ICP analyzer

Patent metadata

Field	Value
Publication number	US-10490395-B2
Application number	US-201615163858-A
Country	US
Kind code	B2
Filing date	May 25, 2016
Priority date	May 27, 2015
Publication date	Nov 26, 2019
Grant date	Nov 26, 2019

Abstract

An ICP analyzer 100 includes a self-oscillation radio-frequency power supply unit 120 for supplying radio-frequency power for generating plasma to an induction coil 111 wound around a plasma torch 110 . To check the type of plasma torch 110 , the analyzer 100 further includes: a frequency measurement section 121 for measuring an output frequency of the power supply unit 120 ; a storage unit 190 holding a reference output frequency for each type of plasma torch; and a torch checker 132 for determining whether or not the output frequency measured by the frequency measurement section 121 after the plasma is lit agrees with any one of the reference output frequencies, and for giving notification of the determination result.

First claim

The invention claimed is:

1. An inductively coupled plasma analyzer including a self-oscillation power supply unit for supplying radio-frequency power for generating plasma to an induction coil wound around a plasma torch, the analyzer comprising:
a frequency counter for measuring an output frequency of the power supply unit;
a memory holding a set of plural reference output frequencies corresponding to each type of plasma torch from a set of plural types of plasma torches, each of the reference output frequencies being a frequency of the radio-frequency power supplied from the power supply unit when an appropriate radio-frequency power is supplied to a corresponding type of plasma torch;
an input unit for inputting a type of the plasma torch installed in the inductively coupled plasma analyzer; and
a control unit configured to determine whether or not the output frequency measured by the frequency counter after the plasma is lit agrees with the reference output frequency corresponding to the type of plasma torch input through the input unit held in the memory, for giving notification of a determination result; and for modifying operation of the plasma torch or induction coil based on a determination whether or not the output frequency measured by the frequency counter after the plasma is lit agrees with the reference output frequency corresponding to the type of plasma torch input through the input unit held in the memory.

2. The inductively coupled plasma analyzer according to claim 1 , further comprising:
an automatic torch setter for automatically switching the reference output frequency to a value corresponding to a different type of plasma torch when it is determined that the type of plasma torch corresponding to the reference output frequency used in the determination is different from the type of plasma torch installed in the inductively coupled plasma analyzer.

3. The inductively coupled plasma analyzer according to claim 1 , further comprising:
a controller for automatically changing a parameter setting to an optimum value for the plasma torch installed in the inductively coupled plasma analyzer when it is determined that the type of plasma torch corresponding to the reference output frequency used in the determination is different from the type of the installed plasma torch.

4. The inductively coupled plasma analyzer according to claim 1 , further comprising:
a power supply stopper for discontinuing a supply of the radio-frequency power from the power supply unit to the induction coil wound around the plasma torch when notification is given of a determination that the measured output frequency is different from the reference output frequency corresponding to the type of plasma torch previously set in a control unit by an operator.

5. An inductively coupled plasma analyzer including a self-oscillation power supply unit for supplying radio-frequency power for generating plasma to an induction coil wound around a plasma torch, the analyzer comprising:
a frequency counter for measuring an output frequency of the power supply unit;
a memory holding, for each type of plasma torch from a set of plural types of plasma torches, a reference output frequency difference which is the difference between two output frequencies respectively measured before and after the plasma is lit the reference output frequency difference being a difference between two output frequencies of the radio-frequency power supplied from the power supply unit respectively measured before and after the plasma is lit when an appropriate radio-frequency power is supplied to the corresponding type of plasma torch;
an input unit for inputting a type of the plasma torch installed in the inductively coupled plasma analyzer; and
a control unit configured to determine whether or not a difference between the output frequencies respectively measured by the frequency counter before and after the plasma is lit agrees with the reference output frequency difference corresponding to the type of plasma torch input through the input unit held in the memory, for giving notification of a determination result; and for modifying operation of the plasma torch or induction coil based on a determination whether or not the difference between the output frequencies respectively measured by the frequency counter before and after the plasma is lit agrees with the reference output frequency corresponding to the type of plasma torch input through the input unit held in the memory.

6. The inductively coupled plasma analyzer according to claim 5 , further comprising:
an automatic torch setter for automatically switching the reference output frequency difference to a value corresponding to a different type of plasma torch when it is determined that the type of plasma torch corresponding to the reference output frequency difference used in the determination is different from the type of plasma torch installed in the inductively coupled plasma analyzer.

7. The inductively coupled plasma analyzer according to claim 5 , further comprising:
a controller for automatically changing a parameter setting to an optimum value for the plasma torch installed in the inductively coupled plasma analyzer when it is determined that the type of plasma torch corresponding to the reference output frequency difference used in the determination is different from the type of the installed plasma torch.

8. The inductively coupled plasma analyzer according to claim 5 , further comprising:
a power supply stopper for discontinuing a supply of the radio-frequency power from the power supply unit to the induction coil wound around the plasma torch when notification is given of a determination that the difference between the output frequencies respectively measured before and after the plasma is lit is different from the reference output frequency difference corresponding to the type of plasma torch previously set in a control unit by an operator.

9. The inductively coupled plasma analyzer according to claim 1 , further comprising:
a torch-lighting detector for detecting a lighting of the plasma in the plasma torch.

10. The inductively coupled plasma analyzer according to claim 5 , further comprising:
a torch-lighting detector for detecting a lighting of the plasma in the plasma torch.

11. A plasma-torch checking method for an inductively coupled plasma analyzer including a plasma torch and a self-oscillation power supply unit for supplying radio-frequency power for generating plasma to an induction coil wound around the plasma torch, the method including steps of:
measuring an output frequency of the self-oscillation power supply unit by a frequency counter; and
inputting, using an input unit, a type of the plasma torch installed in the inductively coupled plasma analyzer;
determining by a control unit whether or not the measured output frequency agrees with a reference output frequency corresponding to the type of the plasma torch through the input unit held in a memory, giving notification of a determination result, the reference output frequency being a frequency of the radio-frequency power supplied from the power supply unit when an appropriate radio-frequency power is supplied to the corresponding type of the plasma torch; and modifying operation of the plasma torch or induction coil based on a determination whether or not the output frequency measured by the frequency counter after the plasma is lit agrees with the reference output frequency corresponding to the type of the plasma torch through the input unit held in the memory.

Assignees

• Shimadzu Corp

Inventors

• Yasuda Naoki

Classifications

• H05H1/30

  using applied electromagnetic fields, e.g. high frequency or microwave energy (H05H1/28 takes precedence) · CPC title

• H05H1/0037

  by spectrometry · CPC title

• G01N21/73 Primary

  using plasma burners or torches · CPC title

• H01J49/105 Primary

  using high-frequency excitation, e.g. microwave excitation, Inductively Coupled Plasma [ICP] · CPC title