Method and system for recovery of precious metal

Patent metadata

Field	Value
Publication number	US-10400307-B2
Application number	US-201816181411-A
Country	US
Kind code	B2
Filing date	Nov 6, 2018
Priority date	Jun 28, 2016
Publication date	Sep 3, 2019
Grant date	Sep 3, 2019

Abstract

A method and to an arrangement for recovery of precious metal. The method includes calculating a first electrical property of a slurry downstream of a retention screen in a first flow direction A either (i) based on a first difference between the first supplied current and the first received voltage, or (ii) based on a first difference between the first supplied voltage and the first received current, calculating a second electrical property of the slurry upstream of the retention screen either (i) based on a second difference between the second supplied current and the second received voltage, or (ii) based on a second difference between the second supplied voltage and the second received current, and calculating the adsorption particle content of the slurry upstream of the retention screen based on a difference between the first and the second electrical property.

First claim

The invention claimed is:

1. A method for recovery of precious metal, the method comprising:
arranging a plurality of adsorption vessels in series, wherein each adsorption vessel comprises a reactor space, a closed retention space within the reactor space, a retention screen between the reactor space and the closed retention space, a first inlet configured to feed slurry containing precious metal into the reactor space, a second inlet configured to feed adsorption particles into the reactor space, a first outlet configured to feed slurry containing precious metal from the closed retention space, and a second outlet configured to feed adsorption particles from the reactor space;
feeding slurry containing precious metal into the reactor space of each adsorption vessel;
feeding adsorption particles into the reactor space of each adsorption vessel, wherein precious metals are adsorbed into the adsorption particles;
moving the slurry through the plurality of adsorption vessels with a first drive system in a first flow direction so that the slurry moves through the retention screen in the reactor space of at least one adsorption vessel of the plurality of adsorption vessels into the closed retention space of the at least one adsorption vessel, wherein the adsorption particles cannot pass through the retention screen whereas the slurry passes through the retention screen;
moving the adsorption particles with a second drive system through the plurality of adsorption vessels in a second flow direction that is opposite the first direction;
arranging in the at least one adsorption vessel of said plurality of adsorption vessels first electrodes of a first probe in electrical contact with the slurry downstream of the retention screen in the first flow direction;
a first measurement step for either (i) supplying with first electrodes of the first probe a first supplied voltage to the slurry downstream of the retention screen in the first flow direction and receiving with first electrodes of the first probe a first received current from the slurry downstream of the retention screen in the first flow direction, or (ii) supplying with first electrodes of the first probe a first supplied current to the slurry downstream of the retention screen in the first flow direction and receiving with first electrodes of the first probe a first received voltage from the slurry downstream of the retention screen in the first flow direction;
arranging in the at least one adsorption vessel of the plurality of adsorption vessels second electrodes of a second probe in electrical contact with the slurry upstream of the retention screen in the first flow direction;
a second measurement step for either (i) supplying with the second electrodes of the second probe a second supplied voltage to the slurry upstream of the retention screen in the first flow direction and receiving with the second electrodes of the second probe a second received current from the slurry upstream of the retention screen in the first flow direction, or (ii) supplying with the second electrodes of the second probe a second supplied current to the slurry upstream of the retention screen in the first flow direction and receiving with the second electrodes of the second probe a second received voltage from the slurry upstream of the retention screen in the first flow direction;
functionally connecting a data processor device with the first probe and with the second probe;
calculating with the data processor device a first electrical property of the slurry downstream of the retention screen in the first flow direction either (i) based on a first difference between the first supplied current and the first received voltage, or (ii) based on a first difference between the first supplied voltage and the first received current;
calculating with the data processor device a second electrical property of the slurry upstream of the retention screen in the first flow direction either (i) based on a second difference between the second supplied current and the second received voltage, or (ii) based on a second difference between the second supplied voltage and the second received current;
by calculating with the data processor device the adsorption particle content of the slurry upstream of the retention screen in the first flow direction based on a difference between the first electrical property and the second electrical property;
connecting the data processor device to a source of adsorption particles; and
controlling the source of adsorption particles with the data processor device in response to the calculated adsorption particle content.

2. The method according to claim 1 , further comprising the steps of:
connecting the data processor device to the second drive system; and
controlling the second drive system with the data processor device in response to the calculated adsorption particle content.

3. The method according to claim 1 , further comprising the steps of:
connecting the data processor device to the first drive system; and
controlling the first drive system with the data processor device in response to the calculated adsorption particle content.

4. The method according to claim 1 , further comprising the steps of:
arranging a plurality of leaching reactors in series;
connecting the plurality of leaching reactors arranged in series being in fluid connection with the first inlet of the first adsorption vessel of the plurality of adsorption vessels in the first flow direction; and
feeding slurry containing precious metal with the plurality of leaching reactors arranged in series into the reactor space of the first adsorption vessel of said plurality of adsorption vessels in the first flow direction.

5. The method according to claim 1 , further comprising the steps of:
providing a stripping arrangement for stripping precious metal from adsorption particles; and
connecting the stripping arrangement for stripping precious metal from adsorption particles in fluid connection with the first outlet of the last adsorption vessel of the plurality of adsorption vessels in the second flow direction and in fluid connection with the second inlet of the first adsorption vessel of the plurality of adsorption vessels in the second flow direction.

6. The method according to claim 1 , further comprising the steps of:
extending the retention screen a first horizontal level in the reactor space and a second horizontal level in the reactor space, which second horizontal level is vertically below the first horizontal level; and
arranging the second electrodes of the second probe below the first horizontal level.

7. The method according to claim 1 , further comprising the steps of:
arranging a rotatable mixing means of a mixer above a third horizontal level in the reactor space, which third horizontal level is at a distance above a bottom of the reactor space; and
arranging the second electrodes of the second probe above a fourth horizontal level that is half-way between the bottom and the third horizontal level.

8. The method according to claim 1 , further comprising the steps of:
continuously supplying the first supplied voltage or the first supplied current and continuously receiving the first received voltage or the first received current in the first measurement step for a time period between 10 s and 5 min.

9. The method according to claim 1 , further comprising the steps of:
continuously supplying the second supplied voltage or second supplied current and continuously receiving the second received voltage or second received current in the second measurement step for a time period between 10 s and 5 min.

10. A system for recovery of precious metal, the system compri

Assignees

• Outotec Finland Oy

Inventors

• Latva-Kokko Marko
• Kourunen Jari

Classifications

• C22B3/02 Primary

  Apparatus therefor · CPC title

• B01J47/14

  Controlling or regulating · CPC title

• C22B11/04 Primary

  by wet processes (extraction of metal compounds by leaching in organic solutions C22B3/16; treatment or purification of solutions by liquid-liquid extraction C22B3/26) · CPC title

• C22B3/24

  by adsorption on solid substances, e.g. by extraction with solid resins · CPC title

• Y02P10/234

  Cross-Sectional Technologies · mapped topic