Dryer for preparation of dry nanoparticles

Patent metadata

Field	Value
Publication number	US-10473393-B2
Application number	US-201715717656-A
Country	US
Kind code	B2
Filing date	Sep 27, 2017
Priority date	Oct 17, 2016
Publication date	Nov 12, 2019
Grant date	Nov 12, 2019

Abstract

A system for producing dry nanoparticles from a liquid includes a closed tubing system which incorporates a mister, heater and an electrostatic collector therein. The system is able to produce dry nanoparticles from liquid-suspensions and from solvent solutions.

First claim

The invention claimed is:

1. A system for drying liquid-suspended nanoparticles comprising:
a closed tubing system including an access port for receiving a liquid solution therein, wherein the liquid solution contains suspended nanoparticles therein;
a mister for transforming the liquid solution into an aerosol containing droplets, wherein the droplets contain liquid and suspended nanoparticles;
a heater for heating a first portion of the closed tubing system, creating an updraft therein, and causing the aerosol to move through at least a second portion of the closed tubing system and further causing the evaporation of at least some liquid from the droplets in the aerosol, thereby leaving dried nanoparticles; and
an electrostatic collector comprised of one or more electrodes located in a third portion of the closed tubing system, wherein the dried nanoparticles are collected at the one or more electrodes of the electrostatic collector as the aerosol flows therethrough.

2. The system according to claim 1 , wherein the mister is selected from the group consisting of a nebulizer, an atomizer and an electrospray device.

3. The system according to claim 2 , wherein the mister produces aerosol droplets with sizes on the order of approximately 0.1 to 100 microns.

4. The system according to claim 1 , wherein the heater is selected from the group consisting of an infrared lamp, a hotplate and an electrical heating element.

5. The system according to claim 4 , wherein the temperature within the closed tubing system does not exceed 50 degrees Celsius.

6. The system according to claim 1 , wherein an approximate length of the closed tubing system from the mister to the electrostatic collector is at least 1 meter.

7. The system according to claim 1 , further comprising a fourth portion of the closed tubing for receiving any remaining aerosol, which is cooled therein, wherein any additional moisture generated from cooling is caught in a moisture trap at the end of the fourth portion of the closed tubing.

8. The system of claim 1 , wherein the electrostatic collector is comprised of interdigitated electrodes formed of alternating oppositely charged metal plates.

9. The system of claim 1 , wherein the dried nanoparticles have an approximate size range of 1 to 1000 nanometers.

10. A system for creating dry nanoparticles from a solution comprising:
a closed tubing system including an access port for receiving the solution therein, wherein the solution contains materials therein for forming nanoparticles;
a mister for transforming the solution into an aerosol containing droplets, wherein the droplets contain solvent and the materials therein;
a heater for heating a first portion of the closed tubing system, creating an updraft therein, and causing the aerosol to move through at least a second portion of the closed tubing system and further causing the evaporation of at least some liquid from the droplets in the aerosol and formation of dried nanoparticles from the materials; and
an electrostatic collector comprised of one or more electrodes located in a third portion of the closed tubing system, wherein the dried nanoparticles are collected at the one or more electrodes of the electrostatic collector as the aerosol flows therethrough.

11. The system according to claim 10 , wherein the mister is selected from the group consisting of a nebulizer, an atomizer and an electrospray device.

12. The system according to claim 11 , wherein the mister produces aerosol droplets with sizes on the order of approximately 0.1 to 100 microns.

13. The system according to claim 10 , wherein the heater is selected from the group consisting of an infrared lamp, a hotplate and an electrical heating element.

14. The system according to claim 13 , wherein the air temperature within the closed tubing system does not exceed 50 degrees Celsius.

15. The system according to claim 10 , wherein an approximate length of the closed tubing system from the mister to the electrostatic collector is at least 1 meter.

16. The system according to claim 10 , further comprising a fourth portion of the closed tubing for receiving any remaining aerosol, which is cooled therein, wherein any additional moisture generated from cooling is caught in a moisture trap at the end of the fourth portion of the closed tubing.

17. The system of claim 10 , wherein the electrostatic collector is comprised of interdigitated electrodes formed of alternating oppositely charged metal plates.

18. The system of claim 10 , wherein the dried nanoparticles have an approximate size range of 1 to 1000 nanometers.

19. The system of claim 10 , wherein the solvent solution has an initial concentration of up to 14.6 millimolar.

20. The system of claim 10 , wherein a solvent of the solvent solution is selected from the group consisting of ethanol, methanol and acetone.

Assignees

• Univ Georgetown

Inventors

• Van Keuren Edward
• Maglieri Grace
• Kosarzycki Roman
• Der Leon

Classifications

• B03C3/49

  tubular · CPC title

• B03C3/09

  characterised by presence of stationary flat electrodes arranged with their flat surfaces at right angles to the gas stream · CPC title

• B03C3/12

  characterised by separation of ionising and collecting stations · CPC title

• B03C3/76

  by using a mechanical vibrator, e.g. rapping gear {; by using impact} · CPC title

• B03C3/41

  Ionising-electrodes · CPC title