Nozzle for wet gas scrubber

Patent metadata

Field	Value
Publication number	US-10478835-B2
Application number	US-201715793245-A
Country	US
Kind code	B2
Filing date	Oct 25, 2017
Priority date	Nov 22, 2016
Publication date	Nov 19, 2019
Grant date	Nov 19, 2019

Abstract

A nozzle and methods of gas stripping utilizing the nozzle are provided. A nozzle is provided comprising a ceramic nozzle assembly comprising an inlet at one end of a cylindrical portion, an outlet at one end of a conical portion; the cylindrical portion transitioning to the conical portion at an end of the cylindrical portion distal from the inlet; the conical portion transitioning to the cylindrical portion at an end of the conical portion distal from the outlet; and a ceramic vane assembly within the cylindrical portion; the vane assembly comprising a central vane support located substantially concentrically within the cylindrical portion, and a plurality of angled vanes extending from the central vane support to an inner wall of the cylindrical portion; wherein the ceramic nozzle assembly and the ceramic vane assembly are manufactured such that the two assemblies comprise a single piece of ceramic.

First claim

The invention claimed is:

1. A nozzle comprising,
a ceramic nozzle assembly comprising an inlet at one end of a cylindrical portion, an outlet at one end of a conical portion, wherein the cylindrical portion transitioning to the conical portion at an end of the cylindrical portion distal from the inlet, wherein the conical portion transitioning to the cylindrical portion at an end of the conical portion distal from the outlet; and
a ceramic vane assembly within the cylindrical portion, wherein the vane assembly comprising a central vane support located substantially concentrically within the cylindrical portion, and a plurality of angled vanes extending from the central vane support to an inner wall of the cylindrical portion,
wherein the ceramic nozzle assembly and the ceramic vane assembly are manufactured such that the two assemblies comprise a single piece of ceramic,
wherein the central vane support is rounded at ends proximate to the inlet and the outlet and perpendicular to a fluid flow through the nozzle;
wherein the cylindrical portion has an axial dimension of L1 and the conical portion has an axial dimension of L2, wherein the ratio of L1:L2 is 1 to 3.

2. The nozzle of claim 1 , wherein the plurality of angled vanes extending from the central vane support to the inner wall of the cylindrical portion are manufactured such that each edge joining each of the plurality of angled vanes to the central vane support has a greater cross-sectional area in a plane axial to a direction of a flow through the nozzle assembly than the same cross-sectional area at a midpoint of each of the plurality of angled vanes.

3. The nozzle of claim 2 , wherein the plurality of angled vanes extending from the central vane support to the inner wall of the cylindrical portion are manufactured such that each edge joining each of the plurality of angled vanes to the cylindrical portion has a greater cross-sectional area in a plane axial to a direction of a flow through the nozzle assembly than the same cross-sectional area at a midpoint of each of the plurality of angled vanes.

4. The nozzle of claim 1 , wherein the plurality of angled vanes are angled such that an angle of incidence from a flow through the vane assembly is 10 to 60 degrees.

5. The nozzle of claim 4 , wherein the angle of incidence is 20 to 35 degrees.

6. The nozzle of claim 1 , wherein the ratio of L1:L2 is 1.

7. The nozzle of claim 6 , wherein the ratio of L1:L2 is 2.

8. The nozzle of claim 1 , wherein the inlet has a diameter of D1 and the outlet as a diameter of D2, wherein the ratio of D1:D2 is 2 to 3.

9. The nozzle of claim 8 , wherein the ratio of D1:D2 is about 2.67.

10. The nozzle of claim 1 , wherein the single piece of ceramic comprises nitride bonded silicon carbide.

11. A nozzle comprising,
a ceramic nozzle assembly comprising an inlet at one end of a cylindrical portion, an outlet at one end of a conical portion, wherein the cylindrical portion transitioning to the conical portion at an end of the cylindrical portion distal from the inlet, wherein the conical portion transitioning to the cylindrical portion at an end of the conical portion distal from the outlet; and
a ceramic vane assembly within the cylindrical portion, wherein the vane assembly comprising a central vane support located substantially concentrically within the cylindrical portion, and a plurality of angled vanes extending from the central vane support to an inner wall of the cylindrical portion,
wherein the ceramic nozzle assembly and the ceramic vane assembly are manufactured such that the two assemblies comprise a single piece of ceramic, wherein the nozzle is manufactured by one of 3D-printing and co-sintering;
wherein the cylindrical portion has an axial dimension of L1 and the conical portion has an axial dimension of L2, wherein the ratio of L1:L2 is 1 to 3.

12. The nozzle of claim 11 , wherein the plurality of angled vanes extending from the central vane support to the inner wall of the cylindrical portion are manufactured such that each edge joining each of the plurality of angled vanes to the central vane support has a greater cross-sectional area in a plane axial to a direction of a flow through the nozzle assembly than the same cross-sectional area at a midpoint of each of the plurality of angled vanes.

13. The nozzle of claim 12 , wherein the plurality of angled vanes extending from the central vane support to the inner wall of the cylindrical portion are manufactured such that each edge joining each of the plurality of angled vanes to the cylindrical portion has a greater cross-sectional area in a plane axial to a direction of a flow through the nozzle assembly than the same cross-sectional area at a midpoint of each of the plurality of angled vanes.

14. The nozzle of claim 11 , wherein the plurality of angled vanes are angled such that an angle of incidence from a flow through the vane assembly is 10 to 60 degrees.

15. The nozzle of claim 14 , wherein the angle of incidence is 20 to 35 degrees.

16. The nozzle of claim 11 , wherein the ratio of L1:L2 is 1.

17. The nozzle of claim 16 , wherein the ratio of L1:L2 is 2.

18. The nozzle of claim 11 , wherein the inlet has a diameter of D1 and the outlet as a diameter of D2, wherein the ratio of D1:D2 is 2 to 3.

19. The nozzle of claim 18 , wherein the ratio of D1:D2 is about 2.67.

20. The nozzle of claim 11 , wherein the single piece of ceramic comprises nitride bonded silicon carbide.

21. The nozzle of claim 11 , wherein the plurality of angle vanes have a leading edge that is round beveled.

22. A method for removal of a contaminant gas from a gaseous stream comprising,
providing a gaseous stream containing a contaminant;
directing the gaseous stream through a wet gas scrubber; wherein the wet gas scrubber includes the nozzle of claim 1 ;
admitting a scrubbing liquid through the nozzle of claim 1 into the wet gas scrubber;

and mixing the gaseous stream with the scrubbing liquid such that the contaminant is adsorbed or stripped away in liquid droplets from the gaseous stream.

23. The method of claim 22 , wherein the gaseous stream is a flue gas from a refinery component.

24. The method of claim 23 , wherein the refinery component is a fluid catalytic cracker.

25. The method of claim 23 , wherein the contaminant is particulate matter entrained in the flue gas.

26. The method of claim 22 , wherein the contaminant is one of NOx, SOx, CO, and CO2.

Assignees

• Exxonmobil Res & Eng Co

Inventors

• Beatty Glenn M
• Fowler Christopher J
• Subramania Venkatesh
• Das Sandipan K
• Barnes John B
• Johnsen Laura

Classifications

• B05B1/3442

  the interface being a cone having the same axis as the outlet · CPC title

• B01J8/0055 Primary

  using cyclones · CPC title

• B01J19/02

  Apparatus characterised by being constructed of material selected for its chemically-resistant properties · CPC title

• B05B1/12 Primary

  capable of producing different kinds of discharge, e.g. either jet or spray (having selectively-effective outlets B05B1/16) · CPC title

• B01J4/002

  Nozzle-type elements (nozzle-type reactors B01J19/26) · CPC title