Method for producing conductive mayenite type compound
US-2018186650-A1 · Jul 5, 2018 · US
US10450198B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10450198-B2 |
| Application number | US-201615739331-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 21, 2016 |
| Priority date | Jun 25, 2015 |
| Publication date | Oct 22, 2019 |
| Grant date | Oct 22, 2019 |
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An object of the present invention is to provide a method for producing conductive mayenite, with which a reaction is completed in a short time, an operation can be simplified, the reaction is easily controlled, and the cost of energy can be reduced. The present invention is a method for producing conductive mayenite, characterized by mixing a mayenite type compound with a carbon component, placing the resulting mixture in an airtight container, and irradiating the mixture with a microwave in an inert gas atmosphere or in a vacuum atmosphere to heat the mixture.
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The invention claimed is: 1. A method for producing a conductive mayenite, characterized by mixing a mayenite (Ca 12 Al 14 O 33 ) with a carbon component, placing the resulting mixture in an airtight container, and irradiating the mixture with a microwave in an inert gas atmosphere or in a vacuum atmosphere to heat the mixture. 2. The method for producing a conductive mayenite according to claim 1 , characterized in that the mayenite (Ca 12 Al 14 O 33 ) has a crystal structure constituted by three-dimensionally connected cages. 3. The method for producing a conductive mayenite according to claim 1 , characterized in that the carbon component is at least one selected from the group consisting of silicon carbide, active carbon, graphite, carbon black, Ru/carbon, and graphene. 4. The method for producing a conductive mayenite according to claim 1 , characterized in that the airtight container is made of quartz glass. 5. The method for producing a conductive mayenite according to claim 1 , characterized in that the heating conditions of the mixture by the irradiation with the microwave are at 600 to 1200° C. for 5 to 60 minutes. 6. The method for producing a conductive mayenite according to claim 2 , characterized in that the carbon component is at least one selected from the group consisting of silicon carbide, active carbon, graphite, carbon black, Ru/carbon, and graphene. 7. The method for producing a conductive mayenite according to claim 2 , characterized in that the airtight container is made of quartz glass. 8. The method for producing a conductive mayenite according to claim 3 , characterized in that the airtight container is made of quartz glass. 9. The method for producing a conductive mayenite according to claim 6 , characterized in that the airtight container is made of quartz glass. 10. The method for producing a conductive mayenite according to claim 2 , characterized in that the heating conditions of the mixture by the irradiation with the microwave are at 600 to 1200° C. for 5 to 60 minutes. 11. The method for producing a conductive mayenite according to claim 3 , characterized in that the heating conditions of the mixture by the irradiation with the microwave are at 600 to 1200° C. for 5 to 60 minutes. 12. The method for producing a conductive mayenite according to claim 4 , characterized in that the heating conditions of the mixture by the irradiation with the microwave are at 600 to 1200° C. for 5 to 60 minutes. 13. The method for producing a conductive mayenite according to claim 6 , characterized in that the heating conditions of the mixture by the irradiation with the microwave are at 600 to 1200° C. for 5 to 60 minutes. 14. The method for producing a conductive mayenite according to claim 7 , characterized in that the heating conditions of the mixture by the irradiation with the microwave are at 600 to 1200° C. for 5 to 60 minutes. 15. The method for producing a conductive mayenite according to claim 8 , characterized in that the heating conditions of the mixture by the irradiation with the microwave are at 600 to 1200° C. for 5 to 60 minutes. 16. The method for producing a conductive mayenite type compound according to claim 9 , characterized in that the heating conditions of the mixture by the irradiation with the microwave are at 600 to 1200° C. for 5 to 60 minutes.
Carbon black · CPC title
Oxides · CPC title
Silicon carbide · CPC title
by peak-intensities or a ratio thereof only · CPC title
by NMR- or ESR-data · CPC title
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