Electrode and process for preparing the electrode and devices thereof

Patent metadata

Field	Value
Publication number	US-10395853-B2
Application number	US-201615175629-A
Country	US
Kind code	B2
Filing date	Jun 7, 2016
Priority date	Jun 7, 2016
Publication date	Aug 27, 2019
Grant date	Aug 27, 2019

Abstract

An electrode, process for preparing the electrode and devices thereof. An electrode comprising at least one metal deposited on a substrate; and at least one electrically conducting polymer. The devices comprising the electrode for energy storage and molecular separation.

First claim

I claim:

1. A process for preparation of an electrode, wherein the process step comprises:
a) immersing a substrate in brewed green tea for a period of time in the range of 1-24 hours to obtain a modified substrate;
b) immersing the modified substrate as obtained from step (a) in an ammonical AgNO3 solution for a period of time in the range of 10 minutes-8 hours to obtain silver nanoparticle coated substrate;
c) keeping the silver nanoparticle coated substrate as obtained from step (b) in a metal plating solution of the pH ranging between 7-10 for a period of time in the range of 8-24 hours to obtain a metal coated substrate; and
d) polymerizing a monomer on the metal coated substrate as obtained from step (c) by soaking in electrically conducting solution for a period of time in the range of 5-30 minutes to obtain an electrode.

2. The process as claimed in claim 1 , wherein the metal is selected from the group consisting of gold, palladium, nickel and copper.

3. The process as claimed in claim 1 , wherein the substrate is selected from the group consisting of silk cocoons, silk yarn, cotton clothes, cotton threads papers, tree leaves and synthetic substrates.

4. The process as claimed in claim 3 , wherein the synthetic substrate is selected from the group consisting of polycarbonate membranes, anodized alumina oxide membranes, glass slides and conducting glasses.

5. The process as claimed in claim 4 , wherein the conducting glasses is selected from the group consisting of indium doped tin oxide and fluorine doped tin oxide.

6. The process as claimed in claim 1 , wherein the monomer in the electrically conducting solution includes a monomer of the material selected from the group consisting of polyaniline, polyethylene dioxythiophene, polypyrrole and derivatives of polythiophene.

7. The process as claimed in claim 1 , wherein the substrate is not already treated with brewed green tea prior to immersing the substrate in brewed green tea, and wherein immersing the modified substrate as obtained from step (a) includes immersing the modified substrate in ammonical AgNO 3 without immersing the modified substrate in brewed green tea for longer than 24 hours.

8. The process as claimed in claim 7 , wherein polymerizing the monomer includes polymerizing the monomer without keeping the silver nanoparticle coated substrate in the metal plating solution for more than 24 hours.

9. The process as claimed in claim 1 , wherein polymerizing the monomer includes polymerizing the monomer without keeping the silver nanoparticle coated substrate in the metal plating solution for more than 24 hours.

Assignees

• Council Scient Ind Res

Inventors

• Krishnamoorthy Kothandam

Classifications

• D06M15/61

  Polyamines {polyimines} · CPC title

• D06M23/08

  Processes in which the treating agent is applied in powder or granular form (adhesives for multi-layer textile fabrics D06M17/00) · CPC title

• C23C18/2066

  Use of organic or inorganic compounds other than metals, e.g. activation, sensitisation with polymers · CPC title

• C23C18/44

  using reducing agents · CPC title

• H01G11/22

  Electrodes · CPC title