Achieving water release zone for dewatering thick fine tailings based on shearing parameter such as camp number

Patent metadata

Field	Value
Publication number	US-10494277-B2
Application number	US-201314408691-A
Country	US
Kind code	B2
Filing date	Jun 21, 2013
Priority date	Jun 21, 2012
Publication date	Dec 3, 2019
Grant date	Dec 3, 2019

Abstract

Various techniques are provided in relation to flocculation and/or dewatering of thick fine tailings, with shear conditioning of flocculated tailings material in accordance with a pre-determined shearing parameter, such as the Camp Number. One example method of treating thick fine tailings including dispersing a flocculant into the thick fine tailings to form a flocculating mixture; shearing the flocculating mixture to increase yield stress and produce a flocculated mixture; shear conditioning the flocculated mixture to decrease the yield stress and break down flocs, the shear conditioning being performed in accordance with the pre-determined shearing parameter to produce conditioned flocculated material within a water release zone where release water separates from the conditioned flocculated material. The conditioned flocculated material can then be subjected to dewatering, for example by depositing, thickening or filtering. The design, construction and/or operation of a flocculation pipeline assembly can be facilitated.

First claim

The invention claimed is:

1. A method of treating thick fine tailings, comprising:
in a flocculant dispersion stage, dispersing a flocculant into the thick fine tailings under turbulent flow conditions to form a flocculating mixture;
in a floc buildup stage, shearing the flocculating mixture to increase a yield stress of the flocculating mixture, build up flocs and reach a peak yield stress, thereby producing a flocculated mixture;
in a floc breakdown stage, shear conditioning the flocculated mixture under laminar flow conditions in accordance with a pre-determined shearing parameter to decrease the yield stress of the flocculated mixture and break down flocs, the pre-determined shearing parameter being sufficient to produce a conditioned flocculated material that is within a water release zone wherein release water separates from the conditioned flocculated material; and
in a dewatering stage, dewatering the conditioned flocculated material while within the water release zone; and
wherein the floc breakdown stage is performed in a pipeline assembly that is dimensioned based on the pre-determined shearing parameter to obtain the laminar flow conditions and reach the water release zone.

2. The method of claim 1 , wherein the pre-determined shearing parameter comprises a Camp Number.

3. The process of claim 1 , wherein the pre-determined shearing parameter is determined using a test kit comprising:
a vessel for receiving a sample mixture comprising a sample of the thick fine tailings and the flocculant;
a mixing element for mixing the sample mixture within the vessel;
a yield stress measurement device for measuring yield stress of the sample mixture during the mixing;
a timer for measuring the time during the mixing;
a shear rate measurement device for measuring the shear rate of the mixing; and
water release detector for determining when the sample mixture achieves the water release zone where water separates from the sample mixture.

4. The method of claim 1 , wherein the step of dewatering comprises depositing the conditioned flocculated material onto a sub-aerial deposition area.

5. The method of claim 1 , wherein the step of dewatering comprises supplying the conditioned flocculated material into a separation apparatus to separate the release water from a water-reduced tailings material.

6. The method of claim 1 , further comprising a step of empirically deriving the pre-determined shearing parameter.

7. The method of claim 1 , wherein the pre-determined shearing parameter comprises shear rate and residence time variables.

8. The method of claim 1 , wherein the shear conditioning of the flocculated mixture is performed up until a discharge point at which the flocculated mixture is expelled in order to undergo the dewatering.

9. The method of claim 8 , wherein the pre-determined shearing parameter is a Camp Number.

10. The method of any one of claims 9 , wherein the shear conditioning is provided by a pipeline assembly.

11. The method of claim 10 , wherein the pipeline assembly is provided with a length and a diameter sufficient to impart the shear conditioning to the flocculated mixture in accordance with the pre-determined shearing parameter.

12. The method of claim 1 , wherein the shear conditioning of the flocculated mixture is performed exclusively in a pipeline prior to dewatering, and the dewatering comprises depositing the depositing the conditioned flocculated material onto a sub-aerial deposition area.

13. The method of claim 1 , wherein the pre-determined shearing parameter comprises a pre-determined Camp Number that has been determined in laboratory tests, and the shear conditioning is implemented in a pipeline assembly such that the Camp Number is substantially similar.

14. The method of claim 5 , wherein the pre-determined shearing parameter comprises a dimensionless number.

15. The method of claim 6 , wherein the step of empirically deriving the pre-determined shearing parameter comprises:
determining rheological behaviour of a sample flocculation mixture comprising a sample of the thick fine tailings and the flocculant in a laboratory scale mixer, wherein the sample flocculation mixture increases in yield stress to form a sample flocculated mixture and then decreases in yield stress under shearing conditions;
determining a laboratory scale shearing parameter sufficient to bring the sample flocculated mixture within a water release zone in the laboratory scale mixer; and
determining the pre-determined shearing parameter so as to be substantially similar to the laboratory scale shearing parameter.

16. The method of claim 15 , wherein the pre-determined shearing parameter consists of shear rate and residence time variables.

17. The method of claim 15 , wherein the step of empirically deriving the pre-determined shearing parameter comprises laboratory experimentation.

18. The method of claim 17 , further comprising determining an equivalent pipe length and diameter for a pipeline assembly based on the pre-determined shearing parameter in order to provide the shear conditioning.

19. The method of claim 17 , wherein the laboratory scale mixer comprising a paddle mixer.

20. The method of claim 15 , wherein the step of determining rheological behaviour of the sample flocculation mixture, comprises:
determining an optimal flocculant dose range for addition to the sample of the thick fine tailings;
adding the flocculant into the sample of the thick fine tailings sample at the optimal flocculant dose range, to form a sample flocculating mixture;
imparting dispersive mixing to the sample flocculating mixture in order to promote dispersion of the flocculant and floc build up, to form the sample flocculated mixture;
imparting lower mixing to the sample flocculated mixture in order to commence floc breakdown until reaching the water release zone; and
determining a yield stress response over time of the flocculating mixture and the flocculated material and wherein the shear conditioning of the flocculated mixture is performed under laminar flow conditions.

21. The method of claim 20 , wherein the pre-determined shearing parameter consists of a Camp Number.

22. The method of claim 21 , wherein the shear conditioning of the flocculated mixture is performed up until a discharge point at which the flocculated mixture is expelled in order to undergo the dewatering.

23. The method of any one of claims 21 , wherein the shear conditioning is provided by a pipeline assembly.

24. A method of treating thick fine tailings, comprising:
in a flocculant dispersion stage, dispersing a flocculant into the thick fine tailings under turbulent flow conditions to form a flocculating mixture;
in a floc buildup stage, shearing the flocculating mixture to increase a yield stress of the flocculating mixture, build up flocs and reach a peak yield stress, thereby producing a flocculated mixture;
in a floc breakdown stage, shear conditioning the flocculated mixture under laminar flow conditions in accordance with a pre-determined shearing parameter to decrease the yield stress of the flocculated mixture and break down flocs, the pre-determined shearing parameter being sufficient to produce a conditioned flocculated material that is within a water release zone wherein release water separates from the conditioned flocculated material; and
in a dewatering stage, dewatering the conditioned flocculated material while within the water release zon

Assignees

• Suncor Energy Inc

Inventors

• Weiss Marvin
• Sanchez Ana
• Bugg Trevor
• Revington Adrian

Classifications

• C10G2300/1033

  Oil well production fluids · CPC title

• C10G2300/208

  Sediments, e.g. bottom sediment and water or BSW · CPC title

• C10G1/045 Primary

  Separation of insoluble materials · CPC title

• G06F30/13

  Architectural design, e.g. computer-aided architectural design [CAAD] related to design of buildings, bridges, landscapes, production plants or roads · CPC title

• C02F2103/10

  from quarries or from mining activities · CPC title