Drying methods

Patent metadata

Field	Value
Publication number	US-10406494-B2
Application number	US-201615558877-A
Country	US
Kind code	B2
Filing date	Mar 17, 2016
Priority date	Mar 20, 2015
Publication date	Sep 10, 2019
Grant date	Sep 10, 2019

Abstract

A process for drying resinous materials, comprising: delivering, by way of a plurality of resin channels, resin fluid comprising polymer and solvent into at least first and second steam channels (101) having within a flow of steam, the first and second steam channels (101) each receiving resin fluid from a plurality of resin channels, the first and second steam channels each (101) being received by a stage 1 manifold (121), the steam and resin being delivered under conditions so as to separate at least some of the solvent from the resin fluid; and collecting at least some of the polymer from the resin fluid.

First claim

What is claimed:

1. A process for drying resinous materials, comprising:
delivering, by way of a plurality of resin channels, resin fluid comprising polymer and solvent into at least first and second steam channels having within a flow of steam,
the first and second steam channels each receiving resin fluid from a plurality of resin channels,
the first and second steam channels each being received by a stage 1 manifold,
the steam and resin being delivered under conditions so as to separate at least some of the solvent from the resin fluid; and
collecting at least some of the polymer from the resin fluid,
wherein the stage 1 manifold is received by a stage 2 manifold, and wherein the flow at any of the stage 1 and stage 2 manifolds is a choked flow.

2. The process of claim 1 , wherein the mass flow ratio of resin fluid to steam in at least one of the first and second steam channels is in the range of from about 1:10,000 to about 10,000:1.

3. The process of claim 1 , wherein the stage 1 manifold receives from 2 to about 50 steam channels.

4. The process of claim 1 , wherein at least one of the first and second steam channels receives resin fluid from 2 to about 50 resin channels.

5. The process of claim 1 , wherein at least some of the resin channels received by the first steam channel share a resin source with at least some of the resin channels received by the second steam channel.

6. The process of claim 1 , wherein the steam mass flow rate in the first, second, or both steam channels is in the range of from about 0.045 kg/hour to about 6804 kg/hour.

7. The process of claim 6 , wherein the resin fluid flow rate in the first, second, or both steam channels is in the range of from about 0.045 kg/hour to about 4535 kg/hr.

8. The process of claim 1 , wherein the steam velocity in the first, second, or both steam channels is in the range of from about 0.1 to about 1000 m/s.

9. The process of claim 1 , wherein the resin fluid velocity in the first, second, or both steam channels is in the range of from about 1 to about 200 m/s.

10. The process of claim 1 , wherein the mass ratio of the solvent present in the collected polymer to the solvent in the resin fluid is from about 1:1 to about 1:10,000.

11. The process of claim 1 , wherein the collected polymer is in the form of particulate.

12. The process of claim 11 , wherein the collected polymer has an average cross-sectional dimension in the range of from about 400 micrometers to about 1500 micrometers.

13. The process of claim 11 , further comprising heating collected polymer so as to remove solvent from the collected polymer.

14. The process of claim 1 , wherein the stage 1 manifold is received by a stage 2 manifold, wherein the stage 2 manifold is received by a stage 3 manifold, and wherein the flow at any of the stage 1, stage 2, and stage 3 manifolds is a choked flow.

15. The process of claim 1 , wherein at least one resin channel delivers the resin to the steam channel at an angle of between about 1 degrees and about 179 degrees with relation to the direction of flow of the steam in the channel.

16. The process of claim 14 , wherein at least one resin channel delivers the resin to the steam channel at an angle of between about 30 degrees and 120 degrees with relation to the direction of flow of the steam in the channel.

17. The process of claim 1 , wherein multiple resin channels diverge from an inlet.

18. The process of claim 17 , wherein the total cross-sectional area of the resin channels is about the same as the cross-sectional area of the inlet.

19. The process of claim 17 , wherein the stage 1 manifold has a cross-sectional area within about 50% of the total cross-sectional area of the steam channels in fluid communication with the first stage 1 manifold.

Assignees

• Sabic Global Technologies Bv

Inventors

• Gautam Pankaj Singh
• Hocker Thomas
• Hollar Jr William E
• Mahood James Alan
• Peters Richard

Classifications

• B29B13/06 Primary

  by drying (B29B13/08 takes precedence {; drying moulded articles or half products B29C37/0092}) · CPC title

• C08G64/406

  Purifying; Drying · CPC title

• B29B13/065

  of powder or pellets · CPC title

• B01J2/02 Primary

  by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops · CPC title

• C08J3/122

  Pulverisation by spraying · CPC title