Method of real-time prognosis of flooding phenomenon in packed column

Patent metadata

Field	Value
Publication number	US-10472640-B2
Application number	US-201715710849-A
Country	US
Kind code	B2
Filing date	Sep 21, 2017
Priority date	Mar 14, 2017
Publication date	Nov 12, 2019
Grant date	Nov 12, 2019

Abstract

A method of real-time prognosis of a flooding phenomenon in a packed column includes steps as follows. An online data collection step is conducted, wherein a plurality of values of the pressure drop are collected from the packed column under operation. A calculation step is conducted, wherein the values of the pressure drop are used to calculate a plurality of values of a steadiness index. A statistical step is conducted, wherein a value of a monitoring statistic is calculated based on the values of the steadiness index. A control step is conducted, wherein the value of the monitoring statistic is compared to a control limit, and an alarm is triggered when the value of the monitoring statistic is greater than the control limit.

First claim

What is claimed is:

1. A method of real-time prognosis of a flooding phenomenon in a packed column, comprising:
conducting an online data collection step, wherein a plurality of values of a pressure drop are collected from the packed column under operation;
conducting a calculation step, wherein the values of the pressure drop are used to calculate a plurality of values of a steadiness index;
conducting a statistical step, wherein a value of a monitoring statistic is calculated based on the values of the steadiness index; and
conducting a control step, wherein the value of the monitoring statistic is compared to a control limit, and an alarm is triggered when the value of the monitoring statistic is greater than the control limit; and
conducting an adjusting step after the alarm is triggered, wherein an operational condition of the packed column is adjusted to make the value of the monitoring statistic less than the control limit;
wherein each of the values of the steadiness index is calculated by Formula (1), Formula (2) and Formula (3):

S
2

=

∑

i
=
1

n

⁢

(

P
i

-

P
_

)

2

n
-
1

;

(
1
)

δ
2

2

=

∑

i
=
1

n
-
1

⁢

(

P

i
+
1

-

P
i

)

2

2
⁢

(

n
-
1

)

;

(
2
)

R
=

2
⁢

S
2

δ
2

;

(
3
)

wherein R is the steadiness index, S 2 is an estimator of a sample variance, δ 2 /2 is another estimator of the sample variance, P i is an ith value of the pressure drop, n is a sample size of the values of the pressure drop, P is a sample mean of the values of the pressure drop with the sample size of n, and i is an integral from 1 to n.

2. The method of real-time prognosis of the flooding phenomenon in the packed column of claim 1 , wherein the online data collection step is implemented by measuring the values of the pressure drop and delivering the values of the pressure drop to a computer via a sensing and transmitting element installed in the packed column, and the values of the pressure drop are recorded by the computer.

3. The method of real-time prognosis of the flooding phenomenon in the packed column of claim 2 , wherein the packed column further comprises a blower and a liquid pump, and the blower changes a gas flow rate and/or the liquid pump changes a liquid flow rate according to an instruction of the computer.

4. The method of real-time prognosis of the flooding phenomenon in the packed column of claim 1 , wherein the values of the pressure drop used in the calculation step is selected by a method of moving a time widow online.

5. The method of real-time prognosis of the flooding phenomenon in the packed column of claim 4 , wherein a size of the time window is 20, and a step length of the time window is 1.

6. The method of real-time prognosis of the flooding phenomenon in the packed column of claim 1 , wherein the value of the monitoring statistic and the control limit are obtained by a nonparametric statistical process control (SPC) method.

7. The method of real-time prognosis of the flooding phenomenon in the packed column of claim 6 , wherein the nonparametric SPC method is a nonparametric SPC method using Mann-Whitney test.

8. The method of real-time prognosis of the flooding phenomenon in the packed column of claim 1 , wherein, in the control step, the value of the monitoring statistic and the control

Assignees

• Univ Nat Tsing Hua
• Chang Chun Plastics Co Ltd
• Chang Chun Petrochemical Co Ltd

Inventors

• Yao Yuan
• Hseuh Bo-Fan

Classifications

• G01N30/8658

  Optimising operation parameters · CPC title

• B01D3/4211

  of columns · CPC title

• C12N15/70 Primary

  Vectors or expression systems specially adapted for E. coli · CPC title

• G01N30/52

  Physical parameters · CPC title

• G01N2030/889

  monitoring the quality of the stationary phase; column performance · CPC title