Anode material, method for preparing the same, and lithium ion battery
US-2024322131-A1 · Sep 26, 2024 · US
US10421156B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10421156-B2 |
| Application number | US-201615373216-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 8, 2016 |
| Priority date | Dec 10, 2015 |
| Publication date | Sep 24, 2019 |
| Grant date | Sep 24, 2019 |
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A method for treating a raw-material powder includes forming a layer of the raw-material powder and removing oxide film formed on a surface of the raw-material powder from which the layer has been formed.
Opening claim text (preview).
What is claimed is: 1. A method for treating a raw-material powder in an object production system that uses powder bed fusion, the method comprising: forming a first layer of the raw-material powder; and removing oxide film formed on a surface of the raw-material powder from which the first layer has been made through chemical reduction, wherein the removal of the oxide film is performed by generating plasma through application of an AC voltage to an electrode in contact with the first layer in an atmosphere containing hydrogen and/or an inert element. 2. The method according to claim 1 for treating a raw-material powder, wherein: in the formation of the first layer, the first layer is formed in an evacuable enclosure; and the removal of the oxide film is performed with the enclosure evacuated to a sub-atmospheric pressure. 3. The method according to claim 2 for treating a raw-material powder, wherein the sub-atmospheric pressure is a pressure of 10 Pa or more and less than 10 kPa. 4. The method according to claim 2 for treating a raw-material powder, the method further comprising creating an atmosphere by evacuating the enclosure to a first pressure and then delivering an inert element into the enclosure to create the atmosphere of a second pressure that is higher than the first pressure and lower than atmospheric pressure. 5. The method according to any one of claim 2 for treating a raw-material powder, wherein the first layer is formed in a powder container located in the enclosure and electrically insulated from the enclosure. 6. The method according to claim 1 for treating a raw-material powder, wherein after the removal of the oxide film, a second layer is formed on the first layer. 7. The method according to claims 1 a for treating a raw-material powder, wherein the generation of plasma is performed with the first layer heated using a heater or an energy beam. 8. The method according to claim 1 for treating a raw-material powder, wherein the raw-material powder is metal particles formed by water atomization. 9. A method for producing an object using powder bed fusion, the method comprising: treating a raw-material powder by the method according to claim 1 ; and shaping with a beam including solidifying, through irradiation with an energy beam, the raw-material powder from which the oxide film has been removed.
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