Process for preparing detergent composition particles
US-2016186099-A1 · Jun 30, 2016 · US
US10465150B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10465150-B2 |
| Application number | US-201715585189-A |
| Country | US |
| Kind code | B2 |
| Filing date | May 3, 2017 |
| Priority date | May 3, 2016 |
| Publication date | Nov 5, 2019 |
| Grant date | Nov 5, 2019 |
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A cleaning composition comprising a particle said particle comprising: (a) from 30 to 70% by weight thereof of a polymer having a softening point in the range from about 20° C. to about 60° C.; (b) from 20 to 60% by weight thereof of a first material having a BET surface area greater than 100 m2/g and a D50 from about 5 to about 20 μm; (c) from 3 wt % to 15% by weight thereof of a second material having a BET surface area from about 0.01 to about 5 m2/g and a D50 from about 30 to about 100 μm.
Opening claim text (preview).
The invention claimed is: 1. A cleaning composition comprising a particle said particle comprising: (a) from about 40 to about 60% by weight thereof of a polymer comprising from about 69 to about 89% of methylpolyethylene glycol (meth)acrylate and from about 9 to about 29% of a salt of 3-methyl-1-vinylimidazolium; (b) from about 40 to about 50% by weight thereof of a silica having a BET surface area greater than 100 m2/g and a D50 from about 5 to about 20 μm; (c) from about 4 wt % to about 10% by weight thereof of a sulfate having a BET surface area from about 0.01 to about 5 m2/g and a D50 from about 50 to about 80 μm; and (d) citric acid, wherein the residual salt in the silica is less than about 2%, by total weight of the silica. 2. A composition according to claim 1 wherein the composition is an automatic dishwashing composition. 3. A composition according to claim 1 wherein the composition or part thereof is in powder form. 4. A process for making a composition according to claim 1 said process comprising the steps of making the particle by: a) admixing the silica and the sulfate materials; b) adding the polymer in the form of an aqueous solution to the mixture resulting from step a); c) drying the mixture resulting from step b); and d) adding the particle to the remaining components of the composition. 5. A process for making a composition according to claim 1 said process comprising the steps of making the particle by: a) admixing the silica and the sulfate materials; b) adding the polymer in the form of an aqueous solution to the mixture resulting from step a) wherein the aqueous solution comprises from about 20% to about 50% by weight of the solution of the polymer; c) drying the mixture resulting from step b); and d) adding the particle to the remaining components of the composition. 6. A process for making a composition according to claim 1 wherein the particle is made by agglomeration. 7. A process for making a composition according to claim 1 said process comprising the steps of making the particle by: a) admixing the silica and the sulfate materials; b) adding the polymer in the form of an aqueous solution to the mixture resulting from step a); c) drying the mixture resulting from step b) in a fluidized bed; and d) adding the particle to the remaining components of the composition.
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