Separation method and separation device

Patent metadata

Field	Value
Publication number	US-10413861-B2
Application number	US-201414896855-A
Country	US
Kind code	B2
Filing date	Jun 25, 2014
Priority date	Jul 5, 2013
Publication date	Sep 17, 2019
Grant date	Sep 17, 2019

Abstract

A separation method including: preparing a separation device including an absorption processor absorbing into an absorption liquid a target component in a fluid to be processed, by an absorption microduct and a cooling medium microduct positioned for heat exchange; causing the fluid to be processed and the absorption liquid to pass through the absorption microduct in mutual contact, thus causing the target component to be absorbed into the absorption liquid from the fluid to be processed; cooling the fluid to be processed and the absorption liquid by flowing a cooling medium through the cooling medium microduct, and causing heat exchange between the fluid to be processed and absorption liquid flowing through the absorption microduct and the cooling medium; and separating, into the fluid to be processed and the absorption liquid, the mixed fluid of the fluid to be processed after the target component has been absorbed by the absorption liquid.

First claim

The invention claimed is:

1. A separation device for separating a target component as a separation object from a fluid to be processed, the device comprising: an absorption processing unit configured to absorb the target component into an absorption liquid from the fluid to be processed; a post-absorption separation unit configured to separate a mixed fluid into the fluid to be processed and the absorption liquid, the mixed fluid including the fluid to be processed after the target component has been absorbed by the absorption liquid in the absorption processing unit and the absorption liquid after having absorbed the target component, wherein the absorption processing unit includes an absorption duct, the fluid to be processed and the absorption liquid passing through the absorption duct in a state of mutual contact such that the target component is absorbed into the absorption liquid from the fluid to be processed during the process of passing through, the absorption duct being a microduct, and a cooling medium duct disposed at a position at which heat exchange is possible with the absorption duct, a cooling medium having a lower temperature than a temperature of the fluid to be processed and absorption liquid flowing through the absorption duct is passing through the cooling medium duct, and a heat being exchanged between the fluid to be processed and absorption liquid flowing through the absorption duct and the cooling medium, the cooling medium duct being a microduct; and a first controller being configured to control the temperature of the cooling medium flowing through the cooling medium duct by controlling a flow rate of the cooling medium delivered by a cooling medium delivery unit, wherein when the temperature of the cooling medium detected by an exit side cooling medium temperature sensor is higher than 40° C., the first controller is configured to increase the flow rate of the cooling medium, and when the temperature of the cooling medium detected by an entry side cooling medium temperature sensor is lower than 100 C, the first controller is configured to decrease the flow rate of the cooling medium.

2. The separation device according to claim 1 , wherein the post-absorption separation unit mounted to the absorption processing unit includes an interior space communicating with an outlet of the absorption duct, the post-absorption separation unit being configured to separate the mixed fluid by a specific gravity difference, the mixed fluid being discharged from the outlet of the absorption duct and introduced into the interior space of the post-absorption separation unit.

3. A separation device for separating a target component as a separation object from a fluid to be processed, the device comprising:
an absorption processing unit configured to absorb the target component into an absorption liquid from the fluid to be processed;
a post-absorption separation unit configured to separate a mixed fluid into the fluid to be processed and the absorption liquid, the mixed fluid including the fluid to be processed after the target component has been absorbed by the absorption liquid in the absorption processing unit and the absorption liquid after having absorbed the target component;
a fluid to be processed discharge passage connected to the post-absorption separation unit, the fluid to be processed discharge passage being configured to discharge the fluid to be processed after the target component has been absorbed from the interior space of the post-absorption separation unit;
an absorption liquid discharge passage connected to the post-absorption separation unit, the absorption liquid discharge passage being configured to discharge the absorption liquid after having absorbed the target component from the interior space of the post-absorption separation unit;
a first check valve and a first pressure regulating valve provided in the fluid to be processed discharge passage, the first check valve being configured to prevent the fluid to be processed flowing through the fluid to be processed discharge passage from reversely flowing to the absorption separation unit side; and
a second check valve and a second pressure regulating valve provided in the absorption liquid discharge passage, the second check valve being configured to prevent the absorption liquid flowing to the absorption liquid discharge passage from reversely flowing to the absorption separation unit side,
wherein the absorption processing unit includes
an absorption duct, the fluid to be processed and the absorption liquid passing through the absorption duct in a state of mutual contact such that the target component is absorbed into the absorption liquid from the fluid to be processed during the process of passing through, the absorption duct being a microduct, and
a cooling medium duct disposed at a position at which heat exchange is possible with the absorption duct, a cooling medium having a lower temperature than a temperature of the fluid to be processed and absorption liquid flowing through the absorption duct is passing through the cooling medium duct, and a heat being exchanged between the fluid to be processed and absorption liquid flowing through the absorption duct and the cooling medium, the cooling medium duct being a microduct,
wherein the post-absorption separation unit mounted to the absorption processing unit includes an interior space communicating with an outlet of the absorption duct, the post-absorption separation unit being configured to separate the mixed fluid by a specific gravity difference, the mixed fluid being discharged from the outlet of the absorption duct and introduced into the interior space of the post-absorption separation unit, and
wherein the first pressure regulating valve and the second pressure regulating valve are configured to control a pressure of the fluid to be processed discharged to the fluid to be processed discharge passage and the pressure of the absorption liquid discharged to the absorption liquid discharge passage so that the pressure of the fluid to be processed and the absorption liquid become equal.

4. A separation device for separating a target component as a separation object from a fluid to be processed, the device comprising: an absorption processing unit configured to absorb the target component into an absorption liquid from the fluid to be processed, a post-absorption separation unit configured to separate a mixed fluid into the fluid to be processed and the absorption liquid, the mixed fluid including the fluid to be processed after the target component has been absorbed by the absorption liquid in the absorption processing unit and the absorption liquid after having absorbed the target component, wherein the absorption processing unit includes an absorption duct, the fluid to be processed and the absorption liquid passing through the absorption duct in a state of mutual contact such that the target component is absorbed into the absorption liquid from the fluid to be processed during the process of passing through, the absorption duct being a microduct, and a cooling medium duct disposed at a position at which heat exchange is possible with the absorption duct, a cooling medium having a lower temperature than a temperature of the fluid to be processed and absorption liquid flowing through the absorption duct is passing through the cooling medium duct, and a heat being exchanged between the fluid to be processed and absorption liquid flowing through the absorption duct and the cooling medium, the cooling medium duct being a microduct; a diffusion processing unit configured to diffuse the target component from the absorption liquid after having absorbed the target component separated by the post-absorption separation unit, wherein the diffusion processing unit includes a diffusion duct, the target component being diffuse

Assignees

• Kobe Steel Ltd

Inventors

• Fujisawa Akitoshi
• Noishiki Koji
• Matsuoka Akira

Classifications

• F28F2260/02

  having microchannels · CPC title

• F28D9/0037

  the conduits for the other heat-exchange medium also being formed by paired plates touching each other (F28D9/0043 takes precedence) · CPC title

• B01J19/00

  Chemical, physical or physico-chemical processes in general; Their relevant apparatus · CPC title

• B01D2252/204

  Amines · CPC title

• B01D53/1412

  Controlling the absorption process · CPC title