Method of making nanocrystalline metal flakes and nanocrystalline flakes made therefrom

Patent metadata

Field	Value
Publication number	US-10518329-B2
Application number	US-201615373585-A
Country	US
Kind code	B2
Filing date	Dec 9, 2016
Priority date	Dec 11, 2015
Publication date	Dec 31, 2019
Grant date	Dec 31, 2019

Abstract

A method of producing flakes containing nanostructures from a part made of a material. The method includes subjecting the part made of the material to peening by shots driven by ultrasonic energy for a period of time, wherein nanostructures form on the surface of the part and, subsequently, damage to the part caused by continued peening of the part by the shots driven by ultrasonic energy results in separation of flakes containing nanostructures from the part made of the material. Nanocrystalline flakes containing fractured surfaces, microcracks, nanograins and nanolamellae. Sensors comprising nanocrystalline flakes containing fractured surfaces, microcracks, nanograins and nanolamellae.

First claim

What is claimed is:

1. A method of producing flakes containing nano structures from a material, the method comprising:
providing a part made of the material;
subjecting the part made of the material to peening by shots driven by ultrasonic energy for a period of time, wherein nano structures form on the surface of the part and, subsequently, damage to the part caused by continued peening of the part by the shots driven by ultrasonic energy results in separation of flakes containing nanostructures from the part made of the material.

2. The method of claim 1 , wherein the ultrasonic energy density is in the range of 20-500 W/m 2 .

3. The method of claim 1 , wherein the period of time is in the range of 10 seconds to 200 minutes.

4. The method of claim 1 , the material is a metal or an alloy.

5. The method of claim 4 , the alloy is steel.

6. The method of claim 5 , wherein the steel is a stainless steel.

7. The method of claim 1 , the material is one of magnesium, copper, nickel, iron, aluminum, titanium and cobalt.

8. The method of claim 1 , the material is an alloy comprising one of copper, magnesium, nickel, iron, aluminum, titanium and cobalt.

9. The method of claim 1 , the material is a refractory metal.

10. The method of claim 9 , the refractory metal is one of niobium, tantalum, molybdenum and tungsten.

11. The method of claim 1 , the material is an alloy comprising one of niobium, tantalum, molybdenum and tungsten.

12. The method of claim 1 , the nanostructures are nanograins.

13. The method of claim 12 , the nanograins are in the size range of 20-100 nm.

14. The method of claim 12 , wherein the nanostructures are nanolamellae.

15. The method of claim 14 , wherein the thickness of the nanolamellae is in the range of 30-100 nm.

16. The method of claim 1 , wherein the flakes are in the size range of 10-1000 micrometers.

17. The method of claim 1 , wherein the flakes containing nanostructures are in the size range of 10-1000 micrometers.

Assignees

• Purdue Research Foundation

Inventors

• Han Qingyou
• Yin Fei
• Rakita Milan

Classifications

• B22F2999/00

  Aspects linked to processes or compositions used in powder metallurgy · CPC title

• B22F2009/045

  by other means than ball or jet milling · CPC title

• B22F9/04 Primary

  starting from solid material, e.g. by crushing, grinding or milling ({C22C1/1084 takes precedence}; crushing, grinding or milling, in general, see the relevant subclasses, e.g. B02C) · CPC title

• B22F2998/10

  Processes characterised by the sequence of their steps · CPC title

• B22F2304/10

  Micron size particles, i.e. above 1 micrometer up to 500 micrometer · CPC title