Direct analysis sampler
US-10352832-B2 · Jul 16, 2019 · US
US10495551B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10495551-B2 |
| Application number | US-201715832980-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 6, 2017 |
| Priority date | Dec 13, 2016 |
| Publication date | Dec 3, 2019 |
| Grant date | Dec 3, 2019 |
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A sampler for taking samples from a molten metal bath, particularly a molten iron includes a sample chamber assembly having a cover plate and a housing. The housing has first and second openings for an inflow conduit and a gas coupler, respectively. The first face has an analysis zone, a ventilation zone, and a distribution zone. A depth of the analysis zone is 0.5 mm to 1.5 mm. The cover plate and the housing are assembled together to form a sample cavity. The sample chamber assembly chills the molten iron received therein to a solidified white structure metal sample. An analysis surface of the sample lies in a first plane. In a flow direction of the molten iron, there are no increases in width of the sample cavity and a ratio of the length to depth of the sample cavity increases.
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What is claimed is: 1. A sampler for taking samples from a molten metal bath, the sampler comprising: a carrier tube having an immersion end; a sample chamber assembly arranged on the immersion end of the carrier tube, the sample chamber assembly comprising a cover plate and a housing, characterized in that the housing includes: an immersion end having a first opening for an inflow conduit and an opposing end having a second opening for a gas coupler; and a first face extending between the immersion end and the opposing end, wherein the cover plate and the housing are configured to be assembled together to form a sample cavity including a distribution zone, an analysis zone and a ventilation zone, a portion of the analysis zone overlying the distribution zone which is in direct flow communication with the first opening and configured to receive molten iron from the inflow conduit, wherein a depth of the analysis zone is 0.5 mm to 1.5 mm, wherein the sample cavity has dimensions of length, width and depth, wherein the length dimension is along the inflow direction of the molten metal, the depth dimension is perpendicular to the length dimension, and the width dimension is perpendicular to the both the depth dimension and the length dimension, wherein the distribution zone, the analysis zone and the ventilation zone are structured as a plurality of contiguous segments, each segment having a length to depth ratio, the length to depth ratios of the segments successively increasing as the distance from the first opening increases, wherein the assembled cover plate and housing are configured to chill the molten iron received therein to a solidified white structure metal sample, such that an analysis surface of the solidified white structure metal sample lies in a first plane, and wherein the first and second openings are spaced apart from the first plane. 2. The sampler according to claim 1 , characterized in that the sample cavity and the first and second openings are aligned along a common longitudinal axis. 3. The sampler according to claim 1 , characterized in that the analysis zone, distribution zone and ventilation zone are structured as a plurality of contiguous segments, each segment having a length to depth ratio, a sum of the length to depth ratios of the plurality of segments being greater than 25. 4. The sampler according to claim 1 , characterized in that there are no increases in the width dimension of at least a portion of the sample cavity in a flow direction of the molten iron which extends from the end of the distribution zone toward the second opening. 5. The sampler according to claim 1 , characterized in that a total length of the analysis zone and the ventilation zone is between 20 and 50 mm. 6. The sampler according to claim 1 , characterized in that the analysis zone has a uniform depth above the distribution zone. 7. The sampler according to claim 1 , characterized in that a cross-sectional area of at least a portion of the analysis zone gradually tapers in the flow direction of the molten iron. 8. The sampler according to claim 1 , characterized in that a cross-sectional area of the ventilation zone gradually tapers in the flow direction of the molten iron. 9. The sampler according to claim 1 , characterized in that a ratio of a mass of the sample chamber to a mass of the metal received within the sample collection volume is 9 to 12. 10. The sampler according to claim 1 , characterized in that the cover plate accounts for 10 to 20 percent of the mass of the sample chamber. 11. The sampler according to claim 1 , characterized in that a cross-sectional area of the inflow conduit is between 0.25 and 0.5 times of a cross-sectional area of the distribution zone. 12. The sampler according to claim 1 , characterized in that a bottom surface of the distribution zone intersects a closed bottom end of the analysis zone at an angle between 40 and 90°. 13. The sampler according to claim 1 , characterized in that the cover plate includes a sealing member configured to provide a substantially gas tight seal between the cover plate and the housing. 14. The sampler according to claim 1 , characterized in that the cover plate is secured to the housing by a metal clamp to form the sample chamber. 15. The sampler according to claim 1 , characterized in that the first and second openings are the only openings formed in the sample cavity, an end of the inflow conduit being secured within the first opening and an end of the gas coupler being secured within the second opening. 16. The sampler according to claim 1 , characterized in that a cross-sectional area of the inflow conduit is between 0.5 and 2 times of a cross-sectional area of the analysis zone. 17. The sampler according to claim 1 , characterized in that the inflow conduit, the distribution zone, the analysis zone, the ventilation zone and the gas coupler are sequentially arranged in this order in the flow direction of the molten iron. 18. The sampler according to claim 1 , characterized in that the first face of the housing includes a ridge protruding therefrom and surrounding the ventilation zone, the analysis zone and the distribution zone. 19. The sampler according to claim 1 , characterized in that when the cover plate and the housing are assembled together, the cover plate sits flush against the ridge of the housing along the first plane.
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