Systems for modifying pressure differential in a chemical vapor process

Patent metadata

Field	Value
Publication number	US-10465282-B2
Application number	US-201815941570-A
Country	US
Kind code	B2
Filing date	Mar 30, 2018
Priority date	Feb 29, 2016
Publication date	Nov 5, 2019
Grant date	Nov 5, 2019

Abstract

A process for densifying an annular porous structure comprising flowing a reactant gas into an inner diameter (ID) volume and through an ID surface of the annular porous structure, flowing the reactant gas through an outer diameter (OD) surface of the annular porous structure and into an OD volume, flowing the reactant gas from the OD volume through the OD surface of the annular porous structure, and flowing the reactant gas through an ID surface of the annular porous structure and into the ID volume.

First claim

The invention claimed is:

1. An apparatus for densifying an annular porous structure comprising:
a furnace;
a vacuum pump;
a reactant gas source;
a graphite susceptor disposed in the furnace, the graphite susceptor being configured to support a plurality of porous structures and a plurality of spacers disposed between adjacent porous structures, the graphite susceptor having a first opening, a second opening, a third opening, and a fourth opening, and each spacer comprising a solid ring;
an inner diameter (ID) volume defined as being radially inward from a first inside surface of each porous structure in the plurality of porous structures and a second inside surface of each spacer in the plurality of spacers;
an outer diameter (OD) volume defined as being radially outward from a first outer surface of each porous structure in the plurality of porous structures, a second outer surface of each spacer in the plurality of spacers, and an inner surface of the graphite susceptor, the OD volume and the ID volume being in fluid communication via the plurality of porous structures only;
a reversing valve having a first port and a second port, wherein the first port is coupled to a first inlet/outlet in the furnace and the first opening in the graphite susceptor via a first line, and wherein the second port is coupled to a second inlet/outlet in the furnace and the second opening and the third opening in the graphite susceptor via a second line; and
a plug disposed in the fourth opening;
wherein the reversing valve has an energized state and an unenergized state;
wherein the energized state comprises a first two-port state fluidly coupling the first port to the reactant gas source and fluidly coupling the second port to the vacuum pump and the unenergized state comprises a second two-port state fluidly coupling the first port to the vacuum pump and fluidly coupling the second port to the reactant gas source;
wherein, in the energized state, the first port conveys a reactant gas to the furnace and into the first opening of the graphite susceptor and into the ID volume;
wherein, in the energized state, the second port exhausts the reactant gas through at least one of the second opening disposed in the graphite susceptor and the third opening disposed in the graphite susceptor;
wherein, in the unenergized state, the second port conveys the reactant gas to the furnace and through the second opening and the third opening of the graphite susceptor and into the OD volume;
wherein, in the unenergized state, the first port exhausts reactant gas through the first opening disposed in the graphite susceptor.

2. The apparatus of claim 1 , wherein the furnace is at least one of gas heated or induction heated.

3. The apparatus of claim 1 , further comprising a processor configured to toggle the reversing valve from the energized state to the unenergized state.

Assignees

• Goodrich Corp

Inventors

• Rudolph James Warren
• She Ying
• Dardas Zissis A
• Filburn Thomas P
• St Rock Brian
• Linck John

Classifications

• C23C16/45523

  Pulsed gas flow or change of composition over time · CPC title

• C23C16/52

  Controlling or regulating the coating process {(C23C16/45557, C23C16/279 take precedence)} · CPC title

• C04B2235/77

  Density · CPC title

• C23C16/045 Primary

  Coating cavities or hollow spaces, e.g. interior of tubes; Infiltration of porous substrates · CPC title

• C04B35/83

  Carbon fibres in a carbon matrix · CPC title