9 ) at a distance d 2 in the direction of movement of the fluids, the distance d 2 being in the range 0 to 100 mm.

11. The device according to claim 1 , wherein an arc of the mixing chamber ( 9 ) is in the range of 90 to 270 degrees.

12. A catalytic downflow reactor comprising a vessel ( 1 ) comprising at least two beds of catalyst ( 2 ; 14 ) separated by an intermediate zone comprising a fluid mixing device according to claim 1 .

13. The reactor according to claim 12 , wherein the outlet end ( 10 ) of the mixing chamber ( 9 ) of said mixing device is positioned in the radial direction of the vessel of said catalytic reactor ( 1 ).

14. The reactor according to claim 12 , wherein the mixing chamber ( 9 ) of said device is positioned at the periphery of the vessel of said catalytic reactor ( 1 ).

15. The reactor according to claim 12 , wherein said mixing chamber ( 9 ) of said mixing device is positioned at a distance d 1 from the reactor vessel ( 1 ), the distance d 1 being in the range of 0.5 to 25% of the diameter of the reactor.

16. A hydrotreatment, hydrodesulphurization, hydrodenitrogenation, hydrocracking, hydrogenation or hydrodearomatization reaction, comprising subjecting a feed to reaction in a reactor according to claim 12 .

Assignees

• Ifp Energies Now

Inventors

• Beard Philippe
• Bazer-Bachi Frederic
• Plais Cecile
• Augier Frederic
• Haroun Yacine

Classifications

• B01J2208/027

  Beds · CPC title

• B01J2208/00371

  gaseous · CPC title

• C10G45/02

  to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing · CPC title

• C10G65/12

  including cracking steps and other hydrotreatment steps · CPC title

• C10G45/44

  Hydrogenation of the aromatic hydrocarbons · CPC title