Oriented silicon steel and method for manufacturing same

Patent metadata

Field	Value
Publication number	US-10566119-B2
Application number	US-201214646985-A
Country	US
Kind code	B2
Filing date	Dec 11, 2012
Priority date	Nov 26, 2012
Publication date	Feb 18, 2020
Grant date	Feb 18, 2020

Abstract

The invention discloses an oriented silicon steel with excellent magnetic properties and a manufacturing method thereof. The present invention obtains the oriented silicon steel with excellent magnetic properties by controlling the area ratio of small crystal grains of D<5 mm in an oriented silicon steel finished product to be not more than 3%, and controlling the ratio μ17/μ15 of the magnetic conductivity under the magnetic induction of 1.7 T and 1.5 T in the oriented silicon steel finished product to be 0.50 or more. In addition, by using a slab of the oriented silicon steel with suitable components and an optimized cold rolling step, the present invention effectively decreases the heating temperature of the slab and the production cost thereof, and simultaneously better controls the size and ratio of the crystal grains in the oriented silicon steel finished product and the magnetic conductivity in a certain range of magnetic induction, ensures that secondary recrystallization has good Goss texture orientation and finally, stably obtains the oriented silicon steel product with excellent magnetic properties.

First claim

The invention claimed is:

1. A manufacturing method of an oriented silicon steel, comprising the following steps in sequence:
heating a slab of the oriented silicon steel to 1100-1200° C. and then performing a hot rolling to obtain a hot rolled plate;
performing, directly after hot rolling without an annealing treatment of the hot rolled plate, a cold rolling on the hot rolled plate at a cold rolling reduction ratio of 85% or more, so as to obtain a cold rolled plate having a thickness of a finished product of the oriented silicon steel;
performing an annealing treatment on the cold rolled plate to obtain the finished product of the oriented silicon steel, wherein the annealing treatment comprises the following in sequence: decarbonization annealing, coating an annealing separator, high-temperature annealing, applying an insulating coating, and hot-stretching leveling annealing; and the manufacturing method further comprises: before the high-temperature annealing, performing a nitriding treatment on the cold rolled plate; wherein,
the slab of the oriented silicon steel comprises the following components by weight percentage: 2.5-4.0% of Si, 0.010-0.040% of acid-soluble aluminum Al, 0.004-0.012% of N, and 0.015% or less of S; and
an area ratio of small crystal grains having a grain size of less than 5 mm in the finished product of the oriented silicon steel is not more than 3%, and a ratio μ17/μ15 of a magnetic conductivity under magnetic induction of 1.7 T and 1.5 T in the finished product of the oriented silicon steel is 0.50 or more, wherein Goss texture in the finished product is within 7 degrees.

2. The manufacturing method of the oriented silicon steel according to claim 1 , wherein the area ratio of small crystal grains having a grain size of less than 5 mm in the finished product of the oriented silicon steel is not more than 2%.

3. The manufacturing method of the oriented silicon steel according to claim 1 , wherein the ratio μ17/μ15 of the magnetic conductivity under magnetic induction of 1.7 T and 1.5 T in the finished product of the oriented silicon steel is 0.55 or more.

Assignees

• Baoshan Iron & Steel

Inventors

• Yang Guohua
• Liu Xiandong
• Li Guobao
• Yang Yongjie
• Hu Zhuochao
• Hei Hongxu
• Zhang Jun
• Su Dejun
• Sun Huande
• Wu Meihong

Classifications

• C23C8/02

  Pretreatment of the material to be coated (C23C8/04 takes precedence) · CPC title

• C21D8/1222

  Hot rolling · CPC title

• C22C38/06

  containing aluminium · CPC title

• C21D6/008

  containing Si · CPC title

• C22C38/02 Primary

  containing silicon · CPC title