Process for dewatering microfibrillated cellulose
US-10240289-B2 · Mar 26, 2019 · US
US10472767B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10472767-B2 |
| Application number | US-201514755603-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 30, 2015 |
| Priority date | Mar 19, 2014 |
| Publication date | Nov 12, 2019 |
| Grant date | Nov 12, 2019 |
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A method to treat fibrous materials for use in the formation of a biocomposite material that significantly reduces or eliminates the odors emitted from the fibrous materials is provided. In the method, the fibers or fibrous materials are initially treated to extract the raw fiber from the source plant material and the remove unwanted fractions of the fiber, such as the hemicellulose, lignin, and pectin, among others, leaving only the intact cellulose fibers. These cellulose fibers are then further processed in a second step to remove the odor from the cellulose fibers. The second step includes a combination of a second chemical treatment, dehumidification, and/or a cold plasma modification to render the cellulosic fibers odorless.
Opening claim text (preview).
We claim: 1. A method for reducing/eliminating odors in a biocomposite material, the method consisting essentially of the steps of: a) separating a fibrous material from a raw fiber; and b) treating the fibrous material with an odor elimination process prior to performing any step that subject the fibrous material to heat, the odor elimination process consisting of chemically modifying the fibrous material and at least one or more of the steps of: dehumidifying the fibrous material by heating the fibers to a temperature of between about 35° C. to about 50° C. and cold plasma modification of the fibrous material, wherein the method does not include the addition of an oxidizing agent to the fibrous material in the chemical modification step, wherein the step of chemically modifying the fibrous material comprises i) performing a silane modification on the fibrous material; and ii) performing an acrylic modification on the fibrous material, and wherein the method further consists essentially of the step of washing the fibrous material after the acrylic modification step. 2. The method of claim 1 further consisting essentially of the step of washing the fibrous material after each modification step. 3. The method of claim 1 wherein the raw fiber is selected from the group consisting of flax and hemp. 4. The method of claim 1 wherein the odor elimination process does not affect the internal structure of the fibrous material.
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