Distillation device comprising a column which as three or a plurality of cells in series through which fluid flows and method for distilling or extractive distillation by use of the distillation device

Patent metadata

Field	Value
Publication number	US-10569192-B2
Application number	US-201615741350-A
Country	US
Kind code	B2
Filing date	Jun 29, 2016
Priority date	Jul 3, 2015
Publication date	Feb 25, 2020
Grant date	Feb 25, 2020

Abstract

A distillation device comprising a column for separating a feed stream into a head product stream, a bottom product stream and optionally one or more side extraction streams, having three or more cells in 5 series through which fluid flows, wherein at least the first cell is integrated into the bottom of the column, for multi-stage heating and partial evaporation of the liquid flowing through the cells with the exception of the liquid from the last cell in an evaporation stage.

First claim

The invention claimed is:

1. A distillation apparatus comprising:
a column for fractionating a feed stream into a tops product stream, a bottoms product stream, and at least one side draw streams; and
at least three serially liquid-traversed cells, the at least three serially liquid-traversed cells being integrated into a bottom of the column for a partial-evaporation of liquid traversing the at least three serially liquid-traversed cells, wherein
the liquid from each of the at least three serially liquid-traversed cells, with the exception of a last cell of the at least three serially liquid-traversed cells, is passed through a respective evaporator stage and partially-evaporated therein to obtain a partially-evaporated stream in each respective evaporator stage, the partially-evaporated streams being supplied to a respective next downstream cell,
a direct flow of the liquid from a respective immediately preceding cell to the respective next downstream cell is prevented, and
a liquid reflux is provided from at least one of the at least three serially liquid-traversed cells, with the exception of the first cell, into the respective immediately preceding cell.

2. The distillation apparatus according to claim 1 , wherein the partial-evaporation is effected by mass flows, the mass flows being hot condensate.

3. The distillation apparatus according to claim 1 , wherein the liquid reflux is designed as an immersed feed.

4. The distillation apparatus according to claim 1 , wherein the liquid reflux is designed as a siphon.

5. A distillation apparatus comprising:
a column for fractionating a feed stream into a tops product stream, a bottoms product stream, and optionally one or more side draw streams; and
three or more serially liquid-traversed cells, at least a first cell of the serially liquid-traversed cells being integrated into a bottom of the column, for a multistage heating and a partial-evaporation of liquid traversing the serially liquid-traversed cells, wherein
the liquid from each of the three or more serially liquid-traversed cells, with the exception of a last cell of the serially liquid-traversed cells, is passed through a respective evaporator stage and partially-evaporated therein to obtain a partially-evaporated stream in each respective evaporator stage, the partially-evaporated streams being completely or partially supplied to a respective next downstream cell,
a direct flow of the liquid from a respective immediately preceding cell to the respective next downstream cell is prevented,
a liquid reflux is provided from at least one of the three or more serially liquid-traversed cells, with the exception of the first cell, into the respective immediately preceding cell, and
wherein all of the three or more serially liquid-traversed cells are integrated into the bottom of the column.

6. The distillation apparatus according to claim 5 , wherein the heating and partial-evaporation is effected by at least one of in-process and external energy sources.

7. The distillation apparatus according to claim 5 , wherein the heating and partial-evaporation is effected by mass flows.

8. The distillation apparatus according to claim 7 , wherein the mass flows are steam or hot condensate.

9. The distillation apparatus according to claim 7 , wherein the mass flows are hot condensate.

10. The distillation apparatus according to claim 5 , wherein
the heating and the partial-evaporation of the liquid traversing the first cell is effected using in-process mass flows, and
the heating and partial-evaporation of the liquid traversing a penultimate cell is effected using external energy sources.

11. The distillation apparatus according to claim 5 , wherein the respective evaporator stages are heat exchangers.

12. The distillation apparatus according to claim 5 , wherein the liquid reflux is designed as a direct liquid overflow over a weir, as an immersed feed or as a siphon.

13. A process for performing a distillation or an extractive distillation using a distillation apparatus according to claim 5 , in which a feed stream comprising a plurality of components is fractionated into a tops product stream, a bottoms product stream, and optionally one or more side draw streams.

14. The process according to claim 13 , wherein the feed stream is fractionated by extractive distillation such that the tops product stream comprises butane(s) and the bottoms product stream comprises butene(s), and optionally butadiene(s).

15. The process according to claim 14 , wherein the process is an extractive distillation for fractionating a reaction mixture from a dehydrogenation of butanes to produce butenes or from an oxydehydrogenation of butanes to produce butadiene.

16. The process according to claim 13 , wherein the feed stream is fractionated by extractive distillation such that the tops product stream comprises butene(s) and optionally butane(s) and the bottoms product stream comprises butadiene(s).

17. The distillation apparatus according to claim 5 , wherein the liquid reflux is designed as an immersed feed.

18. The distillation apparatus according to claim 5 , wherein the liquid reflux is designed as a siphon.

Assignees

• Basf Se

Inventors

• Asprion Norbert
• Heida Bernd
• Weidert Jan-Oliver
• Lang Ortmund

Classifications

• B01D3/32

  Other features of fractionating columns {; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30} · CPC title

• B01D3/14

  Fractional distillation {or use of a fractionation or rectification column} · CPC title

• B01D3/40

  Extractive distillation · CPC title

• B01D3/326

  Tray supports · CPC title

• B01D3/322 Primary

  Reboiler specifications · CPC title