Composition of heat-expandable microspheres and use thereof
US-2024191049-A1 · Jun 13, 2024 · US
US10457791B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10457791-B2 |
| Application number | US-201715497601-A |
| Country | US |
| Kind code | B2 |
| Filing date | Apr 26, 2017 |
| Priority date | Apr 1, 2009 |
| Publication date | Oct 29, 2019 |
| Grant date | Oct 29, 2019 |
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A method for producing a foamed thermally crosslinked mass system, wherein the mass system is foamed at a first temperature in a first step, and crosslinker substances are added to the mass system in a subsequent step at a second temperature lower than the first temperature, wherein the crosslinker substances are crosslinker substances for thermal crosslinking of the mass system.
Opening claim text (preview).
The invention claimed is: 1. A method for producing a self-adhesive, comprising: foaming a mass system comprising unexpanded microballoons at a first temperature, thereby forming a foamed mass system; mixing crosslinker substances into the foamed mass system at a second temperature, which is lower than the first temperature, thereby forming a blended mass system; and shaping the blended mass system to form a layer, thereby forming a self-adhesive, wherein the crosslinker substances are crosslinker substances for thermal crosslinking of the foamed mass system. 2. The method of claim 1 , wherein the first temperature is equal to or above an expansion temperature of the unexpanded microballoons and the second temperature is below the expansion temperature. 3. The method of claim 1 , wherein: in a first mixing assembly expandable microballoons and optionally further additives are introduced into a first mass system, thereby forming a second mass system; the second mass system is heated under superatmospheric pressure to a temperature which at least corresponds to, and is optionally higher than, an expansion temperature of the expandable microballoons under atmospheric pressure; the expandable microballoons are expanded on emergence from the first mixing assembly, thereby forming a third mass system; the third mass system is introduced into a second mixing assembly, whereby the third mass system is at a temperature below the expansion temperature of the unexpanded microballoons; the crosslinker substances are added to the second mixing assembly, thereby forming a fourth mass system; and the fourth mass system is shaped. 4. The method of claim 1 , wherein: in a first mixing assembly expandable microballoons and optionally further additives are introduced into a first mass system, thereby forming a second mass system; the first mixing assembly comprises a first mixing zone and a second mixing zone; the second mass system is heated under superatmospheric pressure in the first mixing zone to a temperature which is equal to or higher than an expansion temperature of the expandable microballoons under atmospheric pressure, thereby forming a third mass system; the third mass system is transferred from the first mixing zone into the second mixing zone; the third mass system in the second mixing zone is at a temperature below the expansion temperature of the expandable microballoons; the crosslinker substances are added during transfer of the third mass system to the second mixing zone and/or after transfer of the third mass system to the second mixing zone, thereby forming a fourth mass system; and the fourth mass system is shaped. 5. The method of claim 1 , wherein the self-adhesive is applied to a web-form carrier or a release material. 6. The method of claim 1 , wherein thermal crosslinking takes place after shaping. 7. The method of claim 1 , wherein the foamed mass system is in a noncrosslinked state. 8. A self-adhesive produced by the method of claim 1 . 9. A self-adhesive for a single or double-sided self-adhesive tape comprising the self-adhesive of claim 8 .
Pressure-sensitive adhesives [PSA] · CPC title
without carriers · CPC title
Microcapsules · CPC title
Shaping and joining components with different densities or hardness · CPC title
Homopolymers or copolymers of acrylic acid esters · CPC title
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